TR201904063T4 - C4 diasitlerin amonyum tuzlarının fermantasyon ile hazırlanması yöntemleri ve bunların C4 türevlerinin hazırlanmasına yönelik entegre yöntemler. - Google Patents

C4 diasitlerin amonyum tuzlarının fermantasyon ile hazırlanması yöntemleri ve bunların C4 türevlerinin hazırlanmasına yönelik entegre yöntemler. Download PDF

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Publication number
TR201904063T4
TR201904063T4 TR2019/04063T TR201904063T TR201904063T4 TR 201904063 T4 TR201904063 T4 TR 201904063T4 TR 2019/04063 T TR2019/04063 T TR 2019/04063T TR 201904063 T TR201904063 T TR 201904063T TR 201904063 T4 TR201904063 T4 TR 201904063T4
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TR
Turkey
Prior art keywords
salts
diacids
divalent metal
methods
ammonium
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TR2019/04063T
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English (en)
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Ma Chi-Cheng
Werpy Todd
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Archer Daniels Midland Co
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Publication of TR201904063T4 publication Critical patent/TR201904063T4/tr

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D207/00—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom
    • C07D207/02—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D207/18—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
    • C07D207/22—Heterocyclic compounds containing five-membered rings not condensed with other rings, with one nitrogen atom as the only ring hetero atom with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D207/24—Oxygen or sulfur atoms
    • C07D207/26—2-Pyrrolidones
    • C07D207/263—2-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms
    • C07D207/267—2-Pyrrolidones with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to other ring carbon atoms with only hydrogen atoms or radicals containing only hydrogen and carbon atoms directly attached to the ring nitrogen atom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • C07C51/493—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification whereby carboxylic acid esters are formed
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/147—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof
    • C07C29/149—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/41—Preparation of salts of carboxylic acids
    • C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/26—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member
    • C07D307/30—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D307/32—Oxygen atoms
    • C07D307/33—Oxygen atoms in position 2, the oxygen atom being in its keto or unsubstituted enol form
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P7/00—Preparation of oxygen-containing organic compounds
    • C12P7/40—Preparation of oxygen-containing organic compounds containing a carboxyl group including Peroxycarboxylic acids
    • C12P7/44—Polycarboxylic acids
    • C12P7/46—Dicarboxylic acids having four or less carbon atoms, e.g. fumaric acid, maleic acid

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Biotechnology (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

İki değerli metal karbonat tuzlarının çıkarılmasıyla fermantasyon işleminde C4 diasitlerinin amonyum tuzlarının oluşturulmasıyla ilgili yöntemler açıklanmaktadır. C4 diasitlerinin üretimi için fermantasyon sularının pH değeri kalsiyum veya magnezyum bileşiklerini içeren alkalin oksijenin eklenmesiyle kontrol edilmektedir; bu diasitlerin iki değerli metal tuzlarını oluşturmaktadır. Diasitlere ait iki değerli metal tuzları çözünebilir amonyum tuzlarını oluşturan arttırılmış sıcaklıkta ve basınçta amonyum tuzlarının sokulmasıyla amonyumla değiştirilmektedir. C02 veya bikarbonat eş zamanlı olarak arttırılmış sıcaklıkta ve basınçta fermantasyon aracına eklenmektedir. Sıcaklığın ve basıncın azaltılması çözünebilir amonyum diasit tuzlarından ayrılan çözünmeyen iki değerli metal karbonat tuzlarını oluşturmaktadır. İyileştirilen karbonat tuzları ardışık fermantasyonlarda pH kontrol malzemeleri olarak geri dönüştürülebilmektedir. Çözünebilir amonyum diasit tuzları tek pota reaksiyonlarında N-metil-2-pirrolidon (NMP) gama-butirolakton (GBL) ve 1,4-butan-diol (BDO) türevlerinden oluşabilmektedir.
TR2019/04063T 2011-07-21 2012-07-09 C4 diasitlerin amonyum tuzlarının fermantasyon ile hazırlanması yöntemleri ve bunların C4 türevlerinin hazırlanmasına yönelik entegre yöntemler. TR201904063T4 (tr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201161510204P 2011-07-21 2011-07-21
US201161510209P 2011-07-21 2011-07-21

Publications (1)

Publication Number Publication Date
TR201904063T4 true TR201904063T4 (tr) 2019-04-22

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ID=47558393

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TR2019/04063T TR201904063T4 (tr) 2011-07-21 2012-07-09 C4 diasitlerin amonyum tuzlarının fermantasyon ile hazırlanması yöntemleri ve bunların C4 türevlerinin hazırlanmasına yönelik entegre yöntemler.

Country Status (8)

Country Link
US (3) US20140127767A1 (tr)
EP (2) EP2734629A4 (tr)
CN (2) CN103797003B (tr)
BR (2) BR112014001342A2 (tr)
ES (1) ES2717873T3 (tr)
MX (2) MX360202B (tr)
TR (1) TR201904063T4 (tr)
WO (2) WO2013012589A1 (tr)

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* Cited by examiner, † Cited by third party
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CN108138174A (zh) * 2015-10-28 2018-06-08 花王株式会社 C4二羧酸的制造方法

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US20170029353A1 (en) 2017-02-02
CN103797003A (zh) 2014-05-14
BR112014001342A2 (pt) 2017-10-03
CN103827308B (zh) 2016-08-24
US20140162326A1 (en) 2014-06-12
CN103797003B (zh) 2016-10-26
BR112014001382B1 (pt) 2020-11-10
BR112014001382A2 (pt) 2017-04-25
EP2734629A1 (en) 2014-05-28
CN103827308A (zh) 2014-05-28
EP2734509B1 (en) 2018-12-26
MX2014000838A (es) 2015-04-08
WO2013012589A1 (en) 2013-01-24
US20140127767A1 (en) 2014-05-08
WO2013012590A1 (en) 2013-01-24
ES2717873T3 (es) 2019-06-26
EP2734629A4 (en) 2015-02-25
MX360202B (es) 2018-10-25
MX2014000839A (es) 2014-09-22
EP2734509A1 (en) 2014-05-28
EP2734509A4 (en) 2015-03-04

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