US10427073B2 - Rotary pressure filter apparatus with reduced pressure fluctuations - Google Patents

Rotary pressure filter apparatus with reduced pressure fluctuations Download PDF

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Publication number
US10427073B2
US10427073B2 US15/322,320 US201515322320A US10427073B2 US 10427073 B2 US10427073 B2 US 10427073B2 US 201515322320 A US201515322320 A US 201515322320A US 10427073 B2 US10427073 B2 US 10427073B2
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United States
Prior art keywords
sealing member
compartments
cutout portion
rotary
solid
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US15/322,320
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US20180207558A1 (en
Inventor
Anders Bitsch-Larsen
Timothy H. Keyes
Thomas M. Bartos
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BHS Sonthofen GmbH
Ineos US Chemicals Co Inc
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BP Corp North America Inc
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Priority to US15/322,320 priority Critical patent/US10427073B2/en
Assigned to BP CORPORATION NORTH AMERICA INC. reassignment BP CORPORATION NORTH AMERICA INC. ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: BITSCH-LARSEN, Anders, KEYES, TIMOTHY, BARTOS, THOMAS
Publication of US20180207558A1 publication Critical patent/US20180207558A1/en
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Publication of US10427073B2 publication Critical patent/US10427073B2/en
Assigned to INEOS US CHEMICALS COMPANY reassignment INEOS US CHEMICALS COMPANY CHANGE OF NAME (SEE DOCUMENT FOR DETAILS). Assignors: BP AMOCO CHEMICAL COMPANY
Assigned to BHS-SONTHOFEN GMBH, BP AMOCO CHEMICAL COMPANY reassignment BHS-SONTHOFEN GMBH ASSIGNMENT OF ASSIGNORS INTEREST (SEE DOCUMENT FOR DETAILS). Assignors: BP CORPORATION NORTH AMERICA INC.
Assigned to HSBC CORPORATE TRUSTEE COMPANY (UK) LIMITED reassignment HSBC CORPORATE TRUSTEE COMPANY (UK) LIMITED FIRST LIEN INTELLECTUAL PROPERTY SECURITY AGREEMENT Assignors: INEOS US CHEMICALS COMPANY
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D33/00—Filters with filtering elements which move during the filtering operation
    • B01D33/06—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums
    • B01D33/067—Construction of the filtering drums, e.g. mounting or sealing arrangements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D33/00—Filters with filtering elements which move during the filtering operation
    • B01D33/06—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums
    • B01D33/073—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums arranged for inward flow filtration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D33/00—Filters with filtering elements which move during the filtering operation
    • B01D33/06—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums
    • B01D33/073—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums arranged for inward flow filtration
    • B01D33/09—Filters with filtering elements which move during the filtering operation with rotary cylindrical filtering surfaces, e.g. hollow drums arranged for inward flow filtration with surface cells independently connected to pressure distributors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D33/00—Filters with filtering elements which move during the filtering operation
    • B01D33/80—Accessories
    • B01D33/801—Driving means, shaft packing systems or the like
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2201/00—Details relating to filtering apparatus
    • B01D2201/34—Seals or gaskets for filtering elements
    • B01D2201/347—Radial sealings

