US20100261235A1 - Continuous production of biodiesel fuel by enzymatic method - Google Patents

Continuous production of biodiesel fuel by enzymatic method Download PDF

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Publication number
US20100261235A1
US20100261235A1 US12/745,962 US74596208A US2010261235A1 US 20100261235 A1 US20100261235 A1 US 20100261235A1 US 74596208 A US74596208 A US 74596208A US 2010261235 A1 US2010261235 A1 US 2010261235A1
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US
United States
Prior art keywords
catalyst reaction
oil
glycerin
lower alcohol
fat
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
US12/745,962
Other languages
English (en)
Inventor
Nobuyuki Kuratani
Shinji Hama
Hideo Noda
Hideki Fukuda
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BIO-ENERGY Corp
Kansai Chemical Engineering Co Ltd
Bio Energy Corp
Original Assignee
Kansai Chemical Engineering Co Ltd
Bio Energy Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kansai Chemical Engineering Co Ltd, Bio Energy Corp filed Critical Kansai Chemical Engineering Co Ltd
Assigned to BIO-ENERGY CORPORATION, KANSAI CHEMICAL ENGINEERING CO., LTD. reassignment BIO-ENERGY CORPORATION ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: FUKUDA, HIDEKI, HAMA, SHINJI, KURATANI, NOBUYUKI, NODA, HIDEO
Publication of US20100261235A1 publication Critical patent/US20100261235A1/en
Abandoned legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/64Fats; Fatty oils; Ester-type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
    • C12P7/6436Fatty acid esters
    • C12P7/649Biodiesel, i.e. fatty acid alkyl esters
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11CFATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00Preparation of oxygen-containing organic compounds
    • C12P7/62Carboxylic acid esters
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10Feedstock materials
    • C10G2300/1011Biomass
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00Technologies for the production of fuel of non-fossil origin
    • Y02E50/10Biofuels, e.g. bio-diesel
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P30/00Technologies relating to oil refining and petrochemical industry
    • Y02P30/20Technologies relating to oil refining and petrochemical industry using bio-feedstock

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Fats And Perfumes (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Apparatus Associated With Microorganisms And Enzymes (AREA)
US12/745,962 2007-12-14 2008-11-28 Continuous production of biodiesel fuel by enzymatic method Abandoned US20100261235A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2007323381 2007-12-14
JP2007-323381 2007-12-14
PCT/JP2008/072111 WO2009078290A1 (ja) 2007-12-14 2008-11-28 酵素法による連続式バイオディーゼル燃料の生産

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/072111 A-371-Of-International WO2009078290A1 (ja) 2007-12-14 2008-11-28 酵素法による連続式バイオディーゼル燃料の生産

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US14/741,755 Division US9879291B2 (en) 2007-12-14 2015-06-17 Continuous production of biodiesel fuel by enzymatic method

Publications (1)

Publication Number Publication Date
US20100261235A1 true US20100261235A1 (en) 2010-10-14

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Family Applications (2)

Application Number Title Priority Date Filing Date
US12/745,962 Abandoned US20100261235A1 (en) 2007-12-14 2008-11-28 Continuous production of biodiesel fuel by enzymatic method
US14/741,755 Expired - Fee Related US9879291B2 (en) 2007-12-14 2015-06-17 Continuous production of biodiesel fuel by enzymatic method

Family Applications After (1)

Application Number Title Priority Date Filing Date
US14/741,755 Expired - Fee Related US9879291B2 (en) 2007-12-14 2015-06-17 Continuous production of biodiesel fuel by enzymatic method

Country Status (7)

Country Link
US (2) US20100261235A1 (ja)
EP (1) EP2241631B1 (ja)
JP (1) JP5558831B2 (ja)
CN (1) CN101896614A (ja)
BR (1) BRPI0820588A2 (ja)
MY (1) MY153124A (ja)
WO (1) WO2009078290A1 (ja)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5607329B2 (ja) * 2009-09-01 2014-10-15 関西化学機械製作株式会社 酵素法による連続式バイオディーゼル燃料の生産方法
US8889895B2 (en) * 2011-03-08 2014-11-18 Cognis Ip Management Gmbh Process for the distillation of fatty acid esters
JP5986753B2 (ja) * 2012-01-31 2016-09-06 関西化学機械製作株式会社 酵素法による連続式バイオディーゼル燃料の生産方法
CN103305559B (zh) * 2012-03-12 2015-07-22 广州市名花香料有限公司 一种天然风味脂肪酸酯的制备方法
CN104651060B (zh) * 2015-02-03 2017-08-15 江苏卡特环保科技有限公司 生物柴油连续酯交换工艺
KR101534260B1 (ko) * 2015-02-16 2015-07-06 호남바이오영농조합법인 친환경 효소 에너지 조성물 및 이의 제조 방법
CN115106024B (zh) * 2022-07-04 2024-04-16 山东飞扬化工有限公司 一种混流反应器和混流反应设备及其用于生产碳酸酯的方法

