WO2009000657A2 - Composant comportant une couche céramique contenant un colorant et procédé de fabrication - Google Patents
Composant comportant une couche céramique contenant un colorant et procédé de fabrication Download PDFInfo
- Publication number
- WO2009000657A2 WO2009000657A2 PCT/EP2008/057339 EP2008057339W WO2009000657A2 WO 2009000657 A2 WO2009000657 A2 WO 2009000657A2 EP 2008057339 W EP2008057339 W EP 2008057339W WO 2009000657 A2 WO2009000657 A2 WO 2009000657A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- layer
- nanoparticles
- layers
- dye
- component
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
- C23C28/40—Coatings including alternating layers following a pattern, a periodic or defined repetition
- C23C28/42—Coatings including alternating layers following a pattern, a periodic or defined repetition characterized by the composition of the alternating layers
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
- C23C18/1208—Oxides, e.g. ceramics
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/1225—Deposition of multilayers of inorganic material
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/125—Process of deposition of the inorganic material
- C23C18/1262—Process of deposition of the inorganic material involving particles, e.g. carbon nanotubes [CNT], flakes
- C23C18/127—Preformed particles
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
- C23C28/04—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material
- C23C28/042—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material including a refractory ceramic layer, e.g. refractory metal oxides, ZrO2, rare earth oxides
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
- C23C28/04—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material
- C23C28/044—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material coatings specially adapted for cutting tools or wear applications
Definitions
- the invention relates to a component having a ceramic layer forming the surface, wherein the layer is composed of a plurality of layers and incorporated in the microstructure of the layer nanoparticles of a particular dye.
- Such a component is for example from DE
- Turbine blade having a preferably multi-layered layer.
- the layers of such turbine blades have different functions, including the thermal load on the turbine blade and a corrosive attack to prevent or at least reduce.
- thermal overloading of the blade can not be completely ruled out due to operational reasons.
- a dye in the form of nanoparticles is contained in the layer matrix, which causes a color change in thermal stresses that are too large for the component.
- a ther- mal overload of the turbine blade can also nachwei ⁇ sen when the state it has been overload already canceled.
- the object of the invention is to specify a component with a ceramic layer forming the surface, in the matrix of which nanoparticles of a particular dye are incorporated, which permit extended statements about the state of the layer.
- This object is achieved by the initially mentioned component ⁇ he inventively characterized in that the nanoparticles are incorporated into the structural matrix of a layer, adjacent to the layers that have an identical structural matrix without this dye.
- a color change of the surface layer can be regarded as a particular state of wear of the layer.
- wear state is meant in this context, a removal of the layer surface.
- the location may be with the nanoparticles of a ⁇ be approved dye provided in a layer depth, which is considered borderline for the necessity of the exchange of a particular component. As soon as the dye shows on the surface of the layer, this means that an exchange of the relevant component is due.
- AOI automatic optical inspection
- the fiction, modern ⁇ component can be produced particularly advantageously by using a coating material is applied which consist of Kera ⁇ mix precursors for the ceramic to be produced, a suitable solvent for these precursors and the nanoparticles of the specific dye.
- a coating material is applied which consist of Kera ⁇ mix precursors for the ceramic to be produced, a suitable solvent for these precursors and the nanoparticles of the specific dye.
- the solvent is evaporated and initiated a reaction in which the ceramic precursors react to the desired ceramic.
- the dye must have a temperature stability, so that he endures the heat treatment to form the ceramic layer layer.
- the method of applying ceramic precursors to metallic components to form ceramic layers on these components is known per se, and is described, for example, in US 2002/0086111 A1, WO 2004/013378 A1, US 2002/0041928 A1, US Pat WO 03/021004 A1 and WO 2004/104261 Al.
- the processes described in these documents are concerned with the production of ceramic coatings on components in general, using ceramic
- precursors for the ceramics which are often referred to as precursor, include the materials that make up the ceramic material of the trainee layer and also have components that in the context of the running during the heat treatment of the Besichtungsstoffes chemical conversion to a Crosslinking of the ceramic material lead. Examples of ceramic precursors can be found in the documents listed in the prior art and must be selected depending on the application.
- the ceramic to be formed consists of an oxide or a nitride.
- the formation of oxides, nitrides or oxynitrides can advantageously produce particularly stable layers.
- the precursors of such ceramics must provide the elements N and O, respectively, for the formation of the oxide, nitridic or oxynitridic ceramics.
- nanoparticles of another dye are incorporated in at least one of the adjacent layers.
- ⁇ by advantageous additional statements are possible. So z. B. the progressive Schichtabtrag be followed in layers with ⁇ , since every time a new situation is reached, a color change is observed.