Definitions

  • the present teachings relate generally to rotary pressure filter apparatus, and in particular, to a rotary pressure filter apparatus having a sealing member configured to reduce pressure fluctuations.
  • Rotary pressure filter apparatus have been designed to perform more than one of the steps of a multiple-stage separation technique in a single piece of equipment by progressing the material being processed through separate work zones.
  • known rotary pressure filter apparatus perform a filtration in a filter or feed zone to form a filter cake, followed by a washing of the filter cake in one or more wash zones. The washed filter cake may be dried in a drying zone before leaving the rotary pressure filter.
  • Rotary pressure filter apparatus are generally known in the art and are disclosed, for example, in U.S. Pat. Nos. 2,741,369, 7,807,060 and US Pat. App. 20050051473.
  • the present invention solves of the problem of pressure fluctuations in the rotary pressure filter by allowing for more gradual opening of filter compartments as the compartments enter a new zone in the apparatus.
  • the result is the potential for greater capacity in the rotary pressure filter apparatus, as well as improved lifespan for the filter elements as they are less prone to damaging movement as a result of pressure fluctuations.
  • a rotary pressure filter apparatus having improved flow characteristics.
  • the rotary pressure filter includes a housing capable of withstanding an internal pressure above ambient; a rotary drum having at least one generally round cross-section and configured to rotate inside the housing wall around an axis, a length of the axis defining a longitudinal direction; the rotary drum being spaced from the housing to define a generally annular plenum therebetween; at least one sealing member configured to contact the rotary drum, each sealing member separating the annular plenum between the housing and the rotary drum into zones, the sealing members adapted to pressure seal each zone from the other zones, the sealing member extending in a generally tangential direction and in the longitudinal direction, the sealing member having at least one cutout portion such that the size of the at least one cutoff portion in the generally tangential direction is variable along at least one portion of the longitudinal direction; at least one material passageway adapted to allow passage of material between the annular plenum in each zone and a location outside the housing; a plurality of compartment
  • a sealing apparatus for a rotary pressure filter has a a unitary body, the unitary body having a first side extending along a length and a width of the sealing member, a second side of the sealing element being spaced from the first side and connected to the first sides by edges, the volume between the first side and the second side defining a thickness of the sealing member, the second side being curved and concave relative to the first side, the second side configured to fit flush against the surface of a cylindrical drum, the second side having at least one cutout portion such that the width of the sealing is variable along at least one portion of its length; and a mechanism adapted to actuate the sealing member, the mechanism configured to move the sealing member in the direction of its thickness.
  • FIG. 1 shows a side view cross-section of a rotary pressure filter apparatus according to one embodiment of the present invention.
  • FIG. 2 shows a front view cross-section of a rotary pressure filter according to one embodiment of the present invention.
  • FIG. 3 shows an exploded perspective view of a portion of a rotary drum and a sealing member for use in one embodiment according to the present invention.
  • FIG. 4 shows a perspective view of a sealing member for use in one embodiment of the present invention.
  • FIG. 5 a shows a cross section of the sealing member of FIG. 4 .
  • FIG. 5 b shows another cross section of the sealing member of FIG. 4 .
  • FIG. 6 shows a perspective view of another embodiment of the sealing member in accordance with the present invention.
  • FIG. 7 shows a perspective view of another embodiment of the sealing member in accordance with the present invention.
  • FIG. 8 shows a perspective view of another embodiment of the sealing member in accordance with the present invention.
  • Rotary pressure filter apparatus for processing a solid-liquid mixture in a plurality of successive work zones.
  • Rotary pressure filter apparatus are generally known in the art and are disclosed, for example, in U.S. Pat. Nos. 2,741,369, 7,807,060 and US Pat. App. 20050051473.
  • the rotary pressure filter apparatus is used to recover a solid product, or a liquid, or both, from a solid/liquid mixture.
  • the solid product is a pharmaceutical or a food component product.
  • the solid product is a chemical, or in particular, a petrochemical.
  • the product is an aromatic hydrocarbon such as paraxylene.
  • the product is an aromatic carboxylic acid, such as terephthalic acid.
  • FIG. 1 a longitudinal cross section of rotary pressure filter apparatus in accordance with one embodiment of the invention is shown generally at 100 .
  • the rotary pressure filter apparatus 100 operates under a positive pressure to filter and remove liquid from a solid-liquid mixture and to collect a solid product for further processing.
  • the rotary pressure filter apparatus 100 includes a stationary housing 102 capable of withstanding an internal pressure above ambient.
  • the housing 102 is mounted upon a frame 104 .
  • Inside the housing 102 is a rotary filter drum 106 .
