WO2008004462A1 - Appareil de diagnostic de panne de détecteur de gaz d'échappement - Google Patents
Appareil de diagnostic de panne de détecteur de gaz d'échappement Download PDFInfo
- Publication number
- WO2008004462A1 WO2008004462A1 PCT/JP2007/062785 JP2007062785W WO2008004462A1 WO 2008004462 A1 WO2008004462 A1 WO 2008004462A1 JP 2007062785 W JP2007062785 W JP 2007062785W WO 2008004462 A1 WO2008004462 A1 WO 2008004462A1
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- WIPO (PCT)
- Prior art keywords
- exhaust gas
- abnormality diagnosis
- sensor
- gas sensor
- satisfied
- Prior art date
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Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
- G01N27/416—Systems
- G01N27/417—Systems using cells, i.e. more than one cell and probes with solid electrolytes
- G01N27/4175—Calibrating or checking the analyser
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02D—CONTROLLING COMBUSTION ENGINES
- F02D41/00—Electrical control of supply of combustible mixture or its constituents
- F02D41/02—Circuit arrangements for generating control signals
- F02D41/14—Introducing closed-loop corrections
- F02D41/1438—Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor
- F02D41/1444—Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor characterised by the characteristics of the combustion gases
- F02D41/1454—Introducing closed-loop corrections using means for determining characteristics of the combustion gases; Sensors therefor characterised by the characteristics of the combustion gases the characteristics being an oxygen content or concentration or the air-fuel ratio
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F02—COMBUSTION ENGINES; HOT-GAS OR COMBUSTION-PRODUCT ENGINE PLANTS
- F02D—CONTROLLING COMBUSTION ENGINES
- F02D41/00—Electrical control of supply of combustible mixture or its constituents
- F02D41/22—Safety or indicating devices for abnormal conditions
- F02D41/222—Safety or indicating devices for abnormal conditions relating to the failure of sensors or parameter detection devices
Definitions
- the present invention relates to an abnormality diagnosis device for an exhaust gas sensor, and more particularly to an abnormality diagnosis device for an exhaust gas sensor suitable as a device for detecting a sensor element crack in the exhaust gas sensor.
- an abnormality caused by element cracking of an oxygen sensor (hereinafter also simply referred to as “sensor”) disposed in an exhaust passage of an internal combustion engine is detected.
- the oxygen sensor includes a sensor element interposed between the atmosphere and the exhaust gas, and a voltage corresponding to the difference in oxygen partial pressure between the air in the atmosphere layer and the exhaust gas is output. The When the voltage value is an output pattern indicating that the difference in oxygen partial pressure is small or reversed, it is determined that the sensor element is defective, and an abnormality diagnosis is performed. That's right.
- Patent Document 1 Japanese Unexamined Patent Publication No. 2003-14683
- Patent Document 2 Japanese Unexamined Patent Publication No. 2004-353494
- Patent Document 3 Japanese Patent No. 3562030
- the output of the abnormality sensor may show the same output pattern as in the normal state, or A normal oxygen sensor output may show a similar output pattern when an element crack anomaly occurs. More specifically, for example, in a situation where the exhaust gas force is lean, even if the sensor element is cracked and the exhaust gas enters the atmospheric layer from the defect, the oxygen partial pressure does not decrease, An output pattern similar to a normal sensor can be obtained. In addition, depending on the amount of intake air of the internal combustion engine, it may be assumed that even if the sensor element is cracked, the exhaust gas does not enter the atmosphere layer from the defect and the oxygen partial pressure does not decrease. For this reason, there is a risk that an oxygen sensor with a broken element may be mistakenly determined to be normal. It was insufficient as an abnormal diagnosis device.
- the present invention has been made to solve the above-described problems, and it is an object of the present invention to provide an abnormality diagnosis device for an exhaust gas sensor capable of accurately diagnosing an abnormality caused by element cracks in the exhaust gas sensor.
- the first invention is an abnormality diagnosis device for an exhaust gas sensor
- a sensor element is provided in the exhaust passage of the internal combustion engine and interposed between the external air and the exhaust gas, and generates an output signal having a correlation with a difference in oxygen partial pressure between the external air and the exhaust gas.
