WO2001043504A1 - Procede de fabrication d'un dispositif chauffant de film electrothermique - Google Patents
Procede de fabrication d'un dispositif chauffant de film electrothermique Download PDFInfo
- Publication number
- WO2001043504A1 WO2001043504A1 PCT/CN2000/000398 CN0000398W WO0143504A1 WO 2001043504 A1 WO2001043504 A1 WO 2001043504A1 CN 0000398 W CN0000398 W CN 0000398W WO 0143504 A1 WO0143504 A1 WO 0143504A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- electric heating
- heating film
- base material
- protective layer
- film
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 11
- 239000000463 material Substances 0.000 claims abstract description 24
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910052751 metal Inorganic materials 0.000 claims abstract description 9
- 239000002184 metal Substances 0.000 claims abstract description 9
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 7
- 239000010439 graphite Substances 0.000 claims abstract description 7
- 229920000642 polymer Polymers 0.000 claims abstract description 7
- 238000005485 electric heating Methods 0.000 claims description 31
- 238000010438 heat treatment Methods 0.000 claims description 22
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 17
- 229910052709 silver Inorganic materials 0.000 claims description 14
- 239000004332 silver Substances 0.000 claims description 14
- 239000011241 protective layer Substances 0.000 claims description 12
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 claims description 4
- -1 cyanoamino Chemical group 0.000 claims description 4
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 4
- 229910000464 lead oxide Inorganic materials 0.000 claims description 4
- 239000010985 leather Substances 0.000 claims description 4
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 claims description 4
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 claims description 4
- 229920002943 EPDM rubber Polymers 0.000 claims description 3
- 241000779819 Syncarpia glomulifera Species 0.000 claims description 3
- 239000000853 adhesive Substances 0.000 claims description 3
- 230000001070 adhesive effect Effects 0.000 claims description 3
- 229920000180 alkyd Polymers 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 239000010410 layer Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 239000003973 paint Substances 0.000 claims description 3
- 239000001739 pinus spp. Substances 0.000 claims description 3
- 229920002635 polyurethane Polymers 0.000 claims description 3
- 239000004814 polyurethane Substances 0.000 claims description 3
- 239000000843 powder Substances 0.000 claims description 3
- 229940036248 turpentine Drugs 0.000 claims description 3
- 238000005266 casting Methods 0.000 claims description 2
- 229920001971 elastomer Polymers 0.000 claims description 2
- 229920001973 fluoroelastomer Polymers 0.000 claims description 2
- 150000002736 metal compounds Chemical class 0.000 claims description 2
- 238000003825 pressing Methods 0.000 claims description 2
- 238000009413 insulation Methods 0.000 abstract description 7
- 238000000576 coating method Methods 0.000 abstract description 5
- 239000011248 coating agent Substances 0.000 abstract description 4
- 239000000758 substrate Substances 0.000 abstract description 4
- WABPQHHGFIMREM-UHFFFAOYSA-N lead(0) Chemical compound [Pb] WABPQHHGFIMREM-UHFFFAOYSA-N 0.000 abstract description 3
- 239000002002 slurry Substances 0.000 abstract description 3
- 230000002035 prolonged effect Effects 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 230000001680 brushing effect Effects 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 229920001730 Moisture cure polyurethane Polymers 0.000 description 1
- 239000011247 coating layer Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- VTRUBDSFZJNXHI-UHFFFAOYSA-N oxoantimony Chemical compound [Sb]=O VTRUBDSFZJNXHI-UHFFFAOYSA-N 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000007650 screen-printing Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
- H05B3/10—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor
- H05B3/12—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor characterised by the composition or nature of the conductive material
- H05B3/14—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor characterised by the composition or nature of the conductive material the material being non-metallic
- H05B3/145—Carbon only, e.g. carbon black, graphite
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
- H05B3/20—Heating elements having extended surface area substantially in a two-dimensional plane, e.g. plate-heater
- H05B3/34—Heating elements having extended surface area substantially in a two-dimensional plane, e.g. plate-heater flexible, e.g. heating nets or webs
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B2203/00—Aspects relating to Ohmic resistive heating covered by group H05B3/00
- H05B2203/013—Heaters using resistive films or coatings
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B2203/00—Aspects relating to Ohmic resistive heating covered by group H05B3/00
- H05B2203/017—Manufacturing methods or apparatus for heaters
Definitions
- the present invention relates to a method for manufacturing electric heating parts for daily electric heating, heating and heat-retaining daily necessities, in particular to a method for producing electrothermal film heating elements on flexible materials for daily necessities.
