WO2003010383A1 - Sizing agent for carbon fiber, aqueous dispersion of the same, carbon fiber treated by sizing, sheet comprising the carbon fiber, and carbon fiber-reinforced composite material - Google Patents

Sizing agent for carbon fiber, aqueous dispersion of the same, carbon fiber treated by sizing, sheet comprising the carbon fiber, and carbon fiber-reinforced composite material Download PDF

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Publication number
WO2003010383A1
WO2003010383A1 PCT/JP2002/007481 JP0207481W WO03010383A1 WO 2003010383 A1 WO2003010383 A1 WO 2003010383A1 JP 0207481 W JP0207481 W JP 0207481W WO 03010383 A1 WO03010383 A1 WO 03010383A1
Authority
WO
WIPO (PCT)
Prior art keywords
carbon fiber
sizing
ingredient
sheet
composite material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2002/007481
Other languages
English (en)
French (fr)
Inventor
Naoki Sugiura
Masashi Taguchi
Tadayoshi Saitou
Tomonori Okuda
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Chemical Corp
Original Assignee
Mitsubishi Rayon Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Rayon Co Ltd filed Critical Mitsubishi Rayon Co Ltd
Priority to DE60238618T priority Critical patent/DE60238618D1/de
Priority to KR1020047001036A priority patent/KR100549759B1/ko
Priority to JP2003515720A priority patent/JP4101750B2/ja
Priority to EP20020755634 priority patent/EP1413670B1/en
Priority to US10/484,493 priority patent/US7150913B2/en
Priority to AT02755634T priority patent/ATE491837T1/de
Publication of WO2003010383A1 publication Critical patent/WO2003010383A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/11—Compounds containing epoxy groups or precursors thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/04—Reinforcing macromolecular compounds with loose or coherent fibrous material
    • C08J5/06—Reinforcing macromolecular compounds with loose or coherent fibrous material using pretreated fibrous materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/24—Impregnating materials with prepolymers which can be polymerised in situ, e.g. manufacture of prepregs
    • C08J5/248—Impregnating materials with prepolymers which can be polymerised in situ, e.g. manufacture of prepregs using pre-treated fibres
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/55—Epoxy resins
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M7/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made of other substances with subsequent freeing of the treated goods from the treating medium, e.g. swelling, e.g. polyolefins
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/40—Fibres of carbon
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913—Rod, strand, filament or fiber
    • Y10T428/2933—Coated or with bond, impregnation or core
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/30—Self-sustaining carbon mass or layer with impregnant or other layer
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31511—Of epoxy ether

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Textile Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Reinforced Plastic Materials (AREA)
  • Casting Or Compression Moulding Of Plastics Or The Like (AREA)
PCT/JP2002/007481 2001-07-24 2002-07-24 Sizing agent for carbon fiber, aqueous dispersion of the same, carbon fiber treated by sizing, sheet comprising the carbon fiber, and carbon fiber-reinforced composite material Ceased WO2003010383A1 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
DE60238618T DE60238618D1 (de) 2001-07-24 2002-07-24 On davon, geschlichtete carbonfaser, die carbonfaser enthaltendes band sowie mit carbonfaser verstärkter verbundstoff
KR1020047001036A KR100549759B1 (ko) 2001-07-24 2002-07-24 탄소섬유용 사이즈제, 그 수분산액, 사이징 처리된탄소섬유, 그 탄소섬유를 사용한 시트상물, 및탄소섬유강화 복합재료
JP2003515720A JP4101750B2 (ja) 2001-07-24 2002-07-24 炭素繊維用サイズ剤、その水分散液、サイジング処理された炭素繊維、該炭素繊維を使用したシート状物、及び炭素繊維強化複合材料
EP20020755634 EP1413670B1 (en) 2001-07-24 2002-07-24 Sizing agent for carbon fiber, aqueous dispersion of the same, carbon fiber treated by sizing, sheet comprising the carbon fiber, and carbon fiber-reinforced composite material
US10/484,493 US7150913B2 (en) 2001-07-24 2002-07-24 Sizing agent for carbon fiber, aqueous dispersion of the same, carbon fiber treated by sizing, sheet comprising the carbon fiber, and carbon fiber-reinforced composite material
AT02755634T ATE491837T1 (de) 2001-07-24 2002-07-24 Schlichtemittel für carbonfaser, wässrige dispersion davon, geschlichtete carbonfaser, die carbonfaser enthaltendes band sowie mit carbonfaser verstärkter verbundstoff

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2001222848 2001-07-24
JP2001-222848 2001-07-24

Publications (1)

Publication Number Publication Date
WO2003010383A1 true WO2003010383A1 (en) 2003-02-06

Family

ID=19056268

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2002/007481 Ceased WO2003010383A1 (en) 2001-07-24 2002-07-24 Sizing agent for carbon fiber, aqueous dispersion of the same, carbon fiber treated by sizing, sheet comprising the carbon fiber, and carbon fiber-reinforced composite material

Country Status (10)