- Determination means for determining whether or not an execution condition for performing an abnormality diagnosis of an element crack of the exhaust gas sensor is satisfied
- An abnormality diagnosis means for executing the abnormality diagnosis based on an output signal of the exhaust gas sensor when the execution condition is satisfied
- the determination means determines that the execution condition is not satisfied in a lean period in which the air-fuel ratio force S of the exhaust gas is lean.
- the second invention is the same as the first invention
- the lean period includes a period during which a fuel cut of the internal combustion engine is executed.
- the third invention is the first or second invention, wherein
- the abnormality diagnosis means executes the abnormality diagnosis based on an output signal of the exhaust gas sensor during a period when the air-fuel ratio force S of the exhaust gas is lean.
- the fourth invention is an exhaust gas sensor abnormality diagnosis device
- a sensor element is provided in the exhaust passage of the internal combustion engine and interposed between the external air and the exhaust gas, and generates an output signal having a correlation with a difference in oxygen partial pressure between the external air and the exhaust gas.
- Determination means for determining whether or not an execution condition for performing an abnormality diagnosis of an element crack of the exhaust gas sensor is satisfied;
- An abnormality diagnosis means for executing the abnormality diagnosis based on an output signal of the exhaust gas sensor when the execution condition is satisfied,
- the determination means includes
- It includes an integrated intake air amount acquisition means for acquiring an integrated value of the intake air amount of the internal combustion engine, and determines that the execution condition is satisfied when the integrated value is equal to or greater than a predetermined value.
- the fifth invention is the fourth invention, wherein
- the integrated intake air amount obtaining means resets the integrated value when the air-fuel ratio force S lean of the exhaust gas is reached.
- the sixth invention is the fourth or fifth invention, wherein
- the integrated intake air amount acquisition means resets the integrated value when the intake air amount becomes a predetermined value or less.
- the seventh invention is an exhaust gas sensor abnormality diagnosis device
- a sensor element is provided in the exhaust passage of the internal combustion engine and interposed between the external air and the exhaust gas, and generates an output signal having a correlation with a difference in oxygen partial pressure between the external air and the exhaust gas.
- Determination means for determining whether or not an execution condition for performing an abnormality diagnosis of an element crack of the exhaust gas sensor is satisfied
- An abnormality diagnosis means for executing the abnormality diagnosis based on an output signal of the exhaust gas sensor when the execution condition is satisfied
- the abnormality diagnosing means includes canceling means for canceling establishment of the execution condition when a state where the intake air amount of the internal combustion engine is equal to or less than a predetermined value continues for a predetermined time.
- the exhaust gas sensor abnormality diagnosis is prohibited during the lean period during which the air-fuel ratio S of the exhaust gas is lean.
- Fuel lean exhaust gas has a high oxygen partial pressure. For this reason, even if such exhaust gas flows from the element cracking portion of the sensor element to the external air side, a sensor output signal for detecting an element cracking abnormality cannot be detected. others Therefore, according to the present invention, by prohibiting the execution of abnormality diagnosis during a powerful period, it is possible to prevent a sensor in which an element crack abnormality has occurred from being erroneously determined to be normal, and to prevent an element crack abnormality. Detection accuracy can be increased.
- the second aspect of the invention it is possible to prohibit abnormality diagnosis of the exhaust gas sensor during the period when the fuel cut of the internal combustion engine is being executed. During the fuel cut, air flows through the exhaust passage. For this reason, according to the present invention, by prohibiting abnormality diagnosis during such a period, it is possible to prevent a sensor in which an element crack abnormality has occurred from being erroneously determined to be normal, and to detect an element crack abnormality. Accuracy can be increased.
- an abnormality diagnosis of the exhaust gas sensor is executed.
- the exhaust gas sensor abnormality diagnosis execution condition is canceled when a state where the intake air amount Ga is extremely small continues for a predetermined time. If the intake air amount Ga is small, the exhaust gas that has flowed from the exhaust passage side of the cracked part of the element into the external air side may flow out to the exhaust passage side again. If the state of being applied continues, the sensor output signal corresponding to the presence or absence of sensor abnormality cannot be detected. For this reason, according to the present invention, when the low Ga state continues for a predetermined time, the execution of the abnormality diagnosis is canceled, and the sensor in which the element crack abnormality has occurred is erroneously determined to be normal by judging the execution condition again. It is possible to prevent the judgment and improve the detection accuracy of the element crack abnormality.
