US20210193909A1 - Method of manufacturing ultrasonic sensors - Google Patents
Method of manufacturing ultrasonic sensors Download PDFInfo
- Publication number
- US20210193909A1 US20210193909A1 US17/270,425 US201917270425A US2021193909A1 US 20210193909 A1 US20210193909 A1 US 20210193909A1 US 201917270425 A US201917270425 A US 201917270425A US 2021193909 A1 US2021193909 A1 US 2021193909A1
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- US
- United States
- Prior art keywords
- piezoelectric
- sintering
- piezoelectric material
- unit
- ultrasonic sensors
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 238000004519 manufacturing process Methods 0.000 title claims abstract description 13
- 239000000463 material Substances 0.000 claims abstract description 53
- 238000005245 sintering Methods 0.000 claims abstract description 39
- 239000000758 substrate Substances 0.000 claims abstract description 39
- 238000000034 method Methods 0.000 claims abstract description 34
- 238000011049 filling Methods 0.000 claims abstract description 9
- 239000002245 particle Substances 0.000 claims description 20
- 239000000843 powder Substances 0.000 claims description 17
- 239000011230 binding agent Substances 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 4
- 238000005507 spraying Methods 0.000 claims description 4
- 230000000052 comparative effect Effects 0.000 description 10
- 235000012431 wafers Nutrition 0.000 description 10
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- 229910001887 tin oxide Inorganic materials 0.000 description 2
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- XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 description 1
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- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- RAXXELZNTBOGNW-UHFFFAOYSA-O Imidazolium Chemical compound C1=C[NH+]=CN1 RAXXELZNTBOGNW-UHFFFAOYSA-O 0.000 description 1
- 229910003781 PbTiO3 Inorganic materials 0.000 description 1
- PCNDJXKNXGMECE-UHFFFAOYSA-N Phenazine Natural products C1=CC=CC2=NC3=CC=CC=C3N=C21 PCNDJXKNXGMECE-UHFFFAOYSA-N 0.000 description 1
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical group C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 1
- 229910052772 Samarium Inorganic materials 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 229910010252 TiO3 Inorganic materials 0.000 description 1
- 229910008559 TiSrO3 Inorganic materials 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 238000003491 array Methods 0.000 description 1
- JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical class [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 230000015271 coagulation Effects 0.000 description 1
- 238000005345 coagulation Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000003989 dielectric material Substances 0.000 description 1
- 238000001312 dry etching Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- AMGQUBHHOARCQH-UHFFFAOYSA-N indium;oxotin Chemical compound [In].[Sn]=O AMGQUBHHOARCQH-UHFFFAOYSA-N 0.000 description 1
- 239000002608 ionic liquid Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- URLJKFSTXLNXLG-UHFFFAOYSA-N niobium(5+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[Nb+5].[Nb+5] URLJKFSTXLNXLG-UHFFFAOYSA-N 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000010287 polarization Effects 0.000 description 1
- 238000005498 polishing Methods 0.000 description 1
- 239000002952 polymeric resin Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 1
- -1 pyrrolidinium halide Chemical class 0.000 description 1
- 238000007650 screen-printing Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- VEALVRVVWBQVSL-UHFFFAOYSA-N strontium titanate Chemical compound [Sr+2].[O-][Ti]([O-])=O VEALVRVVWBQVSL-UHFFFAOYSA-N 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- ZNOKGRXACCSDPY-UHFFFAOYSA-N tungsten trioxide Chemical compound O=[W](=O)=O ZNOKGRXACCSDPY-UHFFFAOYSA-N 0.000 description 1
- 238000001039 wet etching Methods 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B06—GENERATING OR TRANSMITTING MECHANICAL VIBRATIONS IN GENERAL
- B06B—METHODS OR APPARATUS FOR GENERATING OR TRANSMITTING MECHANICAL VIBRATIONS OF INFRASONIC, SONIC, OR ULTRASONIC FREQUENCY, e.g. FOR PERFORMING MECHANICAL WORK IN GENERAL
- B06B1/00—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency
- B06B1/02—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy
- B06B1/06—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy operating with piezoelectric effect or with electrostriction
- B06B1/0607—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy operating with piezoelectric effect or with electrostriction using multiple elements
- B06B1/0622—Methods or apparatus for generating mechanical vibrations of infrasonic, sonic, or ultrasonic frequency making use of electrical energy operating with piezoelectric effect or with electrostriction using multiple elements on one surface
- B06B1/0629—Square array
-
- H01L41/43—
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/01—Manufacture or treatment
- H10N30/09—Forming piezoelectric or electrostrictive materials
- H10N30/093—Forming inorganic materials
- H10N30/097—Forming inorganic materials by sintering
-
- H01L41/0477—
-
- H01L41/09—
-
- H01L41/332—
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/01—Manufacture or treatment
- H10N30/08—Shaping or machining of piezoelectric or electrostrictive bodies
- H10N30/082—Shaping or machining of piezoelectric or electrostrictive bodies by etching, e.g. lithography
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/01—Manufacture or treatment
- H10N30/08—Shaping or machining of piezoelectric or electrostrictive bodies
- H10N30/084—Shaping or machining of piezoelectric or electrostrictive bodies by moulding or extrusion
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/20—Piezoelectric or electrostrictive devices with electrical input and mechanical output, e.g. functioning as actuators or vibrators
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/80—Constructional details
- H10N30/85—Piezoelectric or electrostrictive active materials
- H10N30/853—Ceramic compositions
- H10N30/8536—Alkaline earth metal based oxides, e.g. barium titanates
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/80—Constructional details
- H10N30/85—Piezoelectric or electrostrictive active materials
- H10N30/853—Ceramic compositions
- H10N30/8548—Lead-based oxides
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/80—Constructional details
- H10N30/87—Electrodes or interconnections, e.g. leads or terminals
-
- H—ELECTRICITY
- H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- H10N30/00—Piezoelectric or electrostrictive devices
- H10N30/80—Constructional details
- H10N30/87—Electrodes or interconnections, e.g. leads or terminals
- H10N30/877—Conductive materials
Definitions
- FIG. 2 is a cross-sectional view illustrating concave portions and convex portions of a micropattern formed on a substrate.
- FIG. 5 conceptually illustrates the shape of particles of a unit piezoelectric body after re-sintering in accordance with a method of the present invention.
- FIG. 9 is a scanning electron microscopy image of a preliminary piezoelectric body after sintering, which was formed in Comparative Example 1.
- FIG. 13 shows the impedance values of an ultrasonic sensor manufactured in Example 2.
- a method of manufacturing ultrasonic sensors includes forming a micropattern having concave and convex portions on an etchable substrate (S 1 ), filling a piezoelectric material in the concave portions of the micropattern (S 2 ), pressurizing the filled piezoelectric material (S 3 ), sintering the piezoelectric material to form preliminary piezoelectric bodies (S 4 ), re-sintering the preliminary piezoelectric bodies to form densely packed unit piezoelectric bodies (S 5 ), and forming electrode terminals at both ends of each of the unit piezoelectric bodies to produce a unit piezoelectric cell (S 6 ).
- the kinds of the solvent and the binder are not particularly limited so long as high concentrations of the solvent and the binder can be homogeneously mixed with the piezoelectric material powder.
- the piezoelectric material 300 is sintered to form preliminary piezoelectric bodies 300 ′.
- the re-sintering is performed at a temperature where the surfaces of the preliminary piezoelectric bodies are melted. Specifically, in S 5 , thermal energy is applied in an amount to melt only the surfaces of the preliminary piezoelectric bodies without changing the phase of the particles of the preliminary piezoelectric bodies to a liquid phase. The volume of the particles of the preliminary piezoelectric bodies increases after coagulation.
- An external circuit or module is connected to the electrode terminals formed at the ends of the re-sintered unit piezoelectric bodies 300 ′′ to drive the ultrasonic sensors 200 .
