TR201810157T4 - 3-iyotpropargilbütilkarbamat (ıpbc) ve n-oktilizotiyazolinon (noıt) içeren antifungal sıvı formülasyonlar. - Google Patents
3-iyotpropargilbütilkarbamat (ıpbc) ve n-oktilizotiyazolinon (noıt) içeren antifungal sıvı formülasyonlar. Download PDFInfo
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- TR201810157T4 TR201810157T4 TR2018/10157T TR201810157T TR201810157T4 TR 201810157 T4 TR201810157 T4 TR 201810157T4 TR 2018/10157 T TR2018/10157 T TR 2018/10157T TR 201810157 T TR201810157 T TR 201810157T TR 201810157 T4 TR201810157 T4 TR 201810157T4
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/80—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
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Abstract
Sıvı formülasyon, en azından, 3-iyodopropargil bütil karbamat (IPBC), n-oktilizotiyazolinon (NOIT) ve standart basınca dayalı olarak >= 250[derece] C olan bir kaynama noktasını sergileyen ve eter, ester veya amid veya alkol gruplarını ihtiva eden en az iki fonksiyonel grubu içeren bir solvent (A) ihtiva eder, burada, formülasyon, esas olarak, 250[derece] C'den daha düşük bir kaynama noktasını sergileyen bir solventten (B) aridir. Bağımsız istemler, aşağıdakilere yönelik olarak içerilir: (1) formülasyon ile, teknik malzemenin muamele görmesi vasıtasıyla elde edilen bir teknik malzeme ve (2) teknik malzemenin, dilütüe edilmiş veya dilütüe edilmemiş formülasyonun, mikro organizmaya veya bunun ortamına temasını ihtiva eden şekilde, mikroorganizma tarafından istilasına ve/veya yıkımına karşı korunması.
Description
TARIFNAME
3-IYOTPROPARGILBÜTILKARBAMAT (IPBC) VE N-OKTILIZOTIYAZOLINON
(NOIT) IÇEREN ANTIFUNGAL sivi FORMÜLASYONLAR
Mevcut bulus, 3-iyotpr0pargilbütilkarbamat (IPBC) ve n-oktilizotiyazolinon (NOIT)
içeren malzeme korumasina yönelik, stabil, antifungal sivi formülasyonlar ile ilgilidir.
2053807, Klebsiella pneumoniae'nin büyümesinin, özellikle açik sogutma sistemlerinde
ve ayni zamanda kagit üretimi esnasinda kontrol edilmesine yönelik olarak, IPBC ve
NOIT`ten olusan sinerjik karisimlari açiklar.
JP 06016506'dan, ahsap, kagit, tekstil, yapistirici madde ve boyalarin küf tarafindan
istila edilmesine karsi uygun olan, lPBC ve NOIT içeren, ksilol ve ayni zamanda su
içerikli ajanlar bilinir.
içeren stabil ajanlari açiklar.
ayrica, ayni zamanda lPBC de içerebilen sinerjik karisimlar bilinir.
Yukarida belirtilen karisimlarin ve ajanlarin dezavantaji, bunlarin VOC'den ari
olmamasi ve/veya depolama stabilitesinin eksikligine sahip olmasidir.
WO 03/049543“de, VOCiden ari veya azaltilmis, stabil sivi formülasyonlar açiklanir,
bunlar, IPBC etken maddesini, polietilenglikol, polipropilenglikol veya
polipropilenglikolgliserinesteri içinde çözünmüs sekilde içerirler.
Esasen, NOIT ve IPBC içeren sekilde VOC'den ari formülasyonlar, IPBC'nin, isi veya
isik mevcudiyetinde parçalanmasi nedeniyle, genel olarak stabilize edilmesi zordur.
Bunun sonucu olarak, bu tür formülasyonlar renk degistirir ve dolayisiyla, çogu
uygulamalara yönelik olarak bir daha uygun degildir.
VOC”den ari formülasyonlari elde etmeye yönelik bir olanak, etken maddeyi, aköz
dispersiyonlar seklinde, ek solventler olmadan formüle etmekte yatar. IPBC ve NOIT,
her durumda, stabil dispersiyonlar veya emülsiyonlar içinde formüle edilmeye izin
vermelerinden dolayi, her iki etken maddeyi içeren stabil dispersiyonlar elde edilemez.
