WO2002072205A3 - Verfahren zur erhöhung des trockenrückstandes bei nass aufgearbeitetem zyklonstaub der chlorierung von titanerz - Google Patents

Verfahren zur erhöhung des trockenrückstandes bei nass aufgearbeitetem zyklonstaub der chlorierung von titanerz Download PDF

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Publication number
WO2002072205A3
WO2002072205A3 PCT/DE2002/000844 DE0200844W WO02072205A3 WO 2002072205 A3 WO2002072205 A3 WO 2002072205A3 DE 0200844 W DE0200844 W DE 0200844W WO 02072205 A3 WO02072205 A3 WO 02072205A3
Authority
WO
WIPO (PCT)
Prior art keywords
chlorination
cyclone dust
dry residue
titanium ore
increasing
Prior art date
Application number
PCT/DE2002/000844
Other languages
English (en)
French (fr)
Other versions
WO2002072205A2 (de
Inventor
Hans-Joerg Bonath
Georg Bombeck
Original Assignee
Kronos Titan Gmbh & Co Ohg
Hans-Joerg Bonath
Georg Bombeck
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kronos Titan Gmbh & Co Ohg, Hans-Joerg Bonath, Georg Bombeck filed Critical Kronos Titan Gmbh & Co Ohg
Priority to US10/467,905 priority Critical patent/US20040136889A1/en
Priority to EP02727201A priority patent/EP1368503A2/de
Priority to JP2002571160A priority patent/JP2004528162A/ja
Priority to CA 2438311 priority patent/CA2438311A1/en
Priority to MXPA03007247A priority patent/MXPA03007247A/es
Publication of WO2002072205A2 publication Critical patent/WO2002072205A2/de
Publication of WO2002072205A3 publication Critical patent/WO2002072205A3/de

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Classifications

    • A—HUMAN NECESSITIES
    • A62—LIFE-SAVING; FIRE-FIGHTING
    • A62D—CHEMICAL MEANS FOR EXTINGUISHING FIRES OR FOR COMBATING OR PROTECTING AGAINST HARMFUL CHEMICAL AGENTS; CHEMICAL MATERIALS FOR USE IN BREATHING APPARATUS
    • A62D3/00—Processes for making harmful chemical substances harmless or less harmful, by effecting a chemical change in the substances
    • A62D3/30—Processes for making harmful chemical substances harmless or less harmful, by effecting a chemical change in the substances by reacting with chemical agents
    • A62D3/33—Processes for making harmful chemical substances harmless or less harmful, by effecting a chemical change in the substances by reacting with chemical agents by chemical fixing the harmful substance, e.g. by chelation or complexation
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/10—Obtaining titanium, zirconium or hafnium
    • C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1218—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes
    • C22B34/1222—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes using a halogen containing agent
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/006—Wet processes
    • C22B7/008—Wet processes by an alkaline or ammoniacal leaching
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
    • C22B7/02—Working-up flue dust
    • A—HUMAN NECESSITIES
    • A62—LIFE-SAVING; FIRE-FIGHTING
    • A62D—CHEMICAL MEANS FOR EXTINGUISHING FIRES OR FOR COMBATING OR PROTECTING AGAINST HARMFUL CHEMICAL AGENTS; CHEMICAL MATERIALS FOR USE IN BREATHING APPARATUS
    • A62D2101/00—Harmful chemical substances made harmless, or less harmful, by effecting chemical change
    • A62D2101/40—Inorganic substances
    • A62D2101/43—Inorganic substances containing heavy metals, in the bonded or free state
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Toxicology (AREA)
  • General Health & Medical Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Business, Economics & Management (AREA)
  • Emergency Management (AREA)
  • Processing Of Solid Wastes (AREA)
  • Treatment Of Sludge (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