Country Link
US (1) US7150913B2 (ja)
EP (1) EP1413670B1 (ja)
JP (1) JP4101750B2 (ja)
KR (1) KR100549759B1 (ja)
CN (1) CN1249292C (ja)
AT (1) ATE491837T1 (ja)
DE (1) DE60238618D1 (ja)
ES (1) ES2355331T3 (ja)
TW (1) TWI220147B (ja)
WO (1) WO2003010383A1 (ja)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008280624A (ja) * 2007-05-08 2008-11-20 Mitsubishi Rayon Co Ltd 炭素繊維用サイズ剤、その水分散液、炭素繊維、及び炭素繊維強化複合材料
JP2008280623A (ja) * 2007-05-08 2008-11-20 Mitsubishi Rayon Co Ltd 炭素繊維用サイズ剤、その水分散液、炭素繊維、及び炭素繊維強化複合材料
WO2013099707A1 (ja) 2011-12-27 2013-07-04 東レ株式会社 サイジング剤塗布炭素繊維、サイジング剤塗布炭素繊維の製造方法、プリプレグおよび炭素繊維強化複合材料
WO2014017340A1 (ja) 2012-07-25 2014-01-30 東レ株式会社 プリプレグおよび炭素繊維強化複合材料
WO2014017339A1 (ja) 2012-07-25 2014-01-30 東レ株式会社 プリプレグおよび炭素繊維強化複合材料
WO2014050264A1 (ja) 2012-09-28 2014-04-03 東レ株式会社 プリプレグおよび炭素繊維強化複合材料
WO2014061336A1 (ja) 2012-10-18 2014-04-24 東レ株式会社 炭素繊維強化樹脂組成物、炭素繊維強化樹脂組成物の製造方法、成形材料、成形材料の製造方法および炭素繊維強化樹脂成形品
WO2018079763A1 (ja) 2016-10-28 2018-05-03 三菱ケミカル株式会社 炭素繊維用サイジング剤、炭素繊維用サイジング剤の水分散液、及びサイジング剤付着炭素繊維束
JP2019065441A (ja) * 2017-10-03 2019-04-25 東レ株式会社 サイジング剤塗布炭素繊維、およびサイジング剤塗布炭素繊維の製造方法、ならびに炭素繊維強化樹脂組成物

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CN101313106A (zh) * 2005-11-25 2008-11-26 东丽株式会社 碳纤维束、预成型料及碳纤维强化复合材料
AU2007245909B2 (en) * 2006-04-28 2012-02-16 Toho Tenax Europe Gmbh Carbon fiber
KR20110074751A (ko) * 2008-10-10 2011-07-01 호도가야 케미칼 컴파니 리미티드 미세탄소섬유 수분산액, 이 수분산액의 제조 방법 및 이를 이용한 물품
CA2753852C (en) * 2009-02-27 2014-05-06 Momentive Specialty Chemicals Inc. Compositions useful for non-cellulose fiber sizing, coating or binding compositions, and composites incorporating same
CN101509864B (zh) * 2009-03-20 2010-12-08 哈尔滨工业大学 一种碳纤维表面能的测量方法
US20110000617A1 (en) 2009-07-02 2011-01-06 E. I. Du Pont De Nemours And Company Process for making a composite
KR20170018479A (ko) 2009-07-02 2017-02-17 이 아이 듀폰 디 네모아 앤드 캄파니 반도체 제조 부품
US9593444B2 (en) * 2010-06-30 2017-03-14 Toray Industries, Inc. Method for producing sizing agent-coated carbon fibers, and sizing agent-coated carbon fibers
KR101696484B1 (ko) * 2010-12-31 2017-01-16 주식회사 효성 탄소섬유용 사이징제, 그 수분산액, 이로 사이징 처리된 탄소섬유 및 그 탄소섬유를 사용한 시트상물
IN2014CN03279A (ja) * 2011-10-04 2015-07-03 Toray Industries
RU2648086C2 (ru) * 2012-09-25 2018-03-22 Мицубиси Гэс Кемикал Компани, Инк. Армированный волокном полиамидный полимерный материал
US9435057B2 (en) 2013-01-25 2016-09-06 Toray Industries, Inc. Sizing agent-coated carbon fiber bundle, carbon fiber bundle production method, and prepreg
CN103788632B (zh) * 2013-12-17 2016-04-06 浙江普利特新材料有限公司 一种高刚性、高耐久性的碳纤维增强聚酰胺复合材料及其制备方法
KR101699013B1 (ko) 2016-05-12 2017-01-23 제갈제영 매출 보상금 지급 방법 및 이를 실행하는 서버
US10106661B2 (en) * 2016-06-22 2018-10-23 Hexcel Corporation Composite material with thermoplastic toughened novolac-based epoxy resin matrix
CN112292488B (zh) * 2018-06-29 2023-12-29 三菱化学株式会社 上浆剂、增强纤维束、纤维增强树脂成型材料及纤维增强复合材料
KR102358401B1 (ko) 2020-04-02 2022-02-03 도레이첨단소재 주식회사 탄소섬유 코팅제 및 이를 이용한 탄소섬유 강화 복합재료
TWI797655B (zh) * 2021-06-28 2023-04-01 臺灣塑膠工業股份有限公司 上漿劑組成物、碳纖維材料與複合材料
US20230087214A1 (en) * 2021-09-22 2023-03-23 Hao-Chia WU Method for splitting carbon fiber tow