- the invention relates to a method for producing a layer on a component, in which a layer of the layer is produced by applying to the component a coating material consisting of a solvent, the dissolved precursors of a ceramic and dispersed nanoparticles.
- a coating material consisting of a solvent, the dissolved precursors of a ceramic and dispersed nanoparticles.
- the provided with the coating material of construction ⁇ part is then subjected to a heat treatment in which the solvent evaporates and the precursors of the ceramic under incorporation of the nanoparticles umgewan- be punched in the ceramic sheet.
- a method is described in the initially set ⁇ led prior art. This produces layers that are also referred to as C3 coatings by various manufacturers.
- the object of the invention is further to provide a manufacturing process for layers with nanoparticles, with the layers can be produced which extended information about the condition of the layer during operation he ⁇ possible.
- This object is achieved with the method-called in that nanoparticles of a color substance ⁇ be used, are the adjacent layers provided with the nanoparticles position without these nanoparticles Herge ⁇ represents.
- An embodiment of the method provides that the Benach ⁇ disclosed documents will be made ⁇ without any coloring nanoparticles ago.
- Another embodiment of the invention provides that the adjacent layers are produced with nanoparticles of another dye. This will achieves the already mentioned advantages that can be displayed visually as the wear of the layer height profiles that allow a precise optical analysis of the wear state Ver ⁇ .
- All multi-layer layers 11 are produced on an indicated component 12 and each form its surface 13.
- three layers 14a are produced without nanoparticles of a particular dye.
- a layer 14b is doped with nanoparticles 15b of a particular dye, which are incorporated into the matrix of this layer.
- the subsequent to the surface layer 14a is slowly consumed. This is removed down to the position 14b, there is a color change, said layer thickness then a degree he ⁇ ranges, which requires an exchange of the component or a retrieval ⁇ preparation of the layer.
- the layer 11 could be, for example, a temperature protection for a turbine blade.
- a layer 11 with a layer sequence is Darge ⁇ provides at which nanoparticle 15b of a single specific dye alternate layers 14a without a dye layers 14b to each other.
- layer sequences with another pattern change so z.
- FIG. 3 is very similar to that of FIG. Instead of the layers without a dye, however, layers 14c with nanoparticles of another specific dye are provided here in alternation with the layers 14b with nanoparticles of a specific material.
- This has the advantage that, depending on the color of the current layer surface is to determine directly to what extent the removal of the layer is already advanced. For this purpose, only the knowledge of the layer structure is necessary so the current surface color of the layer can be assigned to a specific layer depth.
- Possible dyes are preferably ceramic compounds, as described in the already mentioned DE
- a base precursor 1 consisting of 70% zirconium (IV) 2-ethylhexanoate, 3% yttrium (III) 2-ethylhexanoate and 27% propionic acid
- 2nd step Preparation of a base precursor 2 consisting of the binder (58% zirconium (IV) 2-ethylhexanoate, 3% yttrium (III) 2-ethylhexanoate and 39% hexanoic acid) and 1% iron (III) oxide to produce a red color
- 3rd step Preparation of a cover precursor consisting of the binder (58% zirconium (IV) 2-ethylhexanoate, 3% yttrium (III) 2-ethylhexanoate and 39% hexanoic acid) and 2% nanoaluminum oxide, and 1% CrAlCo oxide for the petrol-green color of the topcoat
- 1st step Preparation of a base precursor 1 consisting of 58% zirconium (IV) 2-ethylhexanoate, 3% yttrium (III) 2-ethylhexanoate and 39% acetic acid and 1% CrAlCo oxide for petrol-green dyeing
Abstract
L'invention concerne un composant (12) comportant une couche (11) formant la surface (13), composée de plusieurs strates (14a, 14b). Selon l'invention, seules certaines strates (14b) de la couche (11) sont pourvues de nanoparticules (15b) d'un ou plusieurs colorants prédéterminés. De manière avantageuse, les strates colorées (14b) sont ainsi rendues visibles en cas d'usure (18), ce qui permet d'évaluer l'état d'usure de la couche (11) par une simple inspection optique. L'invention concerne également un procédé de fabrication de telles couches de préférence composées de précurseurs précéramiques.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102007030588A DE102007030588A1 (de) | 2007-06-27 | 2007-06-27 | Bauteil mit einer einen Farbstoff enthaltenden keramischen Schicht und Verfahren zu deren Herstellung |