Her iki etken maddenin mevcudiyetinde, güçlü bir heteroflokülasyon meydana gelir, bu
da sonuç olarak, kisa süre akabinde aglomeratlarin olusmasini ve formülasyonun
kuvvetli sekilde tortulasmasini veya NOIT'in yag çikarmasini içerir.
Esasen, VOC'dan ari, stabil NOIT ve IPBC sivi formülasyonlari, mevcut duruma kadar
bilinir degildir.
Bu nedenle, esasen VOC'dan ari sekilde, stabil NOIT ve IPBC sivi formülasyonlarinin
hazirlanmasi ihtiyaci mevcut olmustur.
Mevcut durumda, en azindan
. 3-IyotpropargiIbütilkarbamat (IPBC)
o N-oktilizotiyazolinon (NOlT) içeren sivi ajanlar bulunmustur
0 bir solvent, standart basinca ( göre, 250°C veya daha fazla bir
kaynama noktasina sahiptir ve eter, ester veya amid veya alkol gruplarindan
seçilen en az iki fonksiyonel gruplari içerir,
. solvent, polietilenglikol, polipropilenglikol, dialkiladipat, dialkilsüksinat ve
dialkilglutarat ve ayni zamanda yukarida belirtilen solventlerin ve
. standart basinca göre, 250°C'den daha düsük bir kaynama noktasina,
agirlikça %0 ila 3 olarak solventlerin agirlik oranina sahip olan sivi
ajanlarin karisimlari gruplarindan seçilir
Bu noktada, bulus çerçevesinin, yukarida bulunan ve asagida kaydedilen, bütün istege
bagli ve olasi kombinasyonlari, genel olarak veya tercih alanlarinda belirtilen
bilesenleri, deger araliklarini veya yöntem parametrelerini içerdigine dikkat edilmelidir.
bulunmasi ve kati bilesenleri içeriginin agirlikça %0 ila 1, tercihen agirlikça %0 ila 0,5
olmasi demektir. Özellikle tercihen, sivi ajanlar, kati bilesenlerden aridir.
Esasen, standart basinca göre, kaynama noktasi 250°C'den daha düsük olan
solventlerden ari olmasi, formülasyon içindeki bu tür solventlerin agirlik oraninin,
agirlikça %0 ila 3, tercihen agirlikça %0 ila 1 ve özellikle tercihen agirlikça %0 ile 0,5
olmasi demektir.
Örnegin, bulusa göre sivi ajanlar, IPBC ve NOIT`i, 90:1 ila 1:90, tercihen &2 ila 2:8 ve
tamamen özellikle tercihen 7:3 ila 3:7'Iik bir agirlik oraninda içerir.
Bulusa göre sivi ajanlar içinde, IPBC ve NOIT etken madde içeriginin toplami, genis bir
aralikta çesitlilik gösterebilir ve yukariya dogru, sadece, seçilen solvent içindeki etken
maddenin maksimum çözünürlügü tarafindan sinirlandirilir. Genel olarak, formülasyon
içinde, örnegin, kendi agirlik oraninin toplamina göre, agirlikça %2 ila 90, tercihen
agirlikça %5 ila 85, tamamen özellikle tercihen agirlikça %30 ila 80 ve daha da tercihen
agirlikça %50 ila 60 IPBC ve NOIT içerilebilir.
Bulusa göre sivi ajanlar, standart basinca ( göre, 250°C veya daha fazla
bir kaynama noktasina sahip olan ve eter, ester veya amid veya alkol gruplarindan
seçilen en az iki fonksiyonel gruplari içeren, en az bir solvent içerir.
Bu tür solventler, polietilenglikol, polipropilenglikol, dialkiladipat, dialkilsüksinat ve
dialkilglutarat gruplarindan seçilir.
Özellikle tercihli solventler, polietilenglikol ve ayni zamanda dialkiladipat, dialkilsüksinat
ve dialkilglutarat ve de yukarida belirtilen solventlerin karisimlaridir.
Polietilen glikoller, tercihen, en az 3 etilen glikol birimlerine sahip türde olanlardir.