- the ordinary daily necessities for electric heating and thermal insulation used by people generally use metal electric heating wire as a heating element, and metal heating wire as an electric heating element has low thermal efficiency, large energy consumption, easy oxidation, poor insulation performance, and long service life.
- the application range of this metal heating wire heating body is also limited to a certain extent. Therefore, people invented the electric heating film heating body, and then applied research to form a batch of new daily life electrical appliances.
- the products of these electric heating films are mostly metal hard materials, and they are fixed and welded. All are relatively convenient, with high thermal efficiency, low energy consumption, not easy oxidation, and good insulation safety.
- the purpose of the present invention is to provide a method for manufacturing a flexible electric heating film heating element.
- the manufactured heating film heating element is fixed on a soft base material, can be bent, can be stretched within a certain range, and the electrode lead can be firmly fixed. It is fixed with the electric heating film layer, with long service life and good insulation safety.
- a method for manufacturing a flexible electric heating film heating element is as follows:
- ⁇ firstly apply a silver paste with a content of more than 50% on any surface of the polymer flexible matrix material polyurethane, fluororubber, EPDM leather in various patterns and shapes, after 100 to 130 ° C, Bake for 5 to 25 minutes, or dry naturally to form a silver paste conductive electrode. At this time, the silver paste content is above 96%, and a lead wire can be soldered on the electrode as a lead-out wire.
- colloidal graphite powder 85 47%, water-soluble alkyd resin cyanoamino paint 8. 55%, three oxygen Antimony powder 5.13%, and any one or several metal compounds of lead oxide, manganese dioxide, and ferric oxide 0.85%.
- Graphite slurry formulated into a homogeneous slurry is coated in the desired pattern shape.
- An electric heating film is formed on the surface of the base material and on the metal electrode.
- an insulating protective layer may be fixed on the surface of the base material having the electric heating film by casting or pressing.
- composition of the silver paste described above is silver powder and turpentine.
- the thickness of the electrothermal film according to the present invention is 10 to 300 microns.
- the above method for fixing the insulating protective layer on the surface of the base material of the electrothermal film according to the present invention can use a polymer prepolymer and a curing agent to be cast and covered on the surface of the base material with the electrothermal film to cure or cure at room temperature to form a strong bond
- the insulating sealing protective layer, or the polymer sheet insulating protective layer that is prefabricated according to the shape and size, is coated with a rubber adhesive and pressed against the surface of the base material of the electric heating film to form a strong bonded insulating protective layer.
- the invention has the advantages that the heating element of the electric heating film is fixed on the flexible base material, can be bent, can be stretched within a certain range, the wire can be firmly fixed on the heating film layer, and has a long service life and good insulation safety.
- FIG. 1 is a schematic diagram of shapes of a silver paste conductive electrode and an electrothermal film coated by the method of the present invention.
- a 2 mm thick polyurethane matrix material that has been processed into the desired shape and size is selected, wiped clean with ethanol, and dried naturally.
- the electrode lead wire can be welded at any point on the electrode.
- colloidal graphite powder Use 100 parts by weight of colloidal graphite powder, 10 parts of water-soluble alkyd resin cyanoamino paint, 6 parts of antimony trioxide powder, and 1 part of lead oxide.
- the colloidal graphite paste is brush-coated on the surface of the base material with the electrode in the shape shown in FIG. 1. The two ends of the brush-coating layer are connected to the electrode part. Dry naturally.
- the polyurethane prepolymer is mixed with the conventionally used curing agent and cast on a base material with an electric heating film and The upper surface of the electrode covers the electrode and the electrothermal film. Its thickness can be 0.1 to 3 mm. It can be vulcanized on a vulcanizing machine at 120 ° C ⁇ 5 ° C.