- FIG. 1 is a diagram for explaining a configuration of a first embodiment of the present invention.
- FIG. 2 is a diagram for explaining a configuration of an oxygen sensor used in Embodiment 1 of the present invention.
- FIG. 3 is a diagram for explaining the principle of oxygen sensor abnormality diagnosis. 4] This is a diagram showing the relationship with the time required for the sensor output to drop when a steady operation with a certain intake air amount Ga is executed after an element crack occurs in the sensor.
- FIG. 1 is a diagram for explaining a hardware configuration according to the first embodiment of the present invention.
- the system of this embodiment includes an internal combustion engine 10.
- An intake passage 12 and an exhaust passage 14 communicate with the internal combustion engine 10.
- An air flow meter 16 for detecting the amount of intake air is disposed in the intake passage 12.
- a throttle valve 18 is disposed downstream of the air flow meter 16. In the vicinity of the throttle valve 18, a slot sensor 20 for detecting the throttle opening is arranged.
- Each cylinder of the internal combustion engine 10 is provided with an injector 22 for injecting fuel into the intake port.
- a crank angle sensor 26 for detecting the rotation angle of the crankshaft 24 is attached in the vicinity of the crankshaft 24 of the internal combustion engine. According to the output of the crank angle sensor, the rotational position of the crankshaft 24, the engine speed NE, and the like can be detected.
- Catalyst 28 is disposed in the exhaust passage 14 of the internal combustion engine 10.
- Catalyst 28 is a three-way catalyst that simultaneously removes harmful components in exhaust gas such as C0, HC (hydrocarbon), and NO near the stoichiometric air-fuel ratio.
- an air-fuel ratio sensor (A / F sensor) 30 is disposed upstream of the catalyst 28.
- the air-fuel ratio sensor 30 is a sensor that linearly detects the oxygen concentration in the exhaust gas, and based on the oxygen concentration in the exhaust gas flowing into the catalyst 28, the air-fuel ratio of the air-fuel mixture burned in the internal combustion engine 10 Is detected.
- an oxygen sensor 40 is disposed downstream of the catalyst 28.
- the oxygen sensor 40 is a sensor for detecting whether the oxygen concentration in the exhaust gas is larger or smaller than a predetermined value, and when the exhaust air-fuel ratio at the sensor position becomes richer than the stoichiometric fuel, a predetermined voltage (for example, 0) is detected. When the exhaust air / fuel ratio becomes leaner than the stoichiometric output, the output is below the specified voltage. For this reason, according to the oxygen sensor 40, fuel-rich exhaust gas (exhaust gas containing HC and C0) or fuel-lean exhaust gas is formed downstream of the catalyst 28. It is possible to judge whether gas (exhaust gas containing NO) has flowed out.
- the apparatus includes an ECU (Electronic Control Unit) 70.
- the ECU 70 is connected to the various sensors described above, the injector 22, and the like.
- the ECU 70 can control the operating state of the internal combustion engine 10 based on the sensor outputs.
- FIG. 2 is a diagram for explaining the configuration of the oxygen sensor 40 used in Embodiment 1 of the present invention.
- the oxygen sensor 40 shown in FIG. 2 is a sensor that is disposed in the exhaust passage 14 of the internal combustion engine 10 and used to detect the air-fuel ratio of the exhaust gas downstream of the catalyst 28.
- the oxygen sensor 40 includes a cover 42 and is assembled in the exhaust passage 14 so that the cover 42 is exposed to the exhaust gas.
- the cover 42 is provided with a hole (not shown) for introducing exhaust gas therein.
- a sensor element 44 is arranged inside the cover 42.
- the sensor element 44 has a tubular structure with one end (the lower end in FIG. 2) closed.
- the outer surface of the tubular structure is covered with a diffusion resistance layer 46.
- the diffusion resistance layer 46 is a heat-resistant porous material such as alumina and has a function of regulating the diffusion rate of the exhaust gas near the surface of the sensor element 44.