Tercihli polietilen glikoller, 3 ila 14, tercihen 3 ila 12 ve özellikle tercihen 3 ila 10
polietilenglikol birimlerine sahiptir. Tamamen özellikle tercihli olanlar, trietilen glikol,
tetraetilen glikol, polietilenglikol 200, polietilenglikol 300, polietilenglikol 400,
polietilenglikol 500 ve polietilenglikol 600'dür. Bu kapsamda, bu, saf bilesikler veya
bunlarin karisimlari olabilir, belirtilen polietilen glikoller ve bunlarin karisimlari, ticari
olarak piyasadan temin edilebilir.
Dialkilglutaratlar, -süksinatlar ve -adipatlar, örnegin, bagimsiz olarak, tercihen bununla
birlikte karisim seklinde, teknik olarak üretim prosesinde ortaya çiktigi gibi,
kullanilabilir. Tercihen, alkil radikalinin düz zincirli veya dallanmis sekilde oldugu ve üç
ve on arasinda karbon atomlarina sahip oldugu türden esterler kullanilir. Bu, özellikle
tercihen, propiI-, n-bütil-, izobütil, s-bütil, n-pentil, n-heksil, n-heptil, n-oktil, 2-etilheksil
diester veya bunlarin karisimlari, tamamen özellikle tercihen diizobütildiester
karisimlaridir.
Bu tür solventlerin miktari, genis bir aralikta çesitlilik gösterebilir. Genel olarak,
formülasyonlarda, agirlikça %5 ila 90, tercihen agirlikça %5 ila 48 ve tamamen özellikle
tercihen agirlikça %40 ila 48 solvent kullanilir.
Bulusa göre ajanlar, buna ek olarak, gerekli durumlarda, en az bir emülgatör içerebilir.
Uygun emülgatörler, örnegin iyonik olmayan ve anyonik emülgatörlerdir.
Örneksel olarak, uygun emülgatörler olarak sunlar belirtilebilir: Polioksietilen- veya
polioksipropilen yag asidi esteri, polioksietilen- veya polioksipropilen yag alkolü eteri,
alkilfeniletoksilatlar veya -propoksilatlar trizarilfeniletoksilatlar veya -propoksilatlar,
polivinilpirolidonlar, poliakrilatlar, alkilpoliglikozitler, fetaminetoksilatlar, yag asidi amid
etoksilatlar, alkilpolialkilenglikol karisim polimerizatlari, polioksipropilen ve gerekli
durumlarda alkoller, alkilfenil gruplari veya trizarilfenil radikallari ile eterlenen veya yag
asitleri ile esterlenen polioksietilen birimlerinden blok kopolimerleri veya yukarida
belirtilen tiplerde, ek olarak sülfonat veya fosfat kalintilari ve de ayrica alkil sülfonatlar,
alkil sülfatlar, aril sülfonatlar tasiyan tensidler.
Tercihen, emülgatörler, iyonojen olmayan, polioksietilen yag asidi esteri, polioksietilen
yag alkolü eteri, alkilfeniletoksilatlar, trizarilfeniletoksilatlar, polivinilpirolidonlar,
poliakrilatlar, gerekli durumlarda alkoller, alkilfenil gruplari veya trizarilfenil radikalleri ile
eterlenen veya yag asitleri ile esterlenen polioksipropilen ve polioksietilen birimlerinden
olusan blok kopolimerler veya yukarida belirtilen emülgatörlerden olusan karisimlar gibi
emülgatörlerdir.
Bulusa göre sivi ajanlar, tercihen, agirlikça %0.001 ila 10, tercihen agirlikça %1 ila 8 ve
tamamen özellikle tercihen agirlikça %1 ila 6 emülgatör içerir.
Bulusa göre sivi ajanlar, gerekli durumlarda, ayni zamanda, örnegin fungisitler,
bakterisitler, algisitler ve/veya insektisitler gibi diger etken maddeleri de içerebilir.