  • the rotary filter drum 106 rotates as indicated by arrow 108 around an axis 110 ( FIG. 1 ) at speed of about 0.4 to 2 RPM, and in some embodiments at a speed of about 0.8 to 1.5 RPM.
  • An axis 110 defines a longitudinal direction of the rotary drum 106 and the rotary pressure filter apparatus 100 .
  • the rotary filter drum 106 is driven by a drive mechanism 112 , which is also mounted on the frame 104 .
  • a shaft 114 connects the drive mechanism 112 to a control head portion 116 of the rotary drum 106 .
  • the surface of the rotary drum 106 is spaced from the inside of the housing 102 such that a generally annular plenum 118 is formed therebetween, Material passageways 120 a, 120 b , 120 c, 120 d, and 120 e, such as inlets and outlet piping, are adapted to allow passage of material between the annular plenum 118 and a location outside the housing 102 .
  • One or more sealing members 122 a, 122 b, 122 c, 122 d, 122 e are configured to contact the rotary drum 106 and divide the annular plenum 118 into a plurality of zones 124 a, 124 b, 124 c, 124 d, 124 e.
  • the sealing members 122 generally contact the rotary drum with enough pressure to pressure seal the zones 124 from each other but still allowing the rotary drum 106 to rotate.
  • the sealing members 122 are each part of a sealing device 126 which includes an actuating mechanism adapted to members 122 in the radial direction to exert force against the rotary drum 106 .
  • the actuating mechanism is a pneumatic device including an inlet 128 for introducing gas into a plenum 130 to exert a pressure force against the outer surface of the respective sealing member 122 .
  • Suitable pressure forces exerted by the pneumatic device include those about 0.8 to 2.0 bar above the highest pressure in any of the zones 124 a - 124 e of the rotary pressure filter apparatus 100 .
  • Those skilled in the art will recognize that other actuating mechanisms may be substituted for the pneumatic device.
  • a plurality of compartments 132 are arranged around the outer surface or circumference of the rotary filter drum 106 and rotate with the filter drum 106 .
  • the compartments 132 each include a filter member 134 (shown in one compartment in FIG. 3 ) adjacent the filter drum.
  • the filter member comprises a filter cloth supported over a metal screen in a filter housing (not shown).
  • the filter cloth is manufactured from a polyether ether ketone (PEEK) polymer or a polyvinylidene difluoride (PVDF) polymer.
  • PEEK polyether ether ketone
  • PVDF polyvinylidene difluoride
  • Each compartment 132 also has associated with it a corresponding outlet pipe 136 which also rotates with the filter drum 106 and the compartments 118 .
  • the outlet pipes 136 are configured such that filtrate received each compartment 118 passes through its corresponding filter member 134 adjacent the filter drum 106 and into its corresponding outlet pipe 136 .
  • the outlet pipes 136 remove the filtrate from the compartments 132 and deliver the filtrate to the control head 116 , where it is collected through additional piping (not shown) and removed from the rotary pressure filter apparatus 100 .
  • the compartments 132 rotate with the rotary drum 106 and accordingly pass sequentially pass through each of the zones 124 a, 124 b , 124 c, 124 d, 124 e.
  • the compartments 132 are arranged in rows of four along the longitudinal direction 110 . Those skilled in the art will recognize that other configurations of the compartments would be suitable as well.
  • a pressurized feed containing a solid-liquid mixture is introduced into the feed inlet material passageway 120 a and into plenum 118 in a first zone designated as feed zone 124 a.
  • the solid-liquid mixture is distributed into compartments 132 .
  • the pressure in the feed zone is maintained at about 3 bar(g) to about 7 bar(g), and in some embodiments, 5 bar(g) to 6 bar(g).
  • liquid of the solid-liquid mixture is forced through the filter member 134 into outlet pipes 136 . Filtrate thus exits the rotary pressure apparatus 100 through outlet pipes 136 .
  • the solid components of the solid-liquid mixture remain on the filter members 134 in the form of a filter cake.
  • wash fluid is introduced into plenum 118 for distribution into the compartments 132 to wash the cake remaining on the filter members 134 .
  • wash fluid in introduced at a rate of about 0.5 kg to about 1.5 kg of wash fluid per 1 kg of filter cake.
  • the wash fluid is removed by outlet 136 .
  • the rotary drum then continues to a second wash zone 124 c, where additional wash fluid is introduced into zone 124 c, designated as a second wash zone, and the cake on the filter members 134 is again washed.
  • the wash fluid is selected to remove impurities from the filter cake while not interfering with further processing of the filter cake to recover the final solid product.
  • the wash fluid comprises water.
  • the wash fluid comprises condensate from another portion of an integrated process.
  • the rotary drum 106 continues its rotation into drying zone, where a hot inert drying gas is introduced in the plenum 118 to dry the filter cake on the filter members 134 .
  • a hot inert drying gas is introduced in the plenum 118 to dry the filter cake on the filter members 134 .
  • the dried filter cake falls from the compartments 132 by gravity into a material passageway 120 e designated as a product chute.
  • a rinse solution may be injected through inlet 121 in order to clean the filter members of the compartments 132 before they continue into the next cycle through the zones.
  • the rotary pressure filter apparatus 100 may include multiple filtering zones and multiple wash zones.
