WO2001090066A3 - Verfahren zur gewinnung von reinem n-vinylpyrrolidon - Google Patents

Verfahren zur gewinnung von reinem n-vinylpyrrolidon Download PDF

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Publication number
WO2001090066A3
WO2001090066A3 PCT/EP2001/006006 EP0106006W WO0190066A3 WO 2001090066 A3 WO2001090066 A3 WO 2001090066A3 EP 0106006 W EP0106006 W EP 0106006W WO 0190066 A3 WO0190066 A3 WO 0190066A3
Authority
WO
WIPO (PCT)
Prior art keywords
vinyl pyrrolidone
obtaining pure
stage
crystallisation
distillation
Prior art date
Application number
PCT/EP2001/006006
Other languages
English (en)
French (fr)
Other versions
WO2001090066A2 (de
Inventor
Bernd Eck
Joerg Heilek
Martin Schmidt-Radde
Herbert Helfert
Original Assignee
Basf Ag
Bernd Eck
Joerg Heilek
Martin Schmidt-Radde
Herbert Helfert
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag, Bernd Eck, Joerg Heilek, Martin Schmidt-Radde, Herbert Helfert filed Critical Basf Ag
Priority to EP01960244A priority Critical patent/EP1284962B1/de
Priority to DE50115263T priority patent/DE50115263D1/de
Priority to AT01960244T priority patent/ATE452123T1/de
Priority to JP2001586255A priority patent/JP5334348B2/ja
Priority to US10/296,046 priority patent/US6703511B2/en
Publication of WO2001090066A2 publication Critical patent/WO2001090066A2/de
Publication of WO2001090066A3 publication Critical patent/WO2001090066A3/de

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
    • C07D207/02—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D207/18—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
    • C07D207/22—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D207/24—Oxygen or sulfur atoms
    • C07D207/26—2-Pyrrolidones
    • C07D207/263—2-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms
    • C07D207/267—2-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to the ring nitrogen atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/16—Separation or purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pyrrole Compounds (AREA)

Abstract

Beschrieben wird ein Verfahren zur Gewinnung von reinem N-Vinylpyrrolidon aus N-Vinylpyrrolidon-haltigen Rohprodukten, umfassend ein ein- oder mehrstufiges Kristallisationsverfahren, dadurch gekennzeichnet, dass man die Mutterlauge der ersten Kristallisationsstufe entweder einer destillativen und/oder extraktiven Reinigung zuführt oder in einen N-Vinylpyrrolidon-haltigen Produktstrom des Herstellungsprozesses zurückführt.
PCT/EP2001/006006 2000-05-26 2001-05-25 Verfahren zur gewinnung von reinem n-vinylpyrrolidon WO2001090066A2 (de)

Priority Applications (5)

Application Number Priority Date Filing Date Title
EP01960244A EP1284962B1 (de) 2000-05-26 2001-05-25 Verfahren zur gewinnung von reinem n-vinylpyrrolidon
DE50115263T DE50115263D1 (de) 2000-05-26 2001-05-25 Verfahren zur gewinnung von reinem n-vinylpyrrolidon
AT01960244T ATE452123T1 (de) 2000-05-26 2001-05-25 Verfahren zur gewinnung von reinem n- vinylpyrrolidon
JP2001586255A JP5334348B2 (ja) 2000-05-26 2001-05-25 純粋なｎ−ビニルピロリドンの取得方法
US10/296,046 US6703511B2 (en) 2000-05-26 2001-05-25 Method for obtaining pure n-vinyl pyrrolidone

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10026233.3 2000-05-26
DE10026233A DE10026233A1 (de) 2000-05-26 2000-05-26 Verfahren zur Gewinnung von reinem N-Vinylpyrrolidon

Publications (2)

Publication Number Publication Date
WO2001090066A2 WO2001090066A2 (de) 2001-11-29
WO2001090066A3 true WO2001090066A3 (de) 2002-08-01

Family

ID=7643725

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2001/006006 WO2001090066A2 (de) 2000-05-26 2001-05-25 Verfahren zur gewinnung von reinem n-vinylpyrrolidon

Country Status (8)