Gerekli durumlarda ek olarak içerilen fungisitler, bakterisitler, algisitler ve/veya
insektisitler olarak, örnegin asagidakiler kullanilabilir:
Azakonazol, azosiklotin, bitertanol, bromukonazol, siprokonazol, diklobütrazol,
difenokonazol, dinikonazol, epoksikonazol, etakonazol, fenbukonazol, fenklorazol,
fenetanil, flukvinkonazol, flusilazol, flutriafol, furkonazol, heksakonazol, imibenkonazol,
ipkonazol, izozofos, miklobütanil, metkonazol, paklobütrazol, penkonazol,
propiyokonazol, protiyokonazol, simeokonazol, (±)-cis-1-(4-kIorfeniI)-2-(1H-1,2,4-
tebukonazol, tetrakonazol, triadimefon, triadimenol, triapentenol, triflumizol, tritikonazol,
unikonazol gibi triazollar ve de bunlarin metal tuzlari ve asit eklentileri;
klotrimazol, bifonazol, klimbazol, ekonazol, fenapamil, imazalil, izokonazol,
ketokonazol, Iombazol, mikonazol, pefurazoat, prokloraz, triflumizol, tiyazolkar 1-
imidazoIiI-1-(4'-kIorofenoksi)-3,3-dimetilbütan-Z-on gibi imidazoller ve de bunlarin metal
tuzlari ve asit eklentileri;
ankimidol, butiobat, fenarimol, mepanipirin, nuarimol, piroksifur, triamirol gibi piridinler
ve pirimidinler;
benodanil, karboksim, karboksimsülfoksid, siklafluramid, fenfuram, flutanil, furkarbanil,
furmeksikloks, mebenil, mepronil, metfuroksam, metsulfovaks, nikobifen, pirokarbolid,
oksikarboksin, Shirlan, Seedvax gibi süksinat dehidrojenaz inhibitörleri;
terbinafin, naftifin, bütenafin, 3-klor0-7-(2-aza-2,7.7-trimetiI-okt-3-en-5-in gibi naftalin
türevleri;
diklorfluanid, tolilfluanid, folpet, florfolpet; Captan, Captofol gibi sülfenamidler;
karbendazim, benomil, fuberidazoller, tiyabendazol gibi benzimidazoller veya bunlarin
tuzlari;
aldimorf, dimetomorf, dodemorf, falimorf, fenpropidin, fenpropimorf, tridemorf,
trimofamid gibi morfolin türevleri ve bunlarin, örnegin p-toluensülfonikasitler ve p-
dodesilfenilsüIfonikasitler gibi arilsülfonikasit tuzlari;
2-merkapt0benzotiyazol gibi benztiyazoller;
benzo[b]tiyofen-S,S-dioksid-karbonikasitsikloheksilamid gibi bentiyofendioksidler;
2,ö-dIkloro-N-(4-trifl0rometiIbenzil)-benzamid, tekloftalam gibi benzamidler;
borikasit, borikasit esteri, boraks gibi bor bilesikleri;
benzilalkolmono-(poli)-hemif0rmal, 1,3-bis(hidroksimetil)-5,5-dimeti-Iimidazolidin-2,4-
dion (D M D M H), bisoksazolidin, n-bütanoI-hemiformal, cis 1-(3-kl0ralil)-3,5.7-triaza-1-
azonyaadamantan klorür, 1-[1,3-bis(hidroksimetiI-2,5-dioksoimidazolidin-4-iI]-1,3-
bis(hidroksimetil)üre, dazomet, dimetiloI-üre, 4,4-dimetiI-0ksazolidin, etilenglikol
hemiformal, 7-etilbisiklooksazolidin, heksa-hidro-S-triazin, heksametilentetramin, N-
hidroksimetil-N'-metiltiy0üre, metilenbis-morfolin, sodyum N-(hidroksi-metil)glisinat, N-
metilolklorasetamid, oksazolidin, paraformaldehit, taurolin, tetrahidro-1,3-oksazin, N-(2-
hidroksipropil)-amin-metan0l, tetrametiIol-asetilen-diüre (TMAD) gibi formaldehit ve
N-metilizotiyazolin-3-on, 5-kl0r-N-metilizotiyazolin-S-on, 4,5-trimetilenizotiyazolinon,
4,5-benzizotiyazolinon gibi izotiyazolinonlar;