- An exhaust side electrode 48, a solid electrolyte layer 50, and an atmosphere side electrode 52 are provided inside the diffusion resistance layer 46.
- the exhaust side electrode 48 and the atmosphere side electrode 52 are electrodes made of a noble metal having a high catalytic action like Pt, and are electrically connected to a control circuit described later.
- the solid electrolyte layer 50 is a sintered body containing ZrO and the like, and conducts oxygen ions.
- an atmosphere chamber 54 that is open to the atmosphere is formed inside the sensor element 44.
- a heater 56 for heating the sensor element 44 is disposed in the atmospheric chamber 54.
- the sensor element 44 exhibits stable output characteristics at an activation temperature of about 400 ° C.
- the heater 56 is electrically connected to the control circuit, and can keep the sensor element 44 heated to an appropriate temperature.
- FIG. 4 is a diagram for explaining the state of the environment around the oxygen sensor 40 disposed in the exhaust passage 14 of the internal combustion engine 10.
- the oxygen sensor 40 generates a sensor output corresponding to the difference in oxygen concentration between the atmosphere layer 54 side and the exhaust passage 14 side of the sensor element 44.
- FIG. 3 (A) when the oxygen sensor 40 is in a normal state, that is, when the sensor element 44 is not defective, the exhaust gas flowing in the exhaust passage 14 is mixed into the atmospheric layer 54. None do. For this reason, the oxygen concentration is always lower on the exhaust passage 14 side than on the atmosphere layer 54 side, and the output of the normal oxygen sensor 40 always generates a positive voltage value.
- FIG. 3B shows a state in which element cracking has occurred in the sensor element 44.
- the exhaust gas in the exhaust passage 14 is pushed by the exhaust pressure and may enter the inside of the atmospheric layer 54 from the element crack portion 60. In such a case, there is no difference in oxygen concentration between the air layer 54 side and the exhaust passage 14 side of the sensor element 44, and no sensor output is generated.
- FIG. 3 (C) is a diagram showing the state of the environment around the oxygen sensor 40 when the fuel cut is executed in the internal combustion engine 10 after the state of FIG. 3 (B).
- a fuel cut that temporarily stops fuel injection is frequently performed according to an operating state or the like.
- the air flows in the exhaust passage 14. Therefore, as shown in FIG. 3 (C), if a fuel cut is performed after the exhaust gas has entered the atmosphere layer 54 from the element cracking portion 60 of the oxygen sensor 40, the sensor element 44 and the atmosphere layer 54 side are exhausted.
- the oxygen concentration difference on the passage 14 side reverses and a negative voltage is generated at the sensor. Therefore, by detecting the negative voltage from the sensor output, it is possible to detect the sensor element crack with high accuracy.
- the abnormality diagnosis of the oxygen sensor is performed further considering the following conditions.
- the time integrated value SUM_Ga of the intake air amount Ga is equal to or greater than the amount of air that the exhaust gas can flow into the atmosphere layer 54, the abnormality of the oxygen sensor described above. A diagnosis will be made. As a result, it is possible to prevent a sensor in which an element crack abnormality has occurred from being erroneously determined to be normal, and to improve the detection accuracy of the element crack abnormality.
- FIG. 5 shows the relationship between the duration when the predetermined low Ga value continues after the integrated value SUM_Ga of the intake air amount Ga becomes equal to or greater than the predetermined value and the negative voltage value generated. .
- the absolute value of the negative voltage value tends to decrease as the duration of the low Ga value increases.
- the absolute value of the negative voltage value tends to decrease as the low Ga value decreases.
- the exhaust gas gas that has flowed into the atmospheric layer 54 of the sensor and the oxygen gas described above when the low Ga state that flows out again continues for a certain period of time. Execution of abnormal diagnosis is prohibited. As a result, it is possible to prevent the sensor in which the element crack abnormality has occurred from being erroneously determined to be normal, and to increase the detection accuracy of the element crack abnormality.
- the exhaust gas flowing through the exhaust passage 14 may become fuel lean due to the influence of the operating state of the internal combustion engine or the like. More specifically, fuel-lean exhaust gas circulates in the exhaust passage 14 during a period in which forced lean control or fuel cut is performed.