Bei der bekannten Aufarbeitung des bei der Chlorierung von Titanerz anfallenden Zyklonstaubes (4) erhält man einen deponiefähigen Filterkuchen (26) mit einem Trockenrückstand von über 40 % (ohne Inertanteile als Stützgerüst), unabhängig davon, ob als Rohstoff Ilmenit, Schlacke oder natürlicher oder künstlicher Rutil, bzw. Mischungen davon eingesetzt werden, wenn einer der oder eine Kombination der folgenden Verfahrensschritte durchgeführt wird: Vor der Anhebung auf einen pH-Wert von 9-12 in einem Neutralisationstank (13) wird eine schnelle Neutralisationsstufe (12) vorgeschaltet, wodurch für alle Volumenelemente der Flüssigkeit die gleichen Fällbedingungen in einem pH-Bereich von 6-9 eingehalten werden können; vor dem Eindicken wird ein (bevorzugt anionisches) erstes Flockungshilfsmittel (22) zugegeben; nach dem Eindicken wird ein (bevorzugt kationisches) Flockungshilfsmittel in den Schlamm eingemischt. Alle Massnahmen verbessern die Flockenbildung und gestalten die Aufarbeitung wirtschaftlicher.
PCT/DE2002/000844 2001-03-13 2002-03-08 Verfahren zur erhöhung des trockenrückstandes bei nass aufgearbeitetem zyklonstaub der chlorierung von titanerz WO2002072205A2 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
US10/467,905 US20040136889A1 (en) 2001-03-13 2002-03-08 Method for increasing the dry residue in processed cyclone dust
EP02727201A EP1368503A2 (de) 2001-03-13 2002-03-08 Verfahren zur erhöhung des trockenrückstandes bei nass aufgearbeitetem zyklonstaub der chlorierung von titanerz
JP2002571160A JP2004528162A (ja) 2001-03-13 2002-03-08 後処理されたサイクロンダストにおける乾燥残留物の増加法
CA 2438311 CA2438311A1 (en) 2001-03-13 2002-03-08 Method for increasing the dry residue in reprocessed cyclone dust
MXPA03007247A MXPA03007247A (es) 2001-03-13 2002-03-08 Procedimiento para aumentar el residuo seco en polvo ciclonico procesado.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE2001111895 DE10111895A1 (de) 2001-03-13 2001-03-13 Verfahren zur Erhöhung des Trockenrückstandes bei aufgearbeitetem Zyklonstaub
DE10111895.3 2001-03-13

Publications (2)

Publication Number Publication Date
WO2002072205A2 WO2002072205A2 (de) 2002-09-19
WO2002072205A3 true WO2002072205A3 (de) 2003-04-17

Family

ID=7677194

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/DE2002/000844 WO2002072205A2 (de) 2001-03-13 2002-03-08 Verfahren zur erhöhung des trockenrückstandes bei nass aufgearbeitetem zyklonstaub der chlorierung von titanerz

Country Status (8)

Country Link
US (1) US20040136889A1 (de)
EP (1) EP1368503A2 (de)
JP (1) JP2004528162A (de)
CA (1) CA2438311A1 (de)
DE (1) DE10111895A1 (de)
MX (1) MXPA03007247A (de)
TW (1) TWI243697B (de)
WO (1) WO2002072205A2 (de)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0405493D0 (en) * 2004-03-12 2004-04-21 Ciba Spec Chem Water Treat Ltd Dewatering process
EA013159B1 (ru) * 2005-04-18 2010-02-26 Ян Просида Способ получения чистых галогенидных солей щелочного и/или щелочно-земельного металла в результате гидролитической обработки галогенидных органических отходов
US7943103B2 (en) * 2006-04-27 2011-05-17 Tronox Llc Waste solids handling
JP4811728B2 (ja) * 2006-11-02 2011-11-09 清水建設株式会社 スラリー脱水処理方法および装置、ならびに懸濁液処理システム
DE102011106864B4 (de) * 2011-06-28 2013-06-20 Kronos International, Inc. Verfahren zur selektiven Abtrennung von Vanadium aus Rückständen der Titandioxidherstellung (Chloridverfahren)
KR101735414B1 (ko) * 2013-01-07 2017-05-29 훈츠만 피앤에이 저머니 게엠베하 티타늄-함유 응집체, 그 제조 방법 및 그 용도
JP7008639B2 (ja) * 2016-05-19 2022-01-25 イルカ・リソーシズ・リミテッド チタン含有材料の細粒の凝集
CN108569797A (zh) * 2017-03-07 2018-09-25 夏燕 一种处理磷矿废水的装置
US20230219817A1 (en) * 2020-06-16 2023-07-13 Yara International Asa Process for the removal of heavy metals from a phosphoric acid containing composition