zimtaldehit, formaldehit, glutardialdehit, ß-bromzimtaldehit, o-fitaldialdehit gibi
aldehitler;
tiyosiyanatometiltiyobenzotiyazol, metilenbistiyosiyanat gibi tiyosiyanatlar;
kuvaterner amonyum bilesikleri ve benzalkonyumklorür,
benzildimetiltetradesilamonyumklorür, benzildimetildodesila monyu mklorü r,
diklorbenziIdimetilalkilamonyumklorür, didesildimetilamonyumklorü r,
dioktildimetilamonyumklorür, N-heksadesiItrimetilamonyumklorür, 1-
heksadesilpiridinyumklorür, iminoktadin-tris(albesilat) gibi guanidinler;
diiyotmetil-p-tolilsülfon, 3-iy0t-2-propiniI-alk0l, 4-kl0rfeniI-3-iy0tpropargiI-formal, 3-brom-
3-iyot-2-propinil-n-heksilkarbamat, 3-iyot-2-propiniI-sikloheksilkarbamat, 3-iy0t-2-
propinil-fenilkarbamat gibi iyot türevleri;
tribromfenol, tetraklorfenol, 3-metil-4-kl0rfenol, 3,5-dimetiI-4-klorfenol, diklorfen, 2-
benzil-4-klorfenol, triklosan, diklosan, heksaklorofen, p-hidroksibenzoikasitmetilester, p-
hidroksibenzoikasitetilester, p-hidroksibenzoikasitpropilester, p-
hidroksibenzoikasitebutilester, p-hidroksibenzoikasitoktilester,o-fenilfenol, m-fenilfenol,
p-fenilfenol, 4-(2-tert.-bütiI-4-metiI-fenoksi)-fenol, 4-(2-izopropiI-4-metiI-fenoksi)-fen0l, 4-
(2,4-dimetiI-fenoksi)-fenol gibi fenoller ve bunlarin alkali ve toprak alkali metal tuzlari;
klor-4,4,5,5-tetrametiI-2-imidazoldinon, ß-brom-ß-nitrostiren, klorasetamid, kloramin T,
3-on, 2,2-dibrom-3-nitriI-propiyonamid, 1,2-dibrom-2,4-disiyan0bütan, halanlar,
halazonlar, mukoklorikassit, feniI-(2-klor-siyan-vinil)sülfon, feniI-(1,2-diklor-2-
siyanvinil)sülf0n, triklorizosiyanür-asit gibi aktive edilmis halojen gruplarina sahip
mikrobisitler;
1-hidroksi-Z-piridintiyon (ve bunun Cu-, Na-, Fe-, Mn-, Zn tuzlari), tetraklor-4-
metilsülfonilpiridin, pirimetanol, mepanipirim, dipiritiyon, 1-hidroksi-4-metiI-6-(2,4,4-
trimetilpentiI)-2(1H)-piridin gibi piridinler;
azoksistrobin, dimoksistrobin, floksastrobin, krezoksim-metil, metominostrobin,
orisastrobin, pikoksistrobin, piraklostrobin, trifloksistrobin, 2,4-dihidro-5-metoksi-2-metil-
(CAS-No. 185336-79-2) gibi metoksiakrilatlar veya benzerleri;
daha yüksek yag asiti, reçine asiti, naftenik asit ve fosforik asit ile kalay, bakir ve çinko
tuzlari gibi metal tuzlari gibi metal sabunlar, örnegin, kalay, bakir, çinko naftenat. -
oktoat, 2-etilheksanoat, -oleat, -fosfat, -benzoat gibi;
kalay, bakir, çinko gibi metallerin tuzlari gibi metal tuzlari ve ayni zamanda kromat ve
dikromat, örnegin bakirhidroksikarbonat, sodyumdikromat, potasyumdikromat,
potasyumkromat, bakirsülfat, bakirklorür, bakirborat, çinkoflorosilikat, bakirflorosilikat;
oksitler, örnegin: kalay, bakir ve çinko metallerinin oksitleri, örnegin tribütiltinoksit,
Cu20, CuO, ZnO gibi;
hidrojen peroksit, perasetik asit, potasyum persülfat gibi oksidasyon ajanlari;
Cufraneb, Ferban, potasyum N-hidroksimetiI-N'-metil-ditiyobarbamat, Na veya K-
dimetilditiyokarbamat, Macozeb, Maneb, Metam, Metiram, Thiram, Zineb, Ziram gibi
ditiyokarbamatlar;
2,4,5,6-tetraklorizoftalodinitril, disodyum-siyano-ditiyoimidokarbamat gibi nitriller;
