WO1979000405A1 - Process for the production of d,l-2-amino-4-methylsulphosphino-butyric acid - Google Patents

Process for the production of d,l-2-amino-4-methylsulphosphino-butyric acid Download PDF

Info

Publication number
WO1979000405A1
WO1979000405A1 PCT/JP1978/000058 JP7800058W WO7900405A1 WO 1979000405 A1 WO1979000405 A1 WO 1979000405A1 JP 7800058 W JP7800058 W JP 7800058W WO 7900405 A1 WO7900405 A1 WO 7900405A1
Authority
WO
WIPO (PCT)
Prior art keywords
amino
methylsulphosphino
production
butyric acid
oxopropylmethylphosphinic
Prior art date
Application number
PCT/JP1978/000058
Other languages
English (en)
French (fr)
Japanese (ja)
Inventor
A Suzuki
S Inouye
T Tsuruoka
T Takematsu
K Mizutani
K Tachibana
Y Sekizawa
Original Assignee
Meiji Seika Kaisha
A Suzuki
S Inouye
T Tsuruoka
T Takematsu
K Mizutani
K Tachibana
Y Sekizawa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Meiji Seika Kaisha, A Suzuki, S Inouye, T Tsuruoka, T Takematsu, K Mizutani, K Tachibana, Y Sekizawa filed Critical Meiji Seika Kaisha
Priority to DE782857282T priority Critical patent/DE2857282T1/de
Publication of WO1979000405A1 publication Critical patent/WO1979000405A1/ja

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/32—Esters thereof
    • C07F9/3205—Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
    • C07F9/3211—Esters of acyclic saturated acids which can have further substituents on alkyl
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/301—Acyclic saturated acids which can have further substituents on alkyl

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
PCT/JP1978/000058 1977-12-19 1978-12-18 Process for the production of d,l-2-amino-4-methylsulphosphino-butyric acid WO1979000405A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DE782857282T DE2857282T1 (de) 1977-12-19 1978-12-18 Process for the production of d,l-2-amino-4-methylsulphosphino-butyric acid

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP77/151632 1977-12-19
JP15163277A JPS5484529A (en) 1977-12-19 1977-12-19 Production of d,l-2-amino-4-methylphosphinobutyric acid

Publications (1)

Publication Number Publication Date
WO1979000405A1 true WO1979000405A1 (en) 1979-07-12

Family

ID=15522776

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP1978/000058 WO1979000405A1 (en) 1977-12-19 1978-12-18 Process for the production of d,l-2-amino-4-methylsulphosphino-butyric acid

Country Status (7)

Country Link
US (1) US4264532A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
EP (1) EP0009022B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
JP (1) JPS5484529A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
DE (1) DE2857282T1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
GB (1) GB2036028B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
IT (1) IT1160363B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
WO (1) WO1979000405A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001515084A (ja) * 1997-08-20 2001-09-18 ヘキスト・シエーリング・アグレボ・ゲゼルシヤフト・ミト・ベシユレンクテル・ハフツング グルホシネートおよびそのための中間体の製造法
CN107286191A (zh) * 2017-04-16 2017-10-24 内蒙古佳瑞米精细化工有限公司 一种草铵膦中间体甲基丙醛基膦酸乙酯的制备方法

