WO2007045574A1 - Verteilervorrichtung für ein gas-flüssigphasengemisch für apparate - Google Patents

Verteilervorrichtung für ein gas-flüssigphasengemisch für apparate Download PDF

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Publication number
WO2007045574A1
WO2007045574A1 PCT/EP2006/067196 EP2006067196W WO2007045574A1 WO 2007045574 A1 WO2007045574 A1 WO 2007045574A1 EP 2006067196 W EP2006067196 W EP 2006067196W WO 2007045574 A1 WO2007045574 A1 WO 2007045574A1
Authority
WO
WIPO (PCT)
Prior art keywords
distributor
gas
distributor plate
liquid phase
plate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2006/067196
Other languages
German (de)
English (en)
French (fr)
Inventor
Wolfgang Gerlinger
Torsten Mattke
Oliver Bey
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to DE502006004540T priority Critical patent/DE502006004540D1/de
Priority to CN200680038659XA priority patent/CN101291724B/zh
Priority to EP06807084A priority patent/EP1940541B1/de
Priority to JP2008536015A priority patent/JP5027147B2/ja
Priority to AT06807084T priority patent/ATE439183T1/de
Priority to US12/090,198 priority patent/US8597586B2/en
Publication of WO2007045574A1 publication Critical patent/WO2007045574A1/de
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0278—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/002—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B01J8/0085—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction promoting uninterrupted fluid flow, e.g. by filtering out particles in front of the catalyst layer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/065—Feeding reactive fluids
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00823—Mixing elements
    • B01J2208/00831—Stationary elements
    • B01J2208/00849—Stationary elements outside the bed, e.g. baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00884—Means for supporting the bed of particles, e.g. grids, bars, perforated plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/192—Details relating to the geometry of the reactor polygonal
    • B01J2219/1928—Details relating to the geometry of the reactor polygonal hexagonal

Definitions

  • the distance between the distributor plate and possible installations of the apparatus is selected such that a cross-flow of the liquid phase above the distributor plate with a low flow velocity is possible, and is accordingly dependent on the substance system and the prevailing volumetric flow. In particular, this distance ensures that the distribution between liquid and gas phase is uniform over the cross-section of the apparatus.
  • the number and arrangement of the through openings in the active surface of the distributor plate depend on the design of the apparatus. If the apparatus comprises devices such as catalyst particles of a fixed bed arranged on a holding rack or contact tubes welded with catalyst particles in a tube plate, the distributor devices according to the invention ensure that the cross section of the apparatus is uniformly exposed to the two-phase mixture.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Dispersion Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Cyclones (AREA)
  • Sawing (AREA)
  • Valve Device For Special Equipments (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
PCT/EP2006/067196 2005-10-20 2006-10-09 Verteilervorrichtung für ein gas-flüssigphasengemisch für apparate Ceased WO2007045574A1 (de)

Priority Applications (6)

Application Number Priority Date Filing Date Title
DE502006004540T DE502006004540D1 (de) 2005-10-20 2006-10-09 Sch für apparate
CN200680038659XA CN101291724B (zh) 2005-10-20 2006-10-09 壳管式反应器
EP06807084A EP1940541B1 (de) 2005-10-20 2006-10-09 Verteilervorrichtung für ein gas-flüssigphasengemisch für apparate
JP2008536015A JP5027147B2 (ja) 2005-10-20 2006-10-09 機器に用いられる気液相混合物のための分配装置
AT06807084T ATE439183T1 (de) 2005-10-20 2006-10-09 Verteilervorrichtung für ein gas- flüssigphasengemisch für apparate
US12/090,198 US8597586B2 (en) 2005-10-20 2006-10-09 Shell-and-tube reactor having a distribution device for a gas-liquid phase mixture

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102005050284.9 2005-10-20
DE102005050284A DE102005050284A1 (de) 2005-10-20 2005-10-20 Verteilervorrichtung für ein Gas-Flüssigphasengemisch für Apparate

Publications (1)

Publication Number Publication Date
WO2007045574A1 true WO2007045574A1 (de) 2007-04-26

Family

ID=37529462

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2006/067196 Ceased WO2007045574A1 (de) 2005-10-20 2006-10-09 Verteilervorrichtung für ein gas-flüssigphasengemisch für apparate

Country Status (7)