  • the rotary pressure filter apparatus does not include a drying zone, for example, as disclosed in commonly assigned U.S. Pat Application Ser. No. 61/922,247.
  • the sealing members 122 in accordance with the present invention are designed to allow the compartments 132 to open more slowly as they enter a new zone. This is achieved by configuring the sealing members 122 to allow only a small portion, and then over time a progressively larger portion, of the compartments 132 to be exposed to the new zone as the compartments 132 rotate through the zones. Accordingly, the sealing members 122 are specifically designed to reduce pressure fluctuations as the compartments pass the sealing member into a new zone, which may each be held at different pressures. The pressure differentials between zones, for example, may be about 2 bar to 6 bar. Reduced pressure fluctuations allow fluid to enter the compartments 132 faster, thereby increasing the capacity of the rotary pressure filter apparatus 100 . Furthermore, the filter members 134 have been shown to have less movement with reduced pressure fluctuations, thereby providing the potential for a longer lifespan of the filter member 134 as well.
  • a sealing member 122 in accordance with one embodiment of the present invention is shown in FIGS. 4, 5A, 5B .
  • the sealing member 122 has a unitary body 224 , preferably made from a metal or polymer material, that extends along a length direction 226 and a width direction 228 .
  • the length direction is the same as the longitudinal direction 110 ( FIG. 1 ) of the rotary drum 106
  • the width direction is the same as the direction generally tangential to the rotary drum 106 .
  • a first side 230 ( FIGS. 5 a and 5 b ) of the sealing member 122 is generally planar.
  • a second side 232 of the sealing member 122 is spaced from the first side and connected to the first side by edges 234 , the volume between the first side and second side defining a thickness 236 of the sealing member in the radial direction of the rotary drum 106 .
  • the second side 232 is curved and concave relative to the first side 230 , and is configured to fit flush against the surface of a cylindrical drum, such as the rotary drum 106 of the rotary pressure filter apparatus 100 .
  • the sealing member 122 includes a cutout portion 240 that varies in its width along at least one portion of its length.
  • the cutout portion is tapered such that the width is narrower at one portion than at another portion of the longitudinal direction.
  • the taper has a linear edge 242 and is a single taper extending substantially the entire longitudinal direction of the sealing member.
  • the cutout portion 240 is variable in its width along its length direction only through a partial thickness 236 of the sealing member 122 , allowing more strength for the sealing member 122 around the cutout portion 240 .
  • the cutout portion 240 allows the compartments 132 to enter open to the pressure in the upstream zone more gradually because as the compartments 132 passes the sealing member 122 , the cutout portion 240 allow fluid communication with only a portion of the compartments, and that portion increases in size gradually over time as the rotary drum 106 continues to rotate. This gradual opening reduces pressure fluctuations of the material in the compartments 132 .
  • FIG. 6 illustrates an alternative embodiment of the sealing member 122 in accordance with the present invention.
  • the sealing member has multiple cutout portions 242 in a saw tooth configuration, each having a tapered edge 244 such that its width varies in its width along at least one portion of its length.
  • FIG. 7 illustrates an alternative embodiment of the sealing member 122 in accordance with the present invention.
  • the sealing member has a single cutout portions 250 having two opposing tapered edges with a generally centered apex 254 such that the cutout portion 250 varies in its width along at least one portion of its length.
  • FIG. 8 illustrates an alternative embodiment of the sealing member 122 in accordance with the present invention.
  • the sealing member 122 has multiple cutout portions 260 , each cutout portion having curved edges 262 such that each cutout portion varies in its width along at least one portion of its length.
  • each of the sealing members 122 may have a cutout portion 240 . In other embodiments, only some of the sealing members have a cutout portion. For example, in the embodiment shown in FIG. 1 , only the sealing members 122 b, 122 c entering the wash zones 124 b , 124 c have cutout portions.
  • the rotary pressure filter apparatus 100 may be used in a variety of separation processes. In some embodiments, the rotary pressure filter apparatus 100 is used to recover a solid product, or a liquid, or both, from a solid/liquid mixture. The solid is recovered from the apparatus as a filter cake that is formed on the filter members 134 . The filtrate is recovered through outlet pipes 136 . In one embodiment, the solid is a petrochemical, such as an aromatic carboxylic acid.
  • the solid product is a crude terephthalic acid product and the liquid includes a solvent containing acetic acid.
  • the crude terephthalic acid is recovered as a filter cake exiting the material passageway 120 e.
  • the solvent is recovered as filtrate exiting outlet pipes 136 .
  • the solid product is a purified terephthalic acid product and the liquid includes water.
  • the purified terephthalic acid is recovered as a filter cake exiting the material passageway 120 e.
  • the water is recovered as filtrate exiting outlet pipes 136 .