- Electrode terminals E 1 and E 2 Any material that is highly electrically conductive and has low resistance may be used without limitation for the electrode terminals E 1 and E 2 .
- An electrically conductive metal such as silver, copper or aluminum may be used as a material for the electrode terminals E 1 and E 2 .
- the electrode terminals may be stacked by screen printing a paste of the electrically conductive material powder according to a designed pattern of terminal wire electrodes (not illustrated), followed by molding and curing the paste.
- the paste is prepared by mixing the electrically conductive material powder with a binder.
- the substrate 100 can be removed by a photolithography process.
- An insulating dielectric material 400 may be filled in a space between the unit piezoelectric bodies to minimize interference between the unit piezoelectric bodies when a voltage is applied and an ultrasonic wave is transmitted and received.
- the insulating material is preferably a polymer resin.
- a micropattern with a line width of 50 ⁇ m was formed on a silicon wafer by a photolithography process.
- the substrate was removed by a photolithography process, an epoxy insulating material was filled, gold metal was deposited, wire electrodes were patterned by a photolithography process, and diced into ultrasonic sensors.
Landscapes
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Ceramic Engineering (AREA)
- Transducers For Ultrasonic Waves (AREA)
- Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR10-2018-0099287 | 2018-08-24 | ||
KR1020180099287A KR101965171B1 (ko) | 2018-08-24 | 2018-08-24 | 초음파센서의 제조방법 |
PCT/KR2019/000931 WO2020040376A1 (en) | 2018-08-24 | 2019-01-22 | Method of manufacturing ultrasonic sensors |
Publications (1)
Publication Number | Publication Date |
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US20210193909A1 true US20210193909A1 (en) | 2021-06-24 |
Family
ID=67624398
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US17/270,425 Pending US20210193909A1 (en) | 2018-08-24 | 2019-01-22 | Method of manufacturing ultrasonic sensors |
Country Status (6)
Country | Link |
---|---|
US (1) | US20210193909A1 (de) |
EP (1) | EP3841622A4 (de) |
JP (1) | JP7285590B2 (de) |
KR (1) | KR101965171B1 (de) |
CN (1) | CN113016085A (de) |
WO (1) | WO2020040376A1 (de) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112671367A (zh) * | 2020-12-24 | 2021-04-16 | 华南理工大学 | 一种新型fbar滤波器及其制备方法 |
Citations (4)
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JPS6087000A (ja) * | 1983-10-19 | 1985-05-16 | Hitachi Ltd | 超音波探触子 |
US20070090729A1 (en) * | 2005-10-25 | 2007-04-26 | Ngk Insulators, Ltd. | Piezoelectric/electrostrictive film and method for producing the same |
US20120169183A1 (en) * | 2010-12-30 | 2012-07-05 | Samsung Electro-Mechanics Co., Ltd. | Ceramic composition for piezoelectric actuator and method of manufacturing the same, and piezoelectric actuator manufactured by using the same |