- lean gas has a high oxygen concentration. For this reason, even if a lean gas flows from the cracked part of the element and a fuel cut is performed after that, it is difficult for the oxygen partial pressure difference to occur in the sensor element 44. It becomes difficult.
- abnormality diagnosis of the oxygen sensor when the exhaust gas is fuel lean is prohibited. As a result, it is possible to prevent a sensor in which an element crack abnormality has occurred from being mistakenly determined to be normal, and to improve the detection accuracy of the element crack abnormality.
- FIG. 6 is a flowchart of a routine for diagnosing an element crack abnormality of the ECU70 force oxygen sensor 40.
- the routine shown in FIG. 6 it is first determined whether or not the precondition is satisfied (step 100).
- the precondition is satisfied (step 100).
- the warm-up state of the internal combustion engine 10 the vehicle speed, the engine speed NE, the active state of the oxygen sensor 40, etc. satisfy the preconditions for executing the abnormality diagnosis.
- step 104 it is next determined whether or not the state of the exhaust gas is lean (step 104).
- the state of the exhaust gas is determined based on whether or not the operating state of the internal combustion engine 10 is during fuel cut or whether or not forced lean control is being performed. It is determined whether or not is lean.
- the routine proceeds to step 102, where the accumulated Ga is reset, and then the present routine is executed again from the beginning.
- step 106 If it is determined in step 106 that the intake air amount Ga has reached the lower limit value, an integrated Ga (SUM_Ga) that is a time integrated value of the intake air amount Ga is then calculated. (Step 108). Here, specifically, the time integrated value of the intake air amount Ga after being reset to zero in step 102 is calculated.
- step 110 it is determined whether the integrated Ga (SUM_Ga) is greater than or equal to a predetermined amount (step 110).
- SUM_Ga 1500 (g)
- Step 112 it is determined that the condition that the exhaust gas is not lean in step 104 and the condition that SUM_Ga in step 110 is greater than or equal to the predetermined amount are satisfied, and the process proceeds to a process for detecting a sensor output described later.
- step 120 it is next determined whether or not the state of the exhaust gas is lean (step 120).
- the state of the exhaust gas is lean based on whether or not the operating state of the internal combustion engine 10 is during fuel cut or whether or not forced lean control is in progress. It is judged whether or not.
- step 120 If it is determined in step 120 that the exhaust gas state is lean, it is next determined whether or not a negative voltage is generated in the output voltage of the oxygen sensor 40 (step 122). As described above, if the exhaust gas state becomes lean when the negative voltage determination condition is set, if there is a sensor with element cracking, the sensor element 44 and the exhaust gas side The oxygen partial pressure with the side is reversed. For this reason, it is possible to accurately determine whether or not the sensor is abnormal by determining whether or not the sensor output has a negative voltage. As a result, when a negative voltage is not generated in the output voltage of the oxygen sensor 40, a normal determination is performed (step 124), and when a negative voltage is generated in the output voltage, an abnormality determination is performed (step 126). ).
- step 130 determines that the intake air amount Ga is smaller than the lower limit value
- the process proceeds to the next step, and a low Ga continuation counter (Ga_CNT) is counted (step 1 32).
- Ga_CNT low Ga continuation counter
- step 134 it is determined whether or not Ga_CNT counted in step 132 is equal to or longer than a predetermined time (step 134).
- the predetermined time is specified as the time (for example, 10 (s)) that exhaust gas that has entered the atmosphere layer 54 flows out to the extent that failure diagnosis cannot be performed thereafter.
- the process returns to step 120 again to determine the air-fuel ratio state of the exhaust gas. .
- step 102 SUM_Ga is reset to zero, and this routine is executed again from the beginning.
- the abnormality diagnosis of the oxygen sensor 40 is performed when the integrated value SUM —Ga of the intake air amount Ga is equal to or greater than a predetermined value.
- the abnormality diagnosis is executed only when the exhaust gas can surely enter the atmosphere layer from the element crack. For this reason, it is possible to prevent the sensor in which the element crack abnormality has occurred from being erroneously determined to be normal, and to improve the detection accuracy of the element crack abnormality.