kinolinler, örnegin: 8-Hidroksikinolin ve bunun Cu tuzlari;
diger fungisitler ve bakterisitler, örnegin Betoksazin, 5-hidr0ksi-2(5H)-furan0n; 4,5-
benzditiyazolinon, 4,5-trimetilenditiyazolinon, N-(2-p-kl0rbenzoiletil)-
hekzaminyumklorü r, 2-okso-2-(4-hid roksi-fenil)asetidroksimasit-klorü r, tris-N-
(sikloheksildiazenyumdioksi)-aIüminyum, N-(siklo-heksildiazenyu mdioksi)-tribütiltin
veya K-tuzlari, bis-N-(sikloheksildi-azenyumdioksi)-bakir, lprovalicarb, Fenhexamid,
Spiroxamin, Carpropamid, Diflumetorin, Quinoxyfen, Famoxadone, Polyoxorim,
asibenzolar-S-metil, furametpir, tifluzamid, metalaksiI-M, bentiyavalikarb, metrafenon,
siflufenamid, Tiadinil, çay agaci yagi, fenoksietanol gibi,
Ag, Zn veya Cu içeren zeolitler tek basina veya polimer malzemeler içinde kapsanmis
Tamamen özellikle tercihen, fungisitler ve bakterisitler sunlardir:
Azakonazol, bromukonazol, siprokonazol, diklobutrazol, dinikonazol,, heksakonazol,
metakonazol, penkonazol, propikonazol, tebukonazol, diklofluanid. tolilfluanid,
triadimefon, floifolpet. metfuroksam, karboksin, benzo[b]tiyofen-S.S-dioksit-
karboksilikasitsikloheksilamid, fenpiklonil, 4-(2,2-difl0r0-1,3-benzodioksoI-4-iI)-1H-pirol-
3-karb0nitril, butenafin, imazalil, N-metiI-izotiyazolin-3-0n, 5-kIor-N-metilizotiyazolin-3-
on, diklor-N-oktiIizotiyazolinon, merkaptobenztiyazol, tiyosiyanatometiltiyobenzotiyazol,
tiyabendazol, benzizotiyazolinon, N-(2-hidroksipr0pil)-amin0-metan0l, benzilalkol-
(hemi)-formal, N-metilolklorasetamid, N-(2-hidroksiprOpiI)-amin-metanol, glutaraldehit,
omadin, Zn-omadin, dimetildikarbonat, 2-brom-2-nitro-1,3-propandiol, betoksazin, 0-
bis(hidroksimetiI)-, tetrametiIoI-asetilen-diüre
(TMAD), etilenglikoI-hemiformal, p-hidroksibenzoikasit, karbendazim, klorofen, 3-metil-
4-klorfen0l, o-fenilfenol.
Algisitler, tercihen, asagidakilerdir:
Asetoklor, asiflorfen, aklonifen, akrolein, alaklor, alloksidim, ametrin, amidosülfüron,
amitrol, amonyum sülfamat, anilofos, asulam, atrazin, azafenidin, aziptrotrin,
azimsülfüron,
benazolin, benfluralin, benfuresat, bensülfüron, bensülfid, bentazon, benzofenkap,
benztiyazuron, bifenoks, bispiribak, bispiribak-sodyum, boraks, bromasil, bromobütid,
bromofenoksim, bromoksinil, bütaklor, bütamifos, butralin, bütilat, bialafos, benzoil-
karbetamid, karfentrazon-etil, karfenstrol, klometoksifen, kloramben, klorbromuron,
klorflurenol, klorürazon, klorimuron, klornitrofen, klorasetik asit, kloransulam-metil,
kinidon-etil, klorotoluron, kloroksuron, klorprofam, klorsülfüron, klortal, klortiyamid,
kinmetilin, kinofulsuron, klefoksidim, kletodim, klomazon, klomeprop, klopiralid,
siyanamid, siyanazin, sikloat, sikloksidim, kloroksinil, klodinafop-propargil, kumiluron,
klometoksifen, sihalofop, sihalofop-bütil, klopirasuluron, siklosülfamuron,
diklosulam, diklorprop, diklorprop-P, diklofop, dietatil, difenoksuron, difenzokuat,
diflufenikan, diflufenzopir, dimefuron, dimepiperat, dimetaklor, dimetipin, dinitramin,
dinoseb, dinoseb asetat, dinoterb, difenamid, dipropetrin, dikuat, ditiyopir, diduron,