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3655344A (en) * 1969-09-02 1972-04-11 Ppg Industries Inc Treatment of titanium tetrachloride drier residue
RO81184A2 (ro) * 1980-10-24 1983-02-01 Institutul De Cercetari Si Proiectari Pentru Epurarea Apelor Reziduale,Ro Procedeu de recuperare a zincului din apele reziduale
DE3305802A1 (de) * 1983-02-19 1984-08-23 Philipp Müller, Nachf. Eugen Bucher GmbH & Co., 7000 Stuttgart Abwasseraufbereitungsverfahren
DE3841590A1 (de) * 1987-12-10 1989-06-22 Nippon Kokan Kk Verfahren zur raffination von eisenion-haltiger saurer loesung
EP0390293A1 (de) * 1989-03-30 1990-10-03 Kemira Pigments B.V. Verfahren zur Verarbeitung von metallchloridhaltigen Abfällen
DE4131577A1 (de) * 1991-09-23 1993-03-25 Kronos Int Inc Verfahren zur erzeugung deponiefaehiger produkte aus metallchloriden ohne inerte anteile
DE4132679A1 (de) * 1991-10-01 1993-04-08 Kronos Int Inc Entfernung von schwermetallen aus abwaessern der titandioxidindustrie
DE4321168A1 (de) * 1992-07-22 1994-01-27 Kronos Titan Gmbh Verfahren zur Herstellung einer Titandioxidsuspension mit einem hohen Feststoffgehalt

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Publication number Priority date Publication date Assignee Title
US5238579A (en) * 1990-09-12 1993-08-24 Falconbridge Limited Method for generating coarse precipitates from solutions or slurries containing ionic species
US5976383A (en) * 1991-04-08 1999-11-02 Romar Technologies, Inc. Recycle process for removing dissolved heavy metals from water with aluminum particles
US5393510A (en) * 1992-07-22 1995-02-28 Rheox, Inc. High solids content titanium dioxide suspension
US5370800A (en) * 1993-05-25 1994-12-06 Stevenson; Sanford M. Method for removing metal compounds from waste water
US6800260B2 (en) * 2002-02-11 2004-10-05 Millennium Inorganic Chemicals, Inc. Processes for treating iron-containing waste streams

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3655344A (en) * 1969-09-02 1972-04-11 Ppg Industries Inc Treatment of titanium tetrachloride drier residue
RO81184A2 (ro) * 1980-10-24 1983-02-01 Institutul De Cercetari Si Proiectari Pentru Epurarea Apelor Reziduale,Ro Procedeu de recuperare a zincului din apele reziduale
DE3305802A1 (de) * 1983-02-19 1984-08-23 Philipp Müller, Nachf. Eugen Bucher GmbH & Co., 7000 Stuttgart Abwasseraufbereitungsverfahren
DE3841590A1 (de) * 1987-12-10 1989-06-22 Nippon Kokan Kk Verfahren zur raffination von eisenion-haltiger saurer loesung
EP0390293A1 (de) * 1989-03-30 1990-10-03 Kemira Pigments B.V. Verfahren zur Verarbeitung von metallchloridhaltigen Abfällen
DE4131577A1 (de) * 1991-09-23 1993-03-25 Kronos Int Inc Verfahren zur erzeugung deponiefaehiger produkte aus metallchloriden ohne inerte anteile
DE4132679A1 (de) * 1991-10-01 1993-04-08 Kronos Int Inc Entfernung von schwermetallen aus abwaessern der titandioxidindustrie
DE4321168A1 (de) * 1992-07-22 1994-01-27 Kronos Titan Gmbh Verfahren zur Herstellung einer Titandioxidsuspension mit einem hohen Feststoffgehalt

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
DATABASE WPI Section Ch Week 198335, Derwent World Patents Index; Class A35, AN 1983-751220, XP002223843 *

Also Published As

Publication number Publication date
TWI243697B (en) 2005-11-21
MXPA03007247A (es) 2003-12-04
DE10111895A1 (de) 2002-09-19
CA2438311A1 (en) 2002-09-19
WO2002072205A2 (de) 2002-09-19
EP1368503A2 (de) 2003-12-10
JP2004528162A (ja) 2004-09-16
US20040136889A1 (en) 2004-07-15

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