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6359896A (ja) * 1986-09-01 1988-03-15 Agency Of Ind Science & Technol 固定化リパ−ゼによる油脂加水分解法
US6982155B1 (en) * 1999-11-26 2006-01-03 Kansai Chemical Engineering Co., Ltd. Process for producing fatty acid lower alcohol ester
US20060063242A1 (en) * 2004-09-20 2006-03-23 Chih-Chung Chou Fuel production
WO2006088254A2 (en) * 2005-02-21 2006-08-24 Nippon Shokubai Co., Ltd. Method for producing fatty acid alkyl esters and/or glycerin
WO2007043552A1 (en) * 2005-10-05 2007-04-19 Kao Corporation Method for producing a useful substance by use of an immobilized enzyme
US20070232818A1 (en) * 2005-11-15 2007-10-04 Domestic Energy Leasing, Llc Transesterification of oil to form biodiesels
CN200967808Y (zh) * 2006-10-26 2007-10-31 冯善茂 环保型生产生物柴油的酯化装置

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2000012743A1 (fr) 1998-09-01 2000-03-09 Kansai Chemical Engineering Co., Ltd. Procede de production d'ester d'alcool inferieur
JP2005350632A (ja) * 2004-06-14 2005-12-22 Electric Power Dev Co Ltd バイオディーゼル燃料の製造方法
JP5186083B2 (ja) * 2005-12-21 2013-04-17 株式会社日本触媒 油脂からの脂肪酸アルキルエステル及び/又はグリセリンの製造方法
US7420072B2 (en) * 2006-05-05 2008-09-02 Orbitek, Inc. Apparatus and method for producing biodiesel fuel

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6359896A (ja) * 1986-09-01 1988-03-15 Agency Of Ind Science & Technol 固定化リパ−ゼによる油脂加水分解法
US6982155B1 (en) * 1999-11-26 2006-01-03 Kansai Chemical Engineering Co., Ltd. Process for producing fatty acid lower alcohol ester
US20060063242A1 (en) * 2004-09-20 2006-03-23 Chih-Chung Chou Fuel production
WO2006088254A2 (en) * 2005-02-21 2006-08-24 Nippon Shokubai Co., Ltd. Method for producing fatty acid alkyl esters and/or glycerin
US20090069586A1 (en) * 2005-02-21 2009-03-12 Nippon Shokubai Co., Ltd. Method for producing fatty acid alkyl esters and/or glycerin
WO2007043552A1 (en) * 2005-10-05 2007-04-19 Kao Corporation Method for producing a useful substance by use of an immobilized enzyme
US20070232818A1 (en) * 2005-11-15 2007-10-04 Domestic Energy Leasing, Llc Transesterification of oil to form biodiesels
CN200967808Y (zh) * 2006-10-26 2007-10-31 冯善茂 环保型生产生物柴油的酯化装置

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
English language machine translation of CN200967808 (10/31/2007), pp. 1-3. *
Shimada, Y., et al., Enzymatic alcoholysis for biodiesel fuel production and application of the reactin to oil processing, 2002, Journa of Moecular Catalysis B: Enzymatic, pp 133 - 142 *

Also Published As

Publication number Publication date
US20150284748A1 (en) 2015-10-08
MY153124A (en) 2014-12-31
CN101896614A (zh) 2010-11-24
BRPI0820588A2 (pt) 2014-11-04
JP5558831B2 (ja) 2014-07-23
WO2009078290A1 (ja) 2009-06-25
US9879291B2 (en) 2018-01-30
EP2241631A1 (en) 2010-10-20
EP2241631B1 (en) 2015-04-15
EP2241631A4 (en) 2011-04-27
JPWO2009078290A1 (ja) 2011-04-28

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AS Assignment

Owner name: KANSAI CHEMICAL ENGINEERING CO., LTD., JAPAN

Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:KURATANI, NOBUYUKI;HAMA, SHINJI;NODA, HIDEO;AND OTHERS;REEL/FRAME:024478/0224

Effective date: 20100414

Owner name: BIO-ENERGY CORPORATION, JAPAN

Free format text: ASSIGNMENT OF ASSIGNORS INTEREST;ASSIGNORS:KURATANI, NOBUYUKI;HAMA, SHINJI;NODA, HIDEO;AND OTHERS;REEL/FRAME:024478/0224

Effective date: 20100414

STCB Information on status: application discontinuation

Free format text: ABANDONED -- FAILURE TO RESPOND TO AN OFFICE ACTION