Country Link
US (1) US8597586B2 (https=)
EP (1) EP1940541B1 (https=)
JP (1) JP5027147B2 (https=)
CN (1) CN101291724B (https=)
AT (1) ATE439183T1 (https=)
DE (2) DE102005050284A1 (https=)
WO (1) WO2007045574A1 (https=)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2008087086A1 (de) * 2007-01-16 2008-07-24 Basf Se Reaktor und verfahren zur herstellung von schwefelwasserstoff
WO2009021736A1 (en) * 2007-08-14 2009-02-19 Saipem S.P.A. Modified tubular reactor and process for effecting catalytic reactions involving thermal exchanges in which it is used
JP2010530296A (ja) * 2007-06-12 2010-09-09 イエフペ 粒状層を含む封入体、及び同封入体内の上昇流として流通する気相及び液相の分配
WO2010083978A3 (de) * 2009-01-21 2011-01-06 Basf Se Rohrbündelreaktor für unkatalysierte oder homogenkatalysierte reaktionen
WO2011080196A1 (en) * 2009-12-28 2011-07-07 Shell Internationale Research Maatschappij B.V. Reactor with gas distribution system in bottom
DE102010053289A1 (de) 2010-12-02 2012-06-06 Linde Ag Vorrichtung zur Durchführung von Gas-Flüssigkeit-Reaktion
RU2500451C2 (ru) * 2008-07-15 2013-12-10 Ифп Реактор для очистки или гидроочистки жидкой нагрузки, например для каталитической очистки дистиллятов сырой тяжелой нефти

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2011512241A (ja) * 2008-01-25 2011-04-21 ビーエーエスエフ ソシエタス・ヨーロピア 高圧反応を行なうための反応装置、反応を開始する方法、および反応を実施する方法
CN103100352B (zh) * 2011-11-10 2015-04-01 中国石油化工股份有限公司 一种上流式反应器气液分布器及应用
EP3476470B1 (en) 2017-10-26 2022-11-09 ALFA LAVAL OLMI S.p.A. Shell-and-tube equipment with distribution device
WO2020050738A1 (en) * 2018-09-06 2020-03-12 Public Joint Stock Company "Sibur Holding" Bubble shell-and-tube apparatus
JP2020185511A (ja) * 2019-05-10 2020-11-19 日揮株式会社 反応装置
CN116196851A (zh) * 2023-03-17 2023-06-02 湖南长科诚享石化科技有限公司 连续逆流接触反应方法及装置

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4233269A (en) * 1978-11-09 1980-11-11 Exxon Research & Engineering Co. Gas liquid distributor
GB2148141A (en) * 1983-10-14 1985-05-30 Hydrocarbon Research Inc Staged flow distribution grid assembly for ebullated bed reactor
US5043145A (en) * 1986-08-21 1991-08-27 Exxon Research & Engineering Company Minimal holdup reactor grid
WO1999039815A1 (en) * 1998-02-06 1999-08-12 Foster Wheeler Usa Corporation Predominantly liquid filled vapor-liquid chemical reactor
WO1999046037A1 (en) * 1998-03-12 1999-09-16 Dsm N.V. Apparatus for effecting gas/liquid contact
WO1999050235A1 (en) * 1998-04-01 1999-10-07 Siirtec-Nigi S.P.A. Apparatus and process for the preparation of urea from carbon dioxide and ammonia
US6123323A (en) * 1996-08-26 2000-09-26 Nippon Shokubai Co., Ltd. Gas-liquid dispersion devices provided with partitioning members, gas-liquid contact apparatus, and wastewater treatment systems provided with the same
US6175040B1 (en) * 1994-05-11 2001-01-16 Urea Casale Sa Reactor for two-phase reactions, in particular for urea synthesis at high pressure and temperature

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5148459B2 (https=) * 1973-04-19 1976-12-21
JPS5363131A (en) * 1977-07-04 1978-06-06 Toshiba Corp Identification card
FR2633196B2 (fr) * 1987-11-30 1991-05-31 Inst Francais Du Petrole Appareil pour injecter une charge d'hydrocarbures dans un reacteur
JPH0642939B2 (ja) * 1990-10-30 1994-06-08 日揮株式会社 並流型気液接触装置および気液反応装置
JP3739903B2 (ja) * 1996-08-27 2006-01-25 株式会社日本触媒 気液分散装置及び気液接触装置並びに廃水処理装置
US6013834A (en) 1999-03-04 2000-01-11 Celanese International Corporation Production of vinyl acetate in a catalytic reactor equipped with filter and distribution bed
EP1201298A1 (en) * 2000-10-24 2002-05-02 Urea Casale S.A. Carbamate condensation unit