- abnormality diagnosis of the oxygen sensor when the exhaust gas is fuel lean is prohibited.
- the exhaust gas surely enters the atmosphere layer from the cracked part of the element, there is an abnormality when there is no oxygen partial pressure difference between the exhaust gas side and the atmosphere layer side. Diagnosis is prohibited. For this reason, it is possible to prevent a sensor in which an element crack abnormality has occurred from being erroneously determined to be normal, and to improve the detection accuracy of the element crack abnormality.
- the element crack abnormality diagnosis is executed for the oxygen sensor 40 arranged downstream of the catalyst 28.
- the sensor that is the object of the abnormality diagnosis is the sensor. Limited les. That is, the abnormality diagnosis may be executed in an air-fuel ratio sensor arranged upstream of the catalyst.
- the oxygen sensor 40 corresponds to the “exhaust gas sensor” in the first aspect of the invention, and the ECU 70 force S and the processing of step 104 described above are executed.
- the “determination means” in the first invention is realized by the “determination means” in the first invention executing the processing of step 124 or 126 described above.
- the oxygen sensor 40 corresponds to the “exhaust gas sensor” in the fourth aspect of the invention, and the ECU 70 force S and the processing of step 108 are executed.
- the “accumulated intake air amount acquisition means” in the fourth invention executes the process of step 110, so that the “determination means” in the fourth invention executes the process of step 124 or 126.
- the “abnormal diagnosis means” in the fourth invention is realized.
- the oxygen sensor 40 corresponds to the “exhaust gas sensor” according to the seventh aspect of the invention, and the ECU 70 power is executed by executing the process of step 136 above.
- the “cancellation means” in the present invention implements the processing of step 124 or 126, thereby realizing the “abnormality diagnosis means” in the seventh invention.
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Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US12/226,774 US8214176B2 (en) | 2006-07-03 | 2007-06-26 | Exhaust gas sensor abnormality diagnostic device |
CN2007800251949A CN101484799B (zh) | 2006-07-03 | 2007-06-26 | 排气传感器的异常诊断装置 |
EP07767591.6A EP2037257B1 (en) | 2006-07-03 | 2007-06-26 | Exhaust gas sensor abnormality diagnostic device |
US13/287,460 US8260576B2 (en) | 2006-07-03 | 2011-11-02 | Exhaust gas sensor abnormality diagnostic device |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2006183597A JP4779835B2 (ja) | 2006-07-03 | 2006-07-03 | 排気ガスセンサの異常診断装置 |
JP2006-183597 | 2006-07-03 |
Related Child Applications (2)
Application Number | Title | Priority Date | Filing Date |
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US12/226,774 A-371-Of-International US8214176B2 (en) | 2006-07-03 | 2007-06-26 | Exhaust gas sensor abnormality diagnostic device |
US13/287,460 Division US8260576B2 (en) | 2006-07-03 | 2011-11-02 | Exhaust gas sensor abnormality diagnostic device |
Publications (1)
Publication Number | Publication Date |
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WO2008004462A1 true WO2008004462A1 (fr) | 2008-01-10 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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PCT/JP2007/062785 WO2008004462A1 (fr) | 2006-07-03 | 2007-06-26 | Appareil de diagnostic de panne de détecteur de gaz d'échappement |
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US (2) | US8214176B2 (ja) |
EP (1) | EP2037257B1 (ja) |
JP (1) | JP4779835B2 (ja) |
CN (1) | CN101484799B (ja) |
WO (1) | WO2008004462A1 (ja) |
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US8260576B2 (en) | 2012-09-04 |
EP2037257A1 (en) | 2009-03-18 |
JP4779835B2 (ja) | 2011-09-28 |
EP2037257B1 (en) | 2018-02-28 |
CN101484799A (zh) | 2009-07-15 |
CN101484799B (zh) | 2012-07-04 |
JP2008014670A (ja) | 2008-01-24 |
US20120046910A1 (en) | 2012-02-23 |
US8214176B2 (en) | 2012-07-03 |
EP2037257A4 (en) | 2013-11-13 |
US20090089011A1 (en) | 2009-04-02 |
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