DNOC, DSMA, 2,4-D, daimuron, dalapon, dazomet, 2,4-DB, desmedifam, dezmetrin,
dikamba, diklobenil, dimetamid, ditiyopir, dimetametrin,
eglinazin, endotal, EPTC, esprokarb, etalfluralin, etidimuron, etofumesat, etobenzanid,
etoksifen, etametsülfüron, etoksisülfüron,
fenoksaprop, fenoksaprop-P, fenuron, flamprop, flamprop-M, flazasülfüron, fluazifop,
fluazifop-P, fuenaklor, flukloralin, flufenaset flumeturon, florokglisofen, floronitrofen,
flupropanat, flurenol, fluridon, fluroklorüron, fluroksipir, fomesafen, fosamin, fosametin,
flamprop-izopropil, flamprop-izopropil-L, flufenpir, flumiklorak-pentil, flumipropin,
flumiokszim, flurtamon, flumiokszim, flupirsülfüron-metil, flutiyaset-metil,
glifosat, glufosinat amonyum
haloksifop, heksazinon,
imazametabenz, izoproturon, izoksaben, izoksapirifop, imazapir, imazakuin, imazetapir,
ioksinil, izopropalin, imazosülfüron, imazomoks, izoksaflutol, imazapik,
ketospiradoks,
MCPA, MCPA-hidrazid, MCPA-tiyoetil, MCPB, mekoprop, mekoprop-P, mefenaset,
mefluidid, mezosülfüron, metam, metamifop, metamitron, metazaklor,
metabenztiyazuron, metazol, metoroptrin. metildimron, metilizotiyosiyanat,
metobromüron, metoksuron, metribuzin, metsülfüron, molinat, monalid, monolinuron,
MSMA, metolaklor, metosulam, metobenzuron,
naproanilid, napropamid, naptalam, neburon, nikosülfüron, norflurazon, sodyumklorat,
oksadiazon, oksiflorfen, oksisülfüron, orbenkarb, orizalin, oksadiargil,
propizamid, prosülfokarb, pirazolat, pirazolsülfüron, pirazoksifen, piribenzoksim,
piributikarb, piridat, parakuat, pebulat, pendimetalin, pentaklorofenol, pentoksazon,
pentanoklor, petrol yagi, fenmedifam, fikloram, piperofos, pretilaklor, primisülfüron,
prodiamin, profoksidim, prometrin, propaklor, propanil, propakuizafob, propazin,
profam, propizoklor, piriminobak-metil, pelargonik asit, piritiyobak, piraflufen etil,
kuinmerak, kuinokloamin, kuizalofop, kuizalofop-P, kuinklorac,
rimsülfü ron
setoksidim, sifuron, simazin, simetrin, sülfosülfüron, sülfometüron, sülfentrazon,
sülkotrion, sülfosat,
Katran yagi, TCA, TCA-sodyum, tebutam, tebutiüron, terbasil, terbumeton, terbütilazin,
terbutrin, tiyazafloron, tifensülfüron, tiyobenkarb, tiyokarbazil, tralkoksidim, trialat,
triasülfüron, tribenuron, triklopir, tridifan, trietazin, trifluralin, tikor, tdiazimin, tiazopir,
triflusülfüron,
vernolat.
Tamamen özellikle tercihen, algisitler, ömegin terbutrin, sibutrin, propazin veya
terbuton gibi triazin bilesikleridir, üre bilesikleri gibi, örnegin, diuron, benztiyazuron,
metabenztiyazuron, tebutiuron ve izoproturon veya urasil, örnegin terbasil gibi.
Gerekli durumlarda, bulusa göre sivi ajanlar, oksidasyon inhibitörleri, radikal tutucular
ve UV absorbanlari sinifindan ek stabilizatörleri veya her durumda, birbirlerinden
bagimsiz olmayan sekilde içerebilir.
Tercihli bir düzenleme formunda, bulusa göre sivi ajanlar, diger bir fungisit, bakterisit,
algisit ve/veya insektisit ihtiva etmez.
Diger bir tercihli düzenleme formunda, bulusa göre sivi ajanlar hiç epoksit ihtiva etmez.