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4233269A (en) * 1978-11-09 1980-11-11 Exxon Research & Engineering Co. Gas liquid distributor
GB2148141A (en) * 1983-10-14 1985-05-30 Hydrocarbon Research Inc Staged flow distribution grid assembly for ebullated bed reactor
US5043145A (en) * 1986-08-21 1991-08-27 Exxon Research & Engineering Company Minimal holdup reactor grid
US6175040B1 (en) * 1994-05-11 2001-01-16 Urea Casale Sa Reactor for two-phase reactions, in particular for urea synthesis at high pressure and temperature
US6123323A (en) * 1996-08-26 2000-09-26 Nippon Shokubai Co., Ltd. Gas-liquid dispersion devices provided with partitioning members, gas-liquid contact apparatus, and wastewater treatment systems provided with the same
WO1999039815A1 (en) * 1998-02-06 1999-08-12 Foster Wheeler Usa Corporation Predominantly liquid filled vapor-liquid chemical reactor
WO1999046037A1 (en) * 1998-03-12 1999-09-16 Dsm N.V. Apparatus for effecting gas/liquid contact
WO1999050235A1 (en) * 1998-04-01 1999-10-07 Siirtec-Nigi S.P.A. Apparatus and process for the preparation of urea from carbon dioxide and ammonia

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7871594B2 (en) 2007-01-16 2011-01-18 Basf Se Reactor and method for production of hydrogen sulphide
US8580208B2 (en) 2007-01-16 2013-11-12 Basf Se Reactor and method for production of hydrogen sulphide
WO2008087086A1 (de) * 2007-01-16 2008-07-24 Basf Se Reaktor und verfahren zur herstellung von schwefelwasserstoff
KR101574356B1 (ko) * 2007-06-12 2015-12-03 아이에프피 에너지 누벨르 입상 베드를 포함하는 엔클로져 및 이 엔클로져에서 상승류로 순환하는 기상 및 액상 분배 방법
JP2010530296A (ja) * 2007-06-12 2010-09-09 イエフペ 粒状層を含む封入体、及び同封入体内の上昇流として流通する気相及び液相の分配
WO2009021736A1 (en) * 2007-08-14 2009-02-19 Saipem S.P.A. Modified tubular reactor and process for effecting catalytic reactions involving thermal exchanges in which it is used
EP3566768A1 (en) * 2007-08-14 2019-11-13 SAIPEM S.p.A. Modified tubular reactor and process for effecting catalytic reactions involving thermal exchanges in which it is used
US9233352B2 (en) 2007-08-14 2016-01-12 Saipem S.P.A. Modified tubular reactor and process for effecting catalytic reactions involving thermal exchanges in which it is used
RU2500451C2 (ru) * 2008-07-15 2013-12-10 Ифп Реактор для очистки или гидроочистки жидкой нагрузки, например для каталитической очистки дистиллятов сырой тяжелой нефти
WO2010083978A3 (de) * 2009-01-21 2011-01-06 Basf Se Rohrbündelreaktor für unkatalysierte oder homogenkatalysierte reaktionen
US9174192B2 (en) 2009-01-21 2015-11-03 Basf Se Tube bundle reactor for uncatalyzed or homogeneously catalyzed reactions
US9149781B2 (en) 2009-12-28 2015-10-06 Shell Oil Company Reactor with gas distribution system in bottom
US9738835B2 (en) 2009-12-28 2017-08-22 Shell Oil Company Process for performing a fischer tropsch reaction
WO2011080196A1 (en) * 2009-12-28 2011-07-07 Shell Internationale Research Maatschappij B.V. Reactor with gas distribution system in bottom
DE102010053289A1 (de) 2010-12-02 2012-06-06 Linde Ag Vorrichtung zur Durchführung von Gas-Flüssigkeit-Reaktion

Also Published As

Publication number Publication date
US20090220391A1 (en) 2009-09-03
CN101291724A (zh) 2008-10-22
JP5027147B2 (ja) 2012-09-19
EP1940541A1 (de) 2008-07-09
DE102005050284A1 (de) 2007-05-10
EP1940541B1 (de) 2009-08-12
CN101291724B (zh) 2010-11-03
ATE439183T1 (de) 2009-08-15
DE502006004540D1 (de) 2009-09-24
JP2009512546A (ja) 2009-03-26
US8597586B2 (en) 2013-12-03

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