WO2002030557A3 - Autoklaven-array - Google Patents

Autoklaven-array Download PDF

Info

Publication number
WO2002030557A3
WO2002030557A3 PCT/EP2001/011249 EP0111249W WO0230557A3 WO 2002030557 A3 WO2002030557 A3 WO 2002030557A3 EP 0111249 W EP0111249 W EP 0111249W WO 0230557 A3 WO0230557 A3 WO 0230557A3
Authority
WO
WIPO (PCT)
Prior art keywords
autoclaves
array
gas
autoclave
controllable
Prior art date
Application number
PCT/EP2001/011249
Other languages
English (en)
French (fr)
Other versions
WO2002030557A2 (de
Inventor
Boris E Bosch
Thomas Riermeier
Uwe Dingerdissen
Gerhard Geiss
Norbert Stoll
Martin Krohn
Robert Lemke
Original Assignee
Degussa
Boris E Bosch
Thomas Riermeier
Uwe Dingerdissen
Gerhard Geiss
Norbert Stoll
Martin Krohn
Robert Lemke
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Degussa, Boris E Bosch, Thomas Riermeier, Uwe Dingerdissen, Gerhard Geiss, Norbert Stoll, Martin Krohn, Robert Lemke filed Critical Degussa
Priority to EP01982380A priority Critical patent/EP1339486A2/de
Priority to AU2002213979A priority patent/AU2002213979A1/en
Priority to US10/381,588 priority patent/US20040013565A1/en
Priority to JP2002533993A priority patent/JP2004510575A/ja
Publication of WO2002030557A2 publication Critical patent/WO2002030557A2/de
Publication of WO2002030557A3 publication Critical patent/WO2002030557A3/de

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/04—Pressure vessels, e.g. autoclaves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00279—Features relating to reactor vessels
    • B01J2219/00306—Reactor vessels in a multiple arrangement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00351—Means for dispensing and evacuation of reagents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00351—Means for dispensing and evacuation of reagents
    • B01J2219/00389—Feeding through valves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00477—Means for pressurising the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00479—Means for mixing reactants or products in the reaction vessels
    • B01J2219/00484—Means for mixing reactants or products in the reaction vessels by shaking, vibrating or oscillating of the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277—Apparatus
    • B01J2219/00495—Means for heating or cooling the reaction vessels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00585—Parallel processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00583—Features relative to the processes being carried out
    • B01J2219/00601—High-pressure processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00686—Automatic
    • B01J2219/00689—Automatic using computers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/0068—Means for controlling the apparatus of the process
    • B01J2219/00702—Processes involving means for analysing and characterising the products
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00718—Type of compounds synthesised
    • B01J2219/00745—Inorganic compounds
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B40/00—Libraries per se, e.g. arrays, mixtures
    • C40B40/18—Libraries containing only inorganic compounds or inorganic materials
    • C—CHEMISTRY; METALLURGY
    • C40—COMBINATORIAL TECHNOLOGY
    • C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
    • C40B60/00—Apparatus specially adapted for use in combinatorial chemistry or with libraries
    • C40B60/14—Apparatus specially adapted for use in combinatorial chemistry or with libraries for creating libraries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Die Erfindung betrifft ein skalierbares Autoklaven-Array zur Untersuchung chemischer Reaktionen, das aus Autoklavenmodulen (1-8) besteht, die jeweils aus einem dichtend über einem Reaktionsgefäss (100) befestigten Reaktormantel bestehen und die unabhängig voneinander über steuerbare Autoklavenventile (11-18) aus einer einen Drucksensor (20, 22) enthaltenden Druckregelkammer (21), die über mindestens ein steuerbares (23, 24, 25, 9) Ventil mit mindestens einer Gaszufuhr und mindestens einem Gasauslass verbunden ist, mit Gas befüllt werden können.
PCT/EP2001/011249 2000-10-02 2001-09-28 Autoklaven-array WO2002030557A2 (de)

Priority Applications (4)

Application Number Priority Date Filing Date Title
EP01982380A EP1339486A2 (de) 2000-10-02 2001-09-28 Autoklaven-array
AU2002213979A AU2002213979A1 (en) 2000-10-02 2001-09-28 Array of autoclaves
US10/381,588 US20040013565A1 (en) 2000-10-02 2001-09-28 Array of autoclaves
JP2002533993A JP2004510575A (ja) 2000-10-02 2001-09-28 オートクレーブアレイ

