UA98372C2 - Способ получения трифтористого титана - Google Patents

Способ получения трифтористого титана

Info

Publication number
UA98372C2
UA98372C2 UAA201010137A UAA201010137A UA98372C2 UA 98372 C2 UA98372 C2 UA 98372C2 UA A201010137 A UAA201010137 A UA A201010137A UA A201010137 A UAA201010137 A UA A201010137A UA 98372 C2 UA98372 C2 UA 98372C2
Authority
UA
Ukraine
Prior art keywords
titanium
transition metal
titanium trifluoride
precipitate
solution
Prior art date
Application number
UAA201010137A
Other languages
English (en)
Ukrainian (uk)
Inventor
Герард Преториус
Original Assignee
Перуке (Пропрайетари) Лимитед
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Перуке (Пропрайетари) Лимитед filed Critical Перуке (Пропрайетари) Лимитед
Publication of UA98372C2 publication Critical patent/UA98372C2/ru

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00Compounds of titanium
    • C01G23/02Halides of titanium
    • C01G23/028Titanium fluoride
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1204Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 preliminary treatment of ores or scrap to eliminate non- titanium constituents, e.g. iron, without attacking the titanium constituent
    • C22B34/1213Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 preliminary treatment of ores or scrap to eliminate non- titanium constituents, e.g. iron, without attacking the titanium constituent by wet processes, e.g. using leaching methods or flotation techniques
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1236Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching
    • C22B34/124Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching using acidic solutions or liquors
    • C22B34/1245Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching using acidic solutions or liquors containing a halogen ion as active agent
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1236Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching
    • C22B34/1259Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining titanium or titanium compounds from ores or scrap by wet processes, e.g. by leaching treatment or purification of titanium containing solutions or liquors or slurries
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1263Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
    • C22B34/1268Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
    • C22B34/1272Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/129Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds by dissociation, e.g. thermic dissociation of titanium tetraiodide, or by electrolysis or with the use of an electric arc
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Catalysts (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)

Abstract

Способ получения трифтористого титана из материала, содержащего титан, включает стадии получения фтористого раствора Ti (IV) из материала, содержащего титан, и восстановление Ti (IV) в растворе переходным металлом или сплавом переходного металла. Переходный металл выбран из марганца, железа, кобальта, никеля и цинка, при этом соль, содержащую аммоний, и аммиак или фторид аммония, добавляют в полученный раствор, содержащий Ti (III), для получения осадка, после чего данный осадок пиролизуют для получения трифтористого титана.
UAA201010137A 2008-01-14 2008-12-29 Способ получения трифтористого титана UA98372C2 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ZA200800404 2008-01-14
PCT/IB2008/055559 WO2009090513A1 (en) 2008-01-14 2008-12-29 The production of titanium trifluoride

Publications (1)

Publication Number Publication Date
UA98372C2 true UA98372C2 (ru) 2012-05-10

Family

ID=40673692

Family Applications (1)

Application Number Title Priority Date Filing Date
UAA201010137A UA98372C2 (ru) 2008-01-14 2008-12-29 Способ получения трифтористого титана

Country Status (22)

Country Link
US (1) US20100278685A1 (ru)
EP (1) EP2244980B1 (ru)
JP (1) JP5370692B2 (ru)
KR (1) KR20100125237A (ru)
CN (1) CN101918319B (ru)
AR (1) AR070155A1 (ru)
AT (1) ATE526289T1 (ru)
AU (1) AU2008348005B2 (ru)
BR (1) BRPI0822138A2 (ru)
CA (1) CA2712116C (ru)
CL (1) CL2009000046A1 (ru)
EA (1) EA017080B1 (ru)
EG (1) EG26459A (ru)
ES (1) ES2375236T3 (ru)
MX (1) MX2010007653A (ru)
MY (1) MY147802A (ru)
NZ (1) NZ586672A (ru)
PL (1) PL2244980T3 (ru)
PT (1) PT2244980E (ru)
UA (1) UA98372C2 (ru)
WO (1) WO2009090513A1 (ru)
ZA (1) ZA201005616B (ru)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101245323B1 (ko) * 2010-12-28 2013-03-19 재단법인 포항산업과학연구원 망간단괴로부터의 유가금속 침출방법
CN102153128A (zh) * 2011-05-26 2011-08-17 中国地质科学院矿产综合利用研究所 一种制备氟化钪的方法
CN102616836B (zh) * 2012-03-31 2014-07-02 攀枝花东方钛业有限公司 三价钛溶液的制备方法
RU2717418C1 (ru) * 2019-10-04 2020-03-23 Федеральное государственное бюджетное учреждение науки Институт химии Дальневосточного отделения Российской академии наук (ИХ ДВО РАН) Способ переработки титансодержащего минерального сырья
CN110817947B (zh) * 2019-11-15 2020-11-20 北京理工大学 一种低温离子液体中制备三氯化钛粉体的装置及方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1985000160A1 (en) * 1983-06-27 1985-01-17 Occidental Research Corporation Process for making titanium metal from titanium ore
JPH01252531A (ja) * 1987-12-04 1989-10-09 Nkk Corp フッ化チタンの製造方法
US4917872A (en) * 1987-12-04 1990-04-17 Nkk Corporation Method for producing titanium fluoride
JPH062917B2 (ja) * 1988-05-18 1994-01-12 日本鋼管株式会社 金属チタンの製造方法
NZ231769A (en) * 1988-12-20 1991-01-29 Univ Melbourne Production of tif 4 from ore containing tio 2
JPH06505306A (ja) * 1991-02-21 1994-06-16 ザ・ユニバーシティー・オブ・メルボルン 金属チタンならびにチタン鉄鉱および関連鉱物を処理する際に有用な中間体の製造方法
JP4257467B2 (ja) * 1999-03-18 2009-04-22 住友金属工業株式会社 チタンの回収方法
JP3800122B2 (ja) * 2002-04-04 2006-07-26 住友金属工業株式会社 チタンのフッ化物イオンを含む水溶液中の不純物金属イオンの除去方法
CN100507032C (zh) * 2005-01-27 2009-07-01 派鲁克(私人)有限公司 制备钛的方法
CN101016167A (zh) * 2006-02-09 2007-08-15 朱作远 预热氯气低温氯化法高纯TiCl4生产技术

Also Published As

Publication number Publication date
BRPI0822138A2 (pt) 2015-06-23
JP2011509905A (ja) 2011-03-31
PT2244980E (pt) 2011-12-21
CL2009000046A1 (es) 2009-12-18
ES2375236T3 (es) 2012-02-28
CN101918319A (zh) 2010-12-15
CA2712116A1 (en) 2009-07-23
AU2008348005A1 (en) 2009-07-23
ATE526289T1 (de) 2011-10-15
EP2244980A1 (en) 2010-11-03
US20100278685A1 (en) 2010-11-04
ZA201005616B (en) 2011-04-28
MX2010007653A (es) 2011-02-23
JP5370692B2 (ja) 2013-12-18
PL2244980T3 (pl) 2012-02-29
EA201001160A1 (ru) 2011-02-28
KR20100125237A (ko) 2010-11-30
NZ586672A (en) 2011-06-30
MY147802A (en) 2013-01-31
WO2009090513A1 (en) 2009-07-23
EG26459A (en) 2013-11-13
EA017080B1 (ru) 2012-09-28
CN101918319B (zh) 2013-01-09
AU2008348005B2 (en) 2012-11-01
CA2712116C (en) 2013-06-25
EP2244980B1 (en) 2011-09-28
AR070155A1 (es) 2010-03-17

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