Diger bir tercihli düzenleme formunda, bulusa göre sivi ajanlar, formik asit, format
tuzlari veya format esterleri grubundan hiçbir stabilizatör ihtiva etmez.
Özellikle tercihli bir düzenleme formunda, bulusa göre sivi ajanlar, agirlikça %20 ila 35
emülgatör içerir, burada, yukarida belirtilen dört bilesenin toplami, sivi ajanin toplam
tercihen agirlikça %98 ila100 olur.
Daha tercihli diger bir düzenleme formunda, yukarida belirtilen sivi ajanlar, hiçbir diger
etken madde, hiçbir epoksit ve formik asit, format tuzlari veya format esterleri
grubundan hiçbir stabilizatör ihtiva etmez.
Bulusa göre sivi ajanlar, örnegin, kendiliginden bilinen sekilde, tekli bilesenlerin
karistirilmasi vasitasiyla üretilmeye izin verir.
Bulus, buna ek olarak, bulusa göre sivi ajanlarin, teknik malzemelerin korunmasina
yönelik olarak kullanilmasi ile ilgilidir. Teknik malzemeler olarak, özellikle yapistirici
madde, tutkal, kagit, karton, deri, ahsap, ahsap esasli malzeme, ahsap-plastik
kompozit, boyama maddesi, kaplama maddesi, temizlik, sogutma yaglari maddesi ve
isi transfer sivilari düsünülebilir. Tamamen özellikle tercihli olanlar, boyama maddesi,
kaplama maddesi, temizlik, ahsap ve ahsap esasli malzemedir.
Bulus, ayrica, teknik malzemelerin, mikroorganizmalar tarafindan istila edilmesine
ve/veya bozulmasina karsi korunmasina yönelik bir yöntem ile ilgilidir, karakteristik
özelligi, bulusa göre sivi ajanin, seyreltilmemis veya seyreltilmis sekilde,
mikroorganizmanin üzerine veya bunun yasam bölgesine nüfuz ettirilmesinin mümkün
olmasidir.
Bulus, ayrica, teknik malzemelerin, bulusa göre sivi ajanlar ile muamele görmesi
vasitasiyla elde edilebilen teknik malzemeler ile ilgilidir.
Boyalar ve kaplama kompozisyonlari durumunda, sivi olan ve ayni zamanda
kurutulmus olan sistem, mikroorganizmalar, özellikle mantarlar ve algler tarafindan
istilaya karsi korunur. Teknik malzemelerin yikimina veya degismesine neden
olabilecek mikroorganizmalar olarak, örnegin, bakteriler, mantarlar, mayalar, algler ve
sümüksü organizmalar belirtilebilir. Tercihen, bulusa göre sivi ajanlar, mantarlara,
özellikle küf mantarlarina, ahsabin rengini degistiren ve ahsabi parçalayan mantarlara
(basidiomisetler) karsi ve ayni zamanda alglere karsi kullanilir.
Örnegin, asagidaki türde mikroorganizmalar belirtilebilir:
Altemaria, örnegin Altemaria tenuis, Aspergillus, örnegin Aspergillus niger,
Chaetomium, örnegin Chaetomium globosum, Coniophora, örnegin Coniophora
puetana, Lentinus, örnegin Lentinus tigrinus, Penicillium, örnegin Penicillium glaucum,
Polyporus, örnegin Polyporus versicolor, Aureobasidium, örnegin Aureobasidium
pullulans, Sclerophoma, örnegin Sclerophoma pityophila, Trichoderma, örnegin
Trichoderma viride, Escherichia, örnegin Escherichia coli, Pseudomonas, örnegin
Pseudomonas aeruginosa ve Staphylococcus, örnegin Staphylococcus aureus.
Bulusa göre sivi ajanlarin uygulama orani, mücadele edilecek olan
mikroorganizmalarin tipine ve ortaya çikisina ve ayni zamanda korunacak olan
malzemenin bilesimine göre tasarlanir. Optimum kullanim miktari, test dizileri
vasitasiyla kolaylikla ve teknikte uzman kisilerce iyi bilinen bir sekilde belirlenebilir.
Genel olarak, bulusa göre sivi ajan, korunacak olan malzemeye göre, agirlikça %0,001
ila 5, tