WO2005120702A1 - Procédé pour produire une masse d'oxyde multimétallique - Google Patents

Procédé pour produire une masse d'oxyde multimétallique Download PDF

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Publication number
WO2005120702A1
WO2005120702A1 PCT/EP2005/005962 EP2005005962W WO2005120702A1 WO 2005120702 A1 WO2005120702 A1 WO 2005120702A1 EP 2005005962 W EP2005005962 W EP 2005005962W WO 2005120702 A1 WO2005120702 A1 WO 2005120702A1
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WO
WIPO (PCT)
Prior art keywords
multimetal oxide
mixture
sources
group
elemental
Prior art date
Application number
PCT/EP2005/005962
Other languages
German (de)
English (en)
Inventor
Hartmut Hibst
Frieder Borgmeier
Frank Rosowski
Klaus Joachim MÜLLER-ENGEL
Original Assignee
Basf Aktiengesellschaft
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE102004027999A external-priority patent/DE102004027999A1/de
Application filed by Basf Aktiengesellschaft filed Critical Basf Aktiengesellschaft
Priority to EP05745626A priority Critical patent/EP1755779A1/fr
Priority to JP2007526256A priority patent/JP5517407B2/ja
Publication of WO2005120702A1 publication Critical patent/WO2005120702A1/fr

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24—Chromium, molybdenum or tungsten
    • B01J23/28—Molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24—Chromium, molybdenum or tungsten
    • B01J23/31—Chromium, molybdenum or tungsten combined with bismuth
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56—Platinum group metals
    • B01J23/64—Platinum group metals with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/652—Chromium, molybdenum or tungsten
    • B01J23/6525—Molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/887—Molybdenum containing in addition other metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/8877—Vanadium, tantalum, niobium or polonium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
    • B01J27/057—Selenium or tellurium; Compounds thereof
    • B01J27/0576—Tellurium; Compounds thereof
    • B01J35/30—
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0221—Coating of particles
    • B01J37/0223—Coating of particles by rotation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/36—Methods for preparing oxides or hydroxides in general by precipitation reactions in aqueous solutions
    • C01B13/366—Methods for preparing oxides or hydroxides in general by precipitation reactions in aqueous solutions by hydrothermal processing
    • C—CHEMISTRY; METALLURGY
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    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B19/00—Selenium; Tellurium; Compounds thereof
    • C01B19/002—Compounds containing, besides selenium or tellurium, more than one other element, with -O- and -OH not being considered as anions
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    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B19/00—Selenium; Tellurium; Compounds thereof
    • C01B19/008—Salts of oxyacids of selenium or tellurium
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    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G39/00—Compounds of molybdenum
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G39/00—Compounds of molybdenum
    • C01G39/006—Compounds containing, besides molybdenum, two or more other elements, with the exception of oxygen or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/006—Compounds containing, besides manganese, two or more other elements, with the exception of oxygen or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G47/00—Compounds of rhenium
    • C01G47/006—Compounds containing, besides rhenium, two or more other elements, with the exception of oxygen or hydrogen
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    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00—Compounds of iron
    • C01G49/009—Compounds containing, besides iron, two or more other elements, with the exception of oxygen or hydrogen
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    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G51/00—Compounds of cobalt
    • C01G51/006—Compounds containing, besides cobalt, two or more other elements, with the exception of oxygen or hydrogen
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    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/006—Compounds containing, besides nickel, two or more other elements, with the exception of oxygen or hydrogen
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    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G55/00—Compounds of ruthenium, rhodium, palladium, osmium, iridium, or platinum
    • C01G55/002—Compounds containing, besides ruthenium, rhodium, palladium, osmium, iridium, or platinum, two or more other elements, with the exception of oxygen or hydrogen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
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    • C01P2004/10—Particle morphology extending in one dimension, e.g. needle-like
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    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area

Abstract

L'invention concerne un procédé pour la production hydrothermique de masses d'oxydes multimétalliques contenant du Mo et du V. Selon ce procédé, on utilise, comme sources de constituants élémentaires des masses d'oxydes multimétalliques, pratiquement exclusivement des sources sélectionnées dans le groupe comprenant les oxydes, les hydrates d'oxydes, les oxyacides et les hydroxydes. Une partie des sources contient des constituants élémentaires présentant un nombre d'oxydation inférieur au nombre d'oxydation maximal de chacun de ces derniers.
PCT/EP2005/005962 2004-06-09 2005-06-03 Procédé pour produire une masse d'oxyde multimétallique WO2005120702A1 (fr)

Priority Applications (2)

Application Number Priority Date Filing Date Title
EP05745626A EP1755779A1 (fr) 2004-06-09 2005-06-03 Procédé pour produire une masse d'oxyde multimétallique
JP2007526256A JP5517407B2 (ja) 2004-06-09 2005-06-03 多金属酸化物材料の製造方法

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US57792904P 2004-06-09 2004-06-09
US60/577,929 2004-06-09
DE102004027999.3 2004-06-09
DE102004027999A DE102004027999A1 (de) 2004-06-09 2004-06-09 Verfahren zur Herstellung einer Multimetalloxidmasse

Publications (1)

Publication Number Publication Date
WO2005120702A1 true WO2005120702A1 (fr) 2005-12-22

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PCT/EP2005/005962 WO2005120702A1 (fr) 2004-06-09 2005-06-03 Procédé pour produire une masse d'oxyde multimétallique

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EP (1) EP1755779A1 (fr)
JP (1) JP5517407B2 (fr)
WO (1) WO2005120702A1 (fr)

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2179790A1 (fr) 2008-10-21 2010-04-28 Sued-Chemie AG Catalyseurs d'oxyde mixtes contenant du bismuth
EP2179793A1 (fr) 2008-10-21 2010-04-28 Sued-Chemie AG Catalyseurs d'oxyde mixtes contenant du phosphore
CN101862661A (zh) * 2010-06-04 2010-10-20 浙江大学 一种制备v,s共掺的二氧化钛光催化剂的方法
DE102012207811A1 (de) 2012-05-10 2012-07-12 Basf Se Verfahren der heterogen katalysierten Gasphasenpartialoxidation von (Meth)acrolein zu (Meth)acrylsäure
DE102013202048A1 (de) 2013-02-07 2013-04-18 Basf Se Verfahren zur Herstellung einer katalytisch aktiven Masse, die ein Gemisch aus einem die Elemente Mo und V enthaltenden Multielementoxid und wenigstens einem Oxid des Molybdäns ist
DE102017000862A1 (de) 2017-01-31 2018-08-02 Clariant Produkte (Deutschland) Gmbh Synthese eines MoVNbTe-Katalysators mit reduziertem Gehalt an Niob und Tellur und höherer Aktivität für die oxidative Dehydrierung von Ethan
DE102017000865A1 (de) 2017-01-31 2018-08-02 Clariant Produkte (Deutschland) Gmbh Synthese eines MoVNbTe-Katalysators mit erhöhter spezifischer Oberfläche und höherer Aktivität für die oxidative Dehyxdrierung von Ethan zu Ethylen
CN111132764A (zh) * 2017-09-19 2020-05-08 科莱恩国际有限公司 用于将乙烷氧化脱氢成乙烯的MoVNbTe壳催化剂的合成
WO2020223048A1 (fr) 2019-05-02 2020-11-05 Dow Global Technologies Llc Processus de réduction de sous-produits d'aldéhyde dans la production d'acide acrylique à l'aide de catalyseurs hautement actifs et sélectifs
WO2021213823A1 (fr) 2020-04-21 2021-10-28 Basf Se Procédé de production d'un oxyde multi-élément catalytiquement actif contenant les éléments mo, w, v et cu
WO2022090019A1 (fr) 2020-10-29 2022-05-05 Basf Se Procédé de production d'un catalyseur à noyau-enveloppe
WO2023028434A1 (fr) * 2021-08-23 2023-03-02 Dow Global Technologies Llc Catalyseur et procédé de déshydrogénation d'alcanes en oléfines

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JP4727506B2 (ja) * 2006-06-07 2011-07-20 旭化成ケミカルズ株式会社 ブロンズ構造を有する酸化物の製造方法
US9409156B2 (en) * 2012-10-19 2016-08-09 Instituto Mexicano Del Petroleo Oxidative dehydrogenation of ethane to ethylene and preparation of multimetallic mixed oxide catalyst for such process
EP3219386A1 (fr) * 2016-03-14 2017-09-20 Evonik Degussa GmbH Procédé de fabrication hydrothermal de catalyseurs d'oxydes mixtes à base de molybdène, bismuth, cobalt et fer
CA2936448C (fr) * 2016-07-19 2024-02-20 Nova Chemicals Corporation Traitement hydrothermal a pression controlee de catalyseur odh
JP7375638B2 (ja) * 2020-03-18 2023-11-08 三菱ケミカル株式会社 不飽和カルボン酸合成用触媒の製造方法
JP7375639B2 (ja) * 2020-03-18 2023-11-08 三菱ケミカル株式会社 不飽和カルボン酸合成用触媒の製造方法

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Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2179793A1 (fr) 2008-10-21 2010-04-28 Sued-Chemie AG Catalyseurs d'oxyde mixtes contenant du phosphore
EP2179790A1 (fr) 2008-10-21 2010-04-28 Sued-Chemie AG Catalyseurs d'oxyde mixtes contenant du bismuth
CN101862661A (zh) * 2010-06-04 2010-10-20 浙江大学 一种制备v,s共掺的二氧化钛光催化剂的方法
US9181169B2 (en) 2012-05-10 2015-11-10 Basf Se Process for heterogeneously catalyzed gas phase partial oxidation of (meth)acrolein to (meth)acrylic acid
DE102012207811A1 (de) 2012-05-10 2012-07-12 Basf Se Verfahren der heterogen katalysierten Gasphasenpartialoxidation von (Meth)acrolein zu (Meth)acrylsäure
WO2013167405A1 (fr) 2012-05-10 2013-11-14 Basf Se Procédé d'oxydation partielle en phase gazeuse à catalyse hétérogène de (méth)acroléine pour obtenir de l'acide (méth)acrylique
DE102013202048A1 (de) 2013-02-07 2013-04-18 Basf Se Verfahren zur Herstellung einer katalytisch aktiven Masse, die ein Gemisch aus einem die Elemente Mo und V enthaltenden Multielementoxid und wenigstens einem Oxid des Molybdäns ist
US9061988B2 (en) 2013-02-07 2015-06-23 Basf Se Process for producing a catalytically active composition being a mixture of a multielement oxide comprising the elements Mo and V and at least one oxide of molybdenum
WO2014122043A1 (fr) 2013-02-07 2014-08-14 Basf Se Procédé de fabrication d'une masse à activité catalytique qui constitue un mélange entre un oxyde de plusieurs éléments, lequel contient les éléments mo et v, et au moins un oxyde du molybdène
DE102017000862A1 (de) 2017-01-31 2018-08-02 Clariant Produkte (Deutschland) Gmbh Synthese eines MoVNbTe-Katalysators mit reduziertem Gehalt an Niob und Tellur und höherer Aktivität für die oxidative Dehydrierung von Ethan
DE102017000865A1 (de) 2017-01-31 2018-08-02 Clariant Produkte (Deutschland) Gmbh Synthese eines MoVNbTe-Katalysators mit erhöhter spezifischer Oberfläche und höherer Aktivität für die oxidative Dehyxdrierung von Ethan zu Ethylen
WO2018141652A1 (fr) 2017-01-31 2018-08-09 Clariant Produkte (Deutschland) Gmbh Synthèse d'un catalyseur movnbte ayant une teneur réduite en niobium et en tellure ainsi qu'une activité plus importante pour la déshydrogénation oxydative de l'éthane
WO2018141653A1 (fr) 2017-01-31 2018-08-09 Clariant Produkte (Deutschland) Gmbh Synthèse d'un catalyseur movnbte présentant une surface spécifique plus importante et une activité accrue pour la déshydrogénation oxydante d'éthane en éthylène
US11097254B2 (en) 2017-01-31 2021-08-24 Clariant Produkte (Deutschland) Gmbh Synthesis of a MoVNbTe catalyst having a reduced niobium and tellurium content and higher activity for the oxidative dehydrogenation of ethane
CN111132764A (zh) * 2017-09-19 2020-05-08 科莱恩国际有限公司 用于将乙烷氧化脱氢成乙烯的MoVNbTe壳催化剂的合成
WO2020223048A1 (fr) 2019-05-02 2020-11-05 Dow Global Technologies Llc Processus de réduction de sous-produits d'aldéhyde dans la production d'acide acrylique à l'aide de catalyseurs hautement actifs et sélectifs
WO2021213823A1 (fr) 2020-04-21 2021-10-28 Basf Se Procédé de production d'un oxyde multi-élément catalytiquement actif contenant les éléments mo, w, v et cu
WO2022090019A1 (fr) 2020-10-29 2022-05-05 Basf Se Procédé de production d'un catalyseur à noyau-enveloppe
WO2023028434A1 (fr) * 2021-08-23 2023-03-02 Dow Global Technologies Llc Catalyseur et procédé de déshydrogénation d'alcanes en oléfines

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