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3008186A1 (de) * 1980-03-04 1981-10-15 Hoechst Ag, 6000 Frankfurt Synergistische kombinationen von phosphinothricin
US4466913A (en) * 1981-06-30 1984-08-21 Maiji Seika Kaisha Ltd. Phosphorus-containing compounds and process for producing the same
JPS58131993A (ja) * 1982-01-29 1983-08-06 Meiji Seika Kaisha Ltd ビニルホスフィン酸誘導体の製造法
JPS63140178A (ja) * 1986-12-02 1988-06-11 Nissen Corp 圧力容器の安全装置
JP2682833B2 (ja) * 1988-03-03 1997-11-26 日産化学工業株式会社 有機燐誘導体及びその製造法
DE3907439A1 (de) * 1988-07-14 1990-09-13 Hoechst Ag Verfahren zur herstellung von n-acyl-phosphinothricin-p-estern
DE3913891A1 (de) * 1988-07-14 1990-10-31 Hoechst Ag Verfahren zur herstellung von n-acyl-phosphinothricindiestern
DE3900331A1 (de) * 1989-01-07 1990-07-12 Hoechst Ag Methyl-3,3-dialkoxy-1-propyl-phosphinsaeureester, die entsprechenden 3-oxoverbindungen sowie ein verfahren zu deren herstellung
FR2650157B1 (fr) * 1989-07-26 1993-04-16 Roussel Uclaf Compositions insecticides renfermant comme principe actif le glufosinate ou l'un de ses sels
KR100398892B1 (ko) * 2000-10-05 2003-09-19 전길자 신규한 항진균성 화합물 및 이를 함유하는 항진균 조성물
CN102177164B (zh) * 2008-11-05 2015-02-11 科莱恩金融(Bvi)有限公司 利用烯丙醇/丙烯醛制备二烷基次膦酸、二烷基次膦酸酯和二烷基次膦酸盐的方法,以及它们的用途
DE102008055914A1 (de) * 2008-11-05 2010-05-06 Clariant International Limited Verfahren zur Herstellung von mono-hydroxyfunktionalisierten Dialkylphosphinsäuren, -estern und -salzen mittels Acroleinen und ihre Verwendung
PH12014500673A1 (en) 2011-09-30 2014-05-05 Meiji Seika Pharma Co Ltd Method for producing glufosinate p free acid
CN103183707B (zh) * 2011-12-30 2016-06-15 中化蓝天集团有限公司 一种草胺膦的制备方法
CN103819503B (zh) * 2014-02-15 2016-03-02 山东滨农科技有限公司 一种草铵膦的纯化工艺
CN104497039B (zh) * 2014-12-23 2017-03-15 利尔化学股份有限公司 一种氨基腈的制备方法及用于制备草铵膦的中间体
CN105315303B (zh) * 2015-05-29 2017-07-04 山东潍坊润丰化工股份有限公司 一种草铵膦的分离纯化方法
CN105001259B (zh) * 2015-07-28 2017-07-21 河北威远生化农药有限公司 一种连续化生产3‑(甲基羟基膦酰基)丙醛的工艺和设备
CN107236001A (zh) * 2016-04-06 2017-10-10 四川省乐山市福华通达农药科技有限公司 一种膦醛的合成方法
CN108148091B (zh) * 2016-12-02 2020-01-14 利尔化学股份有限公司 一种草铵膦的清洁制备方法
CN109134534B (zh) * 2018-08-08 2020-09-08 江苏好收成韦恩农化股份有限公司 一种3,3-二烷氧基丙基甲基膦酸酯简易制备方法
CN109879910A (zh) * 2018-10-22 2019-06-14 江苏长青农化股份有限公司 一种草铵膦中间体的制备方法
CN109232645A (zh) * 2018-11-05 2019-01-18 南京红太阳生物化学有限责任公司 一种草铵膦中间体的制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5273825A (en) * 1975-12-16 1977-06-21 Toyobo Co Ltd Preparation of organic phosphorous compounds
JPS52139727A (en) * 1976-05-17 1977-11-21 Hoechst Ag Weed killer

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB694772A (en) * 1948-07-10 1953-07-29 Us Rubber Co Improvements in phosphonic acid esters
US2631162A (en) * 1949-09-13 1953-03-10 Us Rubber Co Method of reacting alpha, alphapolyhalogenated alkanals and organo-phosphorus compounds and products resulting therefrom
US2664438A (en) * 1950-11-03 1953-12-29 Us Rubber Co Dialkyl 3-dodecyloxypropane-1-phosphonate
JPS5521756B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * 1972-06-07 1980-06-12
US3832394A (en) * 1972-07-17 1974-08-27 Meiji Seika Kaisha Methanephosphinylethane substituted amid trimer of alanine
DD130354A1 (de) * 1977-04-06 1978-03-22 Herbert Teichmann Verfahren zur herstellung von substituierten beta-nitroaethan-phosphonsaeure-und-phosphinsaeureestern

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5273825A (en) * 1975-12-16 1977-06-21 Toyobo Co Ltd Preparation of organic phosphorous compounds
JPS52139727A (en) * 1976-05-17 1977-11-21 Hoechst Ag Weed killer