DE102007030588.7 | 2007-06-27 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2009000657A2 true WO2009000657A2 (fr) | 2008-12-31 |
WO2009000657A3 WO2009000657A3 (fr) | 2009-08-06 |
Family
ID=40030261
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/EP2008/057339 WO2009000657A2 (fr) | 2007-06-27 | 2008-06-12 | Composant comportant une couche céramique contenant un colorant et procédé de fabrication |
Country Status (2)
Country | Link |
---|---|
DE (1) | DE102007030588A1 (fr) |
WO (1) | WO2009000657A2 (fr) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2011901A1 (fr) | 2007-06-28 | 2009-01-07 | Siemens Aktiengesellschaft | Composant doté d'une couche céramique dans laquelle sont dispergées des particules et son procédé de fabrication |
WO2010136338A2 (fr) * | 2009-05-27 | 2010-12-02 | Siemens Aktiengesellschaft | Procédé pour produire une couche contenant des particules absorbant un rayonnement d'énergie |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102017216579B4 (de) * | 2017-09-19 | 2019-06-19 | Ford Global Technologies, Llc | Verfahren zur Herstellung einer Fertigungsvorrichtung |
DE102018107998B4 (de) * | 2018-04-05 | 2020-06-04 | Bystronic Laser Ag | Biegewerkzeug, Maschinentisch und Anschlagelement für eine Biegemaschine, Biegemaschine und Verfahren zur Verschleißerkennung |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4774150A (en) * | 1986-03-07 | 1988-09-27 | Kabushiki Kaisha Toshiba | Thermal barrier coating |
US6620525B1 (en) * | 2000-11-09 | 2003-09-16 | General Electric Company | Thermal barrier coating with improved erosion and impact resistance and process therefor |
US6827969B1 (en) * | 2003-12-12 | 2004-12-07 | General Electric Company | Field repairable high temperature smooth wear coating |
EP1645538A1 (fr) * | 2004-10-05 | 2006-04-12 | Siemens Aktiengesellschaft | Compositions de materiaux destinees pour produire un revêtement sur un objet metallique et un composant métallique revêtu |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20020041928A1 (en) | 1997-03-26 | 2002-04-11 | Leonid V. Budaragin | Method for coating substrate with metal oxide coating |
US20020086111A1 (en) | 2001-01-03 | 2002-07-04 | Byun Jeong Soo | Method of forming refractory metal nitride layers using chemisorption techniques |
WO2003021004A1 (fr) | 2001-08-30 | 2003-03-13 | The University Of Dundee | Procede pour produire des composites en ceramique-metal en films minces poreux et composites obtenus par ce procede |
EP1386983B2 (fr) | 2002-07-31 | 2010-06-09 | ItN NANOVATION GMBH | Revêtement en céramique pour une chaudière |
DE102005047739B3 (de) | 2005-09-29 | 2007-02-08 | Siemens Ag | Substrat mit aufgebrachter Beschichtung, und Herstellungsverfahren |
-
2007
- 2007-06-27 DE DE102007030588A patent/DE102007030588A1/de not_active Withdrawn
-
2008
- 2008-06-12 WO PCT/EP2008/057339 patent/WO2009000657A2/fr active Application Filing
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4774150A (en) * | 1986-03-07 | 1988-09-27 | Kabushiki Kaisha Toshiba | Thermal barrier coating |
US6620525B1 (en) * | 2000-11-09 | 2003-09-16 | General Electric Company | Thermal barrier coating with improved erosion and impact resistance and process therefor |
US6827969B1 (en) * | 2003-12-12 | 2004-12-07 | General Electric Company | Field repairable high temperature smooth wear coating |
EP1645538A1 (fr) * | 2004-10-05 | 2006-04-12 | Siemens Aktiengesellschaft | Compositions de materiaux destinees pour produire un revêtement sur un objet metallique et un composant métallique revêtu |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2011901A1 (fr) | 2007-06-28 | 2009-01-07 | Siemens Aktiengesellschaft | Composant doté d'une couche céramique dans laquelle sont dispergées des particules et son procédé de fabrication |
EP2011901B1 (fr) * | 2007-06-28 | 2017-10-18 | Siemens Aktiengesellschaft | Composant doté d'une couche céramique dans laquelle sont dispergées des particules et son procédé de fabrication |
WO2010136338A2 (fr) * | 2009-05-27 | 2010-12-02 | Siemens Aktiengesellschaft | Procédé pour produire une couche contenant des particules absorbant un rayonnement d'énergie |
WO2010136338A3 (fr) * | 2009-05-27 | 2011-01-27 | Siemens Aktiengesellschaft | Procédé pour produire une couche contenant des particules absorbant un rayonnement d'énergie |
CN102449191A (zh) * | 2009-05-27 | 2012-05-09 | 西门子公司 | 含有用于能量辐射的吸收颗粒的层的制造方法 |
US9200370B2 (en) | 2009-05-27 | 2015-12-01 | Siemens Aktiengesellschaft | Method for fabricating a layer with absorbing particles for an energy radiation |
Also Published As
Publication number | Publication date |
---|---|
DE102007030588A1 (de) | 2009-01-02 |
WO2009000657A3 (fr) | 2009-08-06 |
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