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GB2109794A (en) * 1981-09-07 1983-06-08 Toho Beslon Co Emulsion type sizing agent for carbon fibers, process for its preparation and method for using same
JPH07197381A (ja) * 1993-12-28 1995-08-01 Toho Rayon Co Ltd 炭素繊維ストランド用サイジング剤、サイズ処理された炭素繊維ストランド、及びその炭素繊維ストランドを強化繊維としたプリプレグ
JP2000170050A (ja) * 1998-12-04 2000-06-20 Mitsubishi Chemicals Corp 炭素繊維束の製造方法
JP2001316980A (ja) * 2000-03-03 2001-11-16 Sanyo Chem Ind Ltd 繊維の集束用樹脂組成物

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Cited By (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008280623A (ja) * 2007-05-08 2008-11-20 Mitsubishi Rayon Co Ltd 炭素繊維用サイズ剤、その水分散液、炭素繊維、及び炭素繊維強化複合材料
JP2008280624A (ja) * 2007-05-08 2008-11-20 Mitsubishi Rayon Co Ltd 炭素繊維用サイズ剤、その水分散液、炭素繊維、及び炭素繊維強化複合材料
WO2013099707A1 (ja) 2011-12-27 2013-07-04 東レ株式会社 サイジング剤塗布炭素繊維、サイジング剤塗布炭素繊維の製造方法、プリプレグおよび炭素繊維強化複合材料
US10138593B2 (en) 2011-12-27 2018-11-27 Toray Industries, Inc. Sizing agent-coated carbon fibers, process for producing sizing agent-coated carbon fibers, prepreg, and carbon fiber reinforced composite material
EP3401357A1 (en) 2012-07-25 2018-11-14 Toray Industries, Inc. Prepreg and carbon fiber reinforced composite material
WO2014017340A1 (ja) 2012-07-25 2014-01-30 東レ株式会社 プリプレグおよび炭素繊維強化複合材料
WO2014017339A1 (ja) 2012-07-25 2014-01-30 東レ株式会社 プリプレグおよび炭素繊維強化複合材料
US11286359B2 (en) 2012-07-25 2022-03-29 Toray Industries, Inc. Prepreg and carbon fiber-reinforced composite material
US11111345B2 (en) 2012-07-25 2021-09-07 Toray Industries, Inc. Prepreg and carbon fiber-reinforced composite material
US9683326B2 (en) 2012-07-25 2017-06-20 Toray Industries, Inc. Prepreg and carbon fiber reinforced composite material
US9765194B2 (en) 2012-07-25 2017-09-19 Toray Industries, Inc. Prepreg and carbon fiber-reinforced composite material
WO2014050264A1 (ja) 2012-09-28 2014-04-03 東レ株式会社 プリプレグおよび炭素繊維強化複合材料
US9593238B2 (en) 2012-09-28 2017-03-14 Toray Industries, Inc. Prepreg and carbon fiber reinforced composite material
US10501605B2 (en) 2012-10-18 2019-12-10 Toray Industries, Inc. Carbon fiber-reinforced resin composition, method for manufacturing carbon fiber-reinforced resin composition, molding material, method for manufacturing molding material, and carbon fiber-reinforced resin molded article
KR20150047638A (ko) 2012-10-18 2015-05-04 도레이 카부시키가이샤 탄소 섬유 강화 수지 조성물, 탄소 섬유 강화 수지 조성물의 제조 방법, 성형 재료, 성형 재료의 제조 방법 및 탄소 섬유 강화 수지 성형품
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KR20210062745A (ko) 2016-10-28 2021-05-31 미쯔비시 케미컬 주식회사 탄소섬유용 사이징제, 탄소섬유용 사이징제의 수분산액, 및 사이징제 부착 탄소섬유속
US11787913B2 (en) 2016-10-28 2023-10-17 Mitsubishi Chemical Corporation Sizing agent for carbon fibers, aqueous dispersion of sizing agent for carbon fibers, and sizing agent-adhered carbon fiber bundle
JP2019065441A (ja) * 2017-10-03 2019-04-25 東レ株式会社 サイジング剤塗布炭素繊維、およびサイジング剤塗布炭素繊維の製造方法、ならびに炭素繊維強化樹脂組成物

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US7150913B2 (en) 2006-12-19
EP1413670A1 (en) 2004-04-28
JP4101750B2 (ja) 2008-06-18
CN1249292C (zh) 2006-04-05
JPWO2003010383A1 (ja) 2004-11-18
CN1527895A (zh) 2004-09-08
KR20040021649A (ko) 2004-03-10
EP1413670A4 (en) 2009-09-23
ATE491837T1 (de) 2011-01-15
US20040191511A1 (en) 2004-09-30
ES2355331T3 (es) 2011-03-24
KR100549759B1 (ko) 2006-02-08

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