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
CHEMICAL ABSTRACTS Vol. 85, No. 1 (1976-6-5) (Columbus Ohio. U.S.A.) G. EWA, et al. "New synthesis of phosphinothricin and anologs" see page 467, lefthand column, Abstract No. 5777 y Rocz. Chem., 1975, 49(12), 2127-8 (Eng). *
Kagakudaijiten Henshuiinkai" Kagakudaijiten Vol. 4" (1960.12.30) Kyoritsu Shuppan page 715. *
Kotake Muzo "Daiyukikagaku Vol. 3., Shiboo-kukagobutsu II" (1957.8.30) Asakura Shoten, pages 3 and 49. *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001515084A (ja) * 1997-08-20 2001-09-18 ヘキスト・シエーリング・アグレボ・ゲゼルシヤフト・ミト・ベシユレンクテル・ハフツング グルホシネートおよびそのための中間体の製造法
CN107286191A (zh) * 2017-04-16 2017-10-24 内蒙古佳瑞米精细化工有限公司 一种草铵膦中间体甲基丙醛基膦酸乙酯的制备方法

Also Published As

Publication number Publication date
JPS5484529A (en) 1979-07-05
IT1160363B (it) 1987-03-11
DE2857282T1 (de) 1980-12-04
GB2036028A (en) 1980-06-25
JPS61837B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1986-01-11
US4264532A (en) 1981-04-28
GB2036028B (en) 1982-05-06
EP0009022A1 (en) 1980-03-19
IT7830961A0 (it) 1978-12-18
EP0009022B1 (en) 1982-07-07
DE2857282C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1988-08-25

Similar Documents

Publication Publication Date Title
WO1979000405A1 (en) Process for the production of d,l-2-amino-4-methylsulphosphino-butyric acid
DE2963619D1 (en) Process for the production of ethanol and/or acetaldehyde by reacting methanol with synthesis gas
AU520674B2 (en) Production of l-lysine by fermentation
ES450536A1 (es) Procedimiento para la obtencion de cromanonas-(4).
GB1399309A (en) Processes for producing beta-phenylserine derivatives
ES8204978A1 (es) Procedimiento para la fabricacion del acido b-hidroxibutiri-co o sus oligocondensados
ZA786181B (en) Process for the production of acetaldehyde by the reaction of methanol with synthesis gas
AU7674881A (en) Hydroxycyanomethylphosphonic acid
JPS55105658A (en) Manufacture of methyleneebiss*44phenylcarbamic ester*
JPS5599194A (en) Production of aldonic acid by enzyme method
GB1429166A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
GB2006201A (en) Production of nitroguanidine from guanidine nitrate and nitric acid
GB1462472A (en) Process for preparing p-aminobenzoic acid
ATE60092T1 (de) Verfahren zur herstellung von kaliumnitrat.
ES8101611A1 (es) Un procedimiento para preparar vindesina
IE44046L (en) Cyclopropanes
WO1979000358A1 (en) 5-cyano-1-methylpyrol-2-acetic acid and process for the production thereof
IE41605L (en) A tetrapeptide amide
JPS51125252A (en) Process for preparing substituted cyclopropanecarboxylic acid esters
JPS5626861A (en) Manufacture of methyleneebissphenylcarbamic ester and polymethyleneepolyphenylcarbamic ester
YU43223B (en) Process for obtaining special pure 4-amino-5-chloro-1-phenyl-pyridazone(6)
SU642302A1 (ru) Способ получени 2-фтор-2,2-динитроэтилсерной кислоты
JPS5265222A (en) Preparation of phosphoric acid ester having perfluoroalkyl group
GB1515640A (en) Process for the synthesis of 3-benzoylhydratropic acid
JPS51127080A (en) A process for preparing quisqualic acid.

Legal Events

Date Code Title Description
AK Designated states

Designated state(s): DE GB JP US

AL Designated countries for regional patents

Designated state(s): FR

RET De translation (de og part 6b)

Ref country code: DE

Ref document number: 2857282

Date of ref document: 19801204

Format of ref document f/p: P