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10049078A DE10049078A1 (de) 2000-10-02 2000-10-02 Autoklaven-Array
DE10049078.6 2000-10-02

Publications (2)

Publication Number Publication Date
WO2002030557A2 WO2002030557A2 (de) 2002-04-18
WO2002030557A3 true WO2002030557A3 (de) 2002-08-08

Family

ID=7658614

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2001/011249 WO2002030557A2 (de) 2000-10-02 2001-09-28 Autoklaven-array

Country Status (6)

Country Link
US (1) US20040013565A1 (de)
EP (1) EP1339486A2 (de)
JP (1) JP2004510575A (de)
AU (1) AU2002213979A1 (de)
DE (1) DE10049078A1 (de)
WO (1) WO2002030557A2 (de)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102004039210C5 (de) * 2004-08-12 2012-11-15 Rudolf Wild Gmbh & Co. Kg Verfahren zur Bewertung der Produkthaltbarkeit in einem Packmittel
US7807109B2 (en) * 2007-05-14 2010-10-05 Freeslate, Inc. Parallel batch reactor with pressure monitoring
WO2008143739A2 (en) * 2007-05-14 2008-11-27 Symyx Technologies, Inc. Parallel batch reactor
US7655191B2 (en) * 2007-05-14 2010-02-02 Symyx Solutions, Inc. Methods for chemical reactions in a parallel batch reactor
US20080286170A1 (en) * 2007-05-14 2008-11-20 Symyx Technologies, Inc. Parallel batch reactor

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB967261A (en) * 1961-03-18 1964-08-19 Bayer Ag Reactor system
CH644828A5 (en) * 1979-11-10 1984-08-31 Deppen Jean Claude Process for the manufacture of permeable prefabricated components and device for making use of this process
US4670404A (en) * 1985-04-22 1987-06-02 Fike Corporation Micro-scale chemical process simulation methods and apparatus useful for design of full scale processes, emergency relief systems and associated equipment
EP0402018A1 (de) * 1989-05-31 1990-12-12 Halliburton Company Druckregelvorrichtung
WO1998036826A1 (en) * 1997-02-20 1998-08-27 Sinvent As Multiautoclave for combinatorial synthesis of zeolites and other materials
WO2000036399A1 (en) * 1998-12-15 2000-06-22 Union Carbide Chemicals & Plastics Technology Corporation Apparatus and methods for combinatorial chemical analysis

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19835914A1 (de) * 1998-08-07 2000-02-17 Basf Ag Verfahren zum Dosieren eines flüssigen, gasförmigen oder in überkritischem Zustand vorliegenden Mediums in einen Druckreaktor
US6306658B1 (en) * 1998-08-13 2001-10-23 Symyx Technologies Parallel reactor with internal sensing

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB967261A (en) * 1961-03-18 1964-08-19 Bayer Ag Reactor system
CH644828A5 (en) * 1979-11-10 1984-08-31 Deppen Jean Claude Process for the manufacture of permeable prefabricated components and device for making use of this process
US4670404A (en) * 1985-04-22 1987-06-02 Fike Corporation Micro-scale chemical process simulation methods and apparatus useful for design of full scale processes, emergency relief systems and associated equipment
EP0402018A1 (de) * 1989-05-31 1990-12-12 Halliburton Company Druckregelvorrichtung
WO1998036826A1 (en) * 1997-02-20 1998-08-27 Sinvent As Multiautoclave for combinatorial synthesis of zeolites and other materials
WO2000036399A1 (en) * 1998-12-15 2000-06-22 Union Carbide Chemicals & Plastics Technology Corporation Apparatus and methods for combinatorial chemical analysis

Also Published As

Publication number Publication date
EP1339486A2 (de) 2003-09-03
WO2002030557A2 (de) 2002-04-18
US20040013565A1 (en) 2004-01-22
AU2002213979A1 (en) 2002-04-22
DE10049078A1 (de) 2002-04-18
JP2004510575A (ja) 2004-04-08