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Filtration Of Liquid (AREA)
  • Centrifugal Separators (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
US15/322,320 2014-07-25 2015-07-23 Rotary pressure filter apparatus with reduced pressure fluctuations Active 2036-09-17 US10427073B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US15/322,320 US10427073B2 (en) 2014-07-25 2015-07-23 Rotary pressure filter apparatus with reduced pressure fluctuations

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201462029065P 2014-07-25 2014-07-25
US15/322,320 US10427073B2 (en) 2014-07-25 2015-07-23 Rotary pressure filter apparatus with reduced pressure fluctuations
PCT/US2015/041793 WO2016014830A1 (en) 2014-07-25 2015-07-23 Rotary pressure filter apparatus with reduced pressure fluctuations

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US20180207558A1 US20180207558A1 (en) 2018-07-26
US10427073B2 true US10427073B2 (en) 2019-10-01

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US (1) US10427073B2 (enExample)
EP (1) EP3188817B1 (enExample)
JP (1) JP6691102B2 (enExample)
KR (1) KR102506343B1 (enExample)
CN (1) CN106573188B (enExample)
BR (1) BR112017001383A2 (enExample)
CA (1) CA2954196A1 (enExample)
MX (1) MX2017001043A (enExample)
RU (1) RU2691046C2 (enExample)
WO (1) WO2016014830A1 (enExample)

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US10857490B2 (en) * 2014-08-11 2020-12-08 Bp Corporation North America Inc. Separation process having improved capacity
US20210252436A1 (en) * 2018-06-21 2021-08-19 Valmet Ab Vacuum filter
US11202979B2 (en) * 2017-06-20 2021-12-21 Tianhua Institute of Chemical Machinery and Automation Co., Ltd Device for reducing pressure fluctuation of pressure filter frame and pressure filter