US20140239774A1 (en) * | 2012-12-17 | 2014-08-28 | Virginia Tech Intellectual Properties, Inc. | NEW PROCESSING METHOD FOR GRAIN-ORIENTED LEAD-FREE PIEZOELECTRIC Na0.5Bi0.5TiO3-BaTiO3 CERAMICS EXHIBITING GIANT PERFORMANCE |
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JP4065049B2 (ja) * | 1998-03-19 | 2008-03-19 | オリンパス株式会社 | 圧電セラミクス構造体の製造方法及び複合圧電振動子の製造方法 |
JP2002012425A (ja) * | 2000-06-21 | 2002-01-15 | Tokai Rubber Ind Ltd | Pzt薄膜の製法およびそれにより得られたpzt構造体 |
JP2006261656A (ja) * | 2005-02-21 | 2006-09-28 | Brother Ind Ltd | 圧電アクチュエータおよびその製造方法 |
JP5967988B2 (ja) * | 2012-03-14 | 2016-08-10 | キヤノン株式会社 | 圧電材料、圧電素子、液体吐出ヘッド、超音波モータおよび塵埃除去装置 |
DE102013200243A1 (de) * | 2013-01-10 | 2014-07-10 | Robert Bosch Gmbh | Piezoelektrisches Bauteil und Verfahren zur Herstellung eines piezoelektrischen Bauteils |
CN103779272B (zh) * | 2013-01-11 | 2017-06-20 | 北京纳米能源与系统研究所 | 晶体管阵列及其制备方法 |
KR20150110126A (ko) * | 2014-03-24 | 2015-10-02 | 삼성전기주식회사 | 압전소자 및 이를 포함하는 압전진동자 |
JP6122066B2 (ja) * | 2015-06-24 | 2017-04-26 | 国立大学法人 熊本大学 | 高周波超音波圧電素子、その製造方法、及びそれを含む高周波超音波プローブ |
TWM534791U (zh) | 2016-07-20 | 2017-01-01 | 伍鐌科技股份有限公司 | 防震裝置及防震裝置包裝體 |
KR102091701B1 (ko) * | 2016-12-02 | 2020-03-20 | 한국기계연구원 | 손가락 생체정보 인식모듈과, 이것이 적용된 전자기기, 그리고 손가락 생체정보 인식모듈의 제조방법과 트랜스듀서의 제조방법 |
KR101830209B1 (ko) * | 2017-02-16 | 2018-02-21 | 주식회사 베프스 | 압전 센서 제조 방법 및 이를 이용한 압전 센서 |
KR101830205B1 (ko) * | 2017-02-17 | 2018-02-21 | 주식회사 베프스 | 압전 센서 제조 방법 및 이를 이용한 압전 센서 |
KR101850127B1 (ko) | 2017-03-16 | 2018-04-19 | 주식회사 베프스 | 초음파 지문 센서 제조 방법 |
KR101858731B1 (ko) * | 2017-08-22 | 2018-05-16 | 주식회사 베프스 | 압전 센서의 제조방법 |
-
2018
- 2018-08-24 KR KR1020180099287A patent/KR101965171B1/ko active
-
2019
- 2019-01-22 US US17/270,425 patent/US20210193909A1/en active Pending
- 2019-01-22 EP EP19853135.2A patent/EP3841622A4/de active Pending
- 2019-01-22 WO PCT/KR2019/000931 patent/WO2020040376A1/en unknown
- 2019-01-22 CN CN201980055688.4A patent/CN113016085A/zh active Pending
- 2019-01-22 JP JP2021534098A patent/JP7285590B2/ja active Active
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JPS6087000A (ja) * | 1983-10-19 | 1985-05-16 | Hitachi Ltd | 超音波探触子 |
US20070090729A1 (en) * | 2005-10-25 | 2007-04-26 | Ngk Insulators, Ltd. | Piezoelectric/electrostrictive film and method for producing the same |
US20120169183A1 (en) * | 2010-12-30 | 2012-07-05 | Samsung Electro-Mechanics Co., Ltd. | Ceramic composition for piezoelectric actuator and method of manufacturing the same, and piezoelectric actuator manufactured by using the same |
US20140239774A1 (en) * | 2012-12-17 | 2014-08-28 | Virginia Tech Intellectual Properties, Inc. | NEW PROCESSING METHOD FOR GRAIN-ORIENTED LEAD-FREE PIEZOELECTRIC Na0.5Bi0.5TiO3-BaTiO3 CERAMICS EXHIBITING GIANT PERFORMANCE |
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Also Published As
Publication number | Publication date |
---|---|
JP2021535699A (ja) | 2021-12-16 |
KR101965171B1 (ko) | 2019-08-13 |
JP7285590B2 (ja) | 2023-06-02 |
EP3841622A4 (de) | 2022-06-08 |
WO2020040376A1 (en) | 2020-02-27 |
EP3841622A1 (de) | 2021-06-30 |
CN113016085A (zh) | 2021-06-22 |
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