Similar Documents

Publication Publication Date Title
WO2004024620A3 (en) Steam reforming process and apparatus
WO1998039099A8 (en) Apparatus and methods for the preparation of chemical compounds
CA2260810A1 (en) Process for preparing 1,4-butanediol by catalytic hydrogenation of 1,4-butinediol
EP1392428B1 (de) Für versuche mit hohem durchsatz geeignetes system
KR100940551B1 (ko) 이중-유동 밸브 및 내부 처리 용기 유리 시스템
WO2004105947A3 (en) Localized temperature control for spatial arrays of reaction media
MY144083A (en) System and method for performing a chemical experiment
CA2396191A1 (en) Catalytic reactor
WO2002064248A8 (en) Integrated reactors, methods of making same, and methods of conducting simultaneous exothermic and endothermic reactions
EP0056721A3 (de) Apparat für die chemische Synthese von Polynukleotiden
WO2002030557A3 (de) Autoklaven-array
WO2007036526A3 (fr) Reacteur et procede pour le traitement d'une matiere dans un milieu reactionnel fluide
WO2001093998A3 (en) Parallel semicontinuous or continuous reactors
MX2007008365A (es) Reactor catalitico.
DE69400047D1 (de) Hochdruckmelaminreaktor
AU2001284269A1 (en) Propulsion apparatus
EP1172137A3 (de) Labormassstab-Reaktionssystem
ZA200703051B (en) Hydrothermal synthesis in pressure vessels
US5316034A (en) Valve block assembly
WO2006055361A2 (en) Chlorine dioxide generator
CA2118047A1 (en) Method of retrofitting a heterogeneous exothermic synthesis reactor
CA2340712A1 (en) Method and device for carrying out biochemical reactions with a high throughput
EP1347829B1 (de) Array für mehrere behälter
DE69605554T2 (de) Gefäss für chemische synthesen und dieses verwendende system
DE3267955D1 (en) Reactor for the hydrogenation of a coal slurry

Legal Events

Date Code Title Description
AK Designated states

Kind code of ref document: A2

Designated state(s): AE AG AL AM AT AU AZ BA BB BG BR BY BZ CA CH CN CO CR CU CZ DE DK DM DZ EC EE ES FI GB GD GE GH GM HR HU ID IL IN IS JP KE KG KP KR KZ LC LK LR LS LT LU LV MA MD MG MK MN MW MX MZ NO NZ PH PL PT RO RU SD SE SG SI SK SL TJ TM TR TT TZ UA UG US UZ VN YU ZA ZW

AL Designated countries for regional patents

Kind code of ref document: A2

Designated state(s): GH GM KE LS MW MZ SD SL SZ TZ UG ZW AM AZ BY KG KZ MD RU TJ TM AT BE CH CY DE DK ES FI FR GB GR IE IT LU MC NL PT SE TR BF BJ CF CG CI CM GA GN GQ GW ML MR NE SN TD TG

AK Designated states

Kind code of ref document: A3

Designated state(s): AE AG AL AM AT AU AZ BA BB BG BR BY BZ CA CH CN CO CR CU CZ DE DK DM DZ EC EE ES FI GB GD GE GH GM HR HU ID IL IN IS JP KE KG KP KR KZ LC LK LR LS LT LU LV MA MD MG MK MN MW MX MZ NO NZ PH PL PT RO RU SD SE SG SI SK SL TJ TM TR TT TZ UA UG US UZ VN YU ZA ZW

AL Designated countries for regional patents

Kind code of ref document: A3

Designated state(s): GH GM KE LS MW MZ SD SL SZ TZ UG ZW AM AZ BY KG KZ MD RU TJ TM AT BE CH CY DE DK ES FI FR GB GR IE IT LU MC NL PT SE TR BF BJ CF CG CI CM GA GN GQ GW ML MR NE SN TD TG

121 Ep: the epo has been informed by wipo that ep was designated in this application
DFPE Request for preliminary examination filed prior to expiration of 19th month from priority date (pct application filed before 20040101)
WWE Wipo information: entry into national phase

Ref document number: 2001982380

Country of ref document: EP

WWE Wipo information: entry into national phase

Ref document number: 2002533993

Country of ref document: JP

REG Reference to national code

Ref country code: DE

Ref legal event code: 8642

WWE Wipo information: entry into national phase

Ref document number: 10381588

Country of ref document: US

WWP Wipo information: published in national office

Ref document number: 2001982380

Country of ref document: EP

WWW Wipo information: withdrawn in national office

Ref document number: 2001982380

Country of ref document: EP