- the pressure is 1-3 MP / c and the time is 10 To 20 minutes, an insulating protective layer is formed, that is, the preparation of the flexible electric heating film heating body is completed.
- the power of the flexible electric heating film heating body can be from 0.1 to 1 5W / C m 2 , the voltage is from 3 to 24V, and A relay controller is also installed to control the temperature.
- the flexible base material is ethylene-propylene-diene rubber
- the electrode coating method is 80-mesh screen printing, which can control the thickness of the coating to be uniform and dry naturally.
- the metal In addition to lead oxide, the compound can also be added together with an appropriate amount of ferric oxide. After covering the insulating protective layer, it is best to cure at room temperature.
- the base material is selected as leather
- the insulating and protective layer is made of a leather sheet that has been prefabricated according to the shape and size and pressed against the base material with an adhesive to complete the preparation of the flexible electric film heating element.
- the shape and size of the silver paste conductive electrode of the present invention are made of various types of products and processed by brushing when needed.
- the area and shape covered by the brush coating of colloidal graphite paste are also designed according to the needs of different types of products.
- the comprehensive design of the thickness and area of the brush is set according to different parameters such as temperature and voltage required by various products.
Landscapes
- Surface Heating Bodies (AREA)
- Resistance Heating (AREA)
Description
Claims
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AU11270/01A AU1127001A (en) | 1999-12-10 | 2000-10-30 | A manufacture method of electrothermal film heater |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN99117279A CN1074234C (zh) | 1999-12-10 | 1999-12-10 | 一种柔性电热膜发热体的制造方法 |
CN99117279.5 | 1999-12-10 |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2001043504A1 true WO2001043504A1 (fr) | 2001-06-14 |
Family
ID=5279915
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/CN2000/000398 WO2001043504A1 (fr) | 1999-12-10 | 2000-10-30 | Procede de fabrication d'un dispositif chauffant de film electrothermique |
Country Status (3)
Country | Link |
---|---|
CN (1) | CN1074234C (zh) |
AU (1) | AU1127001A (zh) |
WO (1) | WO2001043504A1 (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113873699A (zh) * | 2021-10-11 | 2021-12-31 | 中暖新能源(青岛)有限公司 | 一种发热均匀的电热薄膜材料及其制作方法 |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101227769B (zh) * | 2007-01-19 | 2011-12-28 | 天津市华林伟业科技发展有限公司 | 软体电光转换面发射体的制造方法 |
CN102932974B (zh) * | 2012-11-20 | 2014-10-15 | 叶么华 | 高分子电热膜制备方法 |
CN106726133A (zh) * | 2017-03-06 | 2017-05-31 | 王敏 | 一种石墨烯频谱护眼罩及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4656339A (en) * | 1980-08-28 | 1987-04-07 | Flexwatt Corporation | Electrical resistance heater |
CN1080109A (zh) * | 1992-06-12 | 1993-12-29 | 王涛 | 一种复合电热膜 |
CN1106850A (zh) * | 1994-09-20 | 1995-08-16 | 华中理工大学 | 电发热涂料 |
-
1999
- 1999-12-10 CN CN99117279A patent/CN1074234C/zh not_active Expired - Fee Related
-
2000
- 2000-10-30 AU AU11270/01A patent/AU1127001A/en not_active Abandoned
- 2000-10-30 WO PCT/CN2000/000398 patent/WO2001043504A1/zh active Application Filing
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4656339A (en) * | 1980-08-28 | 1987-04-07 | Flexwatt Corporation | Electrical resistance heater |
CN1080109A (zh) * | 1992-06-12 | 1993-12-29 | 王涛 | 一种复合电热膜 |
CN1106850A (zh) * | 1994-09-20 | 1995-08-16 | 华中理工大学 | 电发热涂料 |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113873699A (zh) * | 2021-10-11 | 2021-12-31 | 中暖新能源(青岛)有限公司 | 一种发热均匀的电热薄膜材料及其制作方法 |
Also Published As
Publication number | Publication date |
---|---|
AU1127001A (en) | 2001-06-18 |
CN1258186A (zh) | 2000-06-28 |
CN1074234C (zh) | 2001-10-31 |
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