Country Link
US (1) US6703511B2 (de)
EP (1) EP1284962B1 (de)
JP (1) JP5334348B2 (de)
CN (1) CN1213027C (de)
AT (1) ATE452123T1 (de)
DE (2) DE10026233A1 (de)
ES (1) ES2336890T3 (de)
WO (1) WO2001090066A2 (de)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10022988A1 (de) * 2000-05-11 2001-11-15 Basf Ag Verfahren zur Aufbereitung von Pyrrolidon- und N-Vinylpyrrolidon-Rückständen
DE10122787A1 (de) 2001-05-10 2002-06-06 Basf Ag Verfahren zur Herstellung einer gereinigten Schmelze wenigstens eines Monomeren
JP2004345994A (ja) * 2003-05-21 2004-12-09 Nippon Shokubai Co Ltd Ｎ−ビニル−２−ピロリドンの精製方法
DE102004058071A1 (de) * 2004-12-01 2006-06-08 Basf Ag Verfahren zur Reinigung von polaren Vinylverbindungen
US7138528B2 (en) * 2005-02-01 2006-11-21 Lyondell Chemical Technology, L.P. Method for crystallizing N-vinyl-2-pyrrolidone
US20090088579A1 (en) * 2005-04-11 2009-04-02 Nippon Shokubai Co., Ltd. Production Method of N-Vinyl-2-Pyrrolidone
JP2009120487A (ja) * 2006-02-17 2009-06-04 Nippon Shokubai Co Ltd Ｎ−ビニル−２−ピロリドンおよびその製造方法
DE102007043759A1 (de) * 2007-09-13 2008-09-11 Basf Se Verfahren zum Betreiben einer kontinuierlichen Abtrennung eines Zielproduktes X in Form von feinteiligem Kristallisat
DE102007043758A1 (de) * 2007-09-13 2008-10-23 Basf Se Verfahren zum Betreiben einer kontinuierlichen Abtrennung eines Zielproduktes X in Form von feinteiligem Kristallisat des Zielproduktes X
ES2400329T3 (es) * 2008-11-28 2013-04-09 Basf Se Procedimiento para la eliminación de subproductos de N-vinilamidas
CN103328443B (zh) * 2011-03-09 2016-08-10 三菱化学工程株式会社 Nmp的蒸馏装置
EP2835365A1 (de) 2013-08-06 2015-02-11 S.P.C.M. Sa Verfahren zur Herstellung N-Ethenyl-N-Alkyl-Alkylamiden
EP3173402B1 (de) * 2015-11-30 2018-03-21 Evonik Degussa GmbH Feinreinigung von isophoronnitril durch schmelzkristallisation
CN113444029B (zh) * 2021-07-03 2023-10-24 乌兰察布市珂玛新材料有限公司 一种n-乙烯基吡咯烷酮精制系统及工艺

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4873336A (en) * 1988-03-28 1989-10-10 Gaf Corporation Process for the preparation of N-vinyl lactams
DE3928982A1 (de) * 1989-09-01 1991-03-07 Basf Ag Verfahren zur herstellung von n,n'-disubstituierten 5-iminopyrrolidin-2-onen
US5508396A (en) * 1994-07-06 1996-04-16 Huels Aktiengesellschaft Process for preparing n-alkyllactams
EP0767169A1 (de) * 1995-10-02 1997-04-09 Basf Aktiengesellschaft Verfahren zur Reinigung von N-Vinylpyrrolidon durch Kristallisation

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0422366B1 (de) * 1989-09-01 1997-01-22 BASF Aktiengesellschaft Verfahren zur Herstellung N-substituierter Pyrrolidin-2-one
US5329021A (en) * 1993-02-04 1994-07-12 Isp Investments Inc. Process for the production of pure vinyl pyrrolidone

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4873336A (en) * 1988-03-28 1989-10-10 Gaf Corporation Process for the preparation of N-vinyl lactams
DE3928982A1 (de) * 1989-09-01 1991-03-07 Basf Ag Verfahren zur herstellung von n,n'-disubstituierten 5-iminopyrrolidin-2-onen
US5508396A (en) * 1994-07-06 1996-04-16 Huels Aktiengesellschaft Process for preparing n-alkyllactams
EP0767169A1 (de) * 1995-10-02 1997-04-09 Basf Aktiengesellschaft Verfahren zur Reinigung von N-Vinylpyrrolidon durch Kristallisation

Also Published As

Publication number Publication date
DE10026233A1 (de) 2001-11-29
WO2001090066A2 (de) 2001-11-29
ATE452123T1 (de) 2010-01-15
ES2336890T3 (es) 2010-04-19
CN1431994A (zh) 2003-07-23
US6703511B2 (en) 2004-03-09
US20030166947A1 (en) 2003-09-04
CN1213027C (zh) 2005-08-03
DE50115263D1 (de) 2010-01-28
JP5334348B2 (ja) 2013-11-06
JP2003534322A (ja) 2003-11-18
EP1284962A2 (de) 2003-02-26
EP1284962B1 (de) 2009-12-16

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