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JP2017502966A (ja) 2013-12-31 2017-01-26 ビーピー・コーポレーション・ノース・アメリカ・インコーポレーテッド 非乾燥ロータリープレッシャーフィルターを用いる固液分離
GB201703029D0 (en) * 2017-02-24 2017-04-12 Invista Tech Sarl Rotary pressure filter
CN108619776A (zh) * 2017-03-22 2018-10-09 天华化工机械及自动化研究设计院有限公司 一种隔离单元及旋转压力过滤机
TW201842956A (zh) 2017-04-28 2018-12-16 美商Ｂｐ公司北美股份有限公司 使用加壓濕氣線路以避免於經純化的對苯二甲酸(pta)過濾器及線路的積垢
US10843995B2 (en) 2017-06-29 2020-11-24 Bp Corporation North America Inc. Processes for manufacturing aromatic carboxylic acids
WO2019019012A1 (en) * 2017-07-25 2019-01-31 Bp Corporation North America Inc. DELIVERY OF A FILTER RINSE PRODUCT OF A PURIFIED AROMATIC CARBOXYLIC ACID FOR ENERGY OPTIMIZATION
PT3578242T (pt) * 2018-06-05 2021-09-28 Andritz Kmpt Gmbh Dispositivo de filtração por vácuo e/ou por pressão para filtrar uma suspensão
ES2893449T3 (es) * 2018-06-05 2022-02-09 ANDRITZ Separation GmbH La invención se refiere a un tambor de filtro para un dispositivo de filtración a vacío y/o a presión
CN112334210A (zh) 2018-06-29 2021-02-05 Bp北美公司 使用大孔滤器的固-液分离方法
CN112930224A (zh) * 2018-10-31 2021-06-08 Bhs桑托芬有限公司 用于减小压力波动的设备
WO2020102639A1 (en) 2018-11-16 2020-05-22 Bp Corporation North America Inc. Process for manufacturing aromatic carboxylic acids
CN110183457A (zh) * 2019-06-27 2019-08-30 浙江天顺药业有限公司 一种阿塞那平及其制备方法
JP2022554096A (ja) * 2019-10-31 2022-12-28 ベーハーエス－ゾントホーフェン ゲーエムベーハー 回転式圧力フィルタ
PL4051658T3 (pl) 2019-10-31 2025-02-03 Ineos Us Chemicals Company Procesy rozdzielania substancji stałej/cieczy
JP7540144B2 (ja) * 2019-11-11 2024-08-27 中国電力株式会社 ストレーナ
US20220355225A1 (en) * 2021-05-10 2022-11-10 Lyco Manufacturing Inc. Externally Fed Screen for Filtration

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10857490B2 (en) * 2014-08-11 2020-12-08 Bp Corporation North America Inc. Separation process having improved capacity
US11202979B2 (en) * 2017-06-20 2021-12-21 Tianhua Institute of Chemical Machinery and Automation Co., Ltd Device for reducing pressure fluctuation of pressure filter frame and pressure filter
US20210252436A1 (en) * 2018-06-21 2021-08-19 Valmet Ab Vacuum filter
US11980837B2 (en) * 2018-06-21 2024-05-14 Valmet Ab Rotary drum vacuum filter with a throttling valve

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RU2017105410A3 (enExample) 2019-01-24
CN106573188A (zh) 2017-04-19
EP3188817A1 (en) 2017-07-12
JP2017529226A (ja) 2017-10-05
BR112017001383A2 (pt) 2018-06-05
MX2017001043A (es) 2017-05-09
KR102506343B1 (ko) 2023-03-03
EP3188817B1 (en) 2021-04-28
CN106573188B (zh) 2019-06-14
CA2954196A1 (en) 2016-01-28
WO2016014830A1 (en) 2016-01-28
RU2017105410A (ru) 2018-08-27
JP6691102B2 (ja) 2020-04-28
RU2691046C2 (ru) 2019-06-07
US20180207558A1 (en) 2018-07-26
KR20170028444A (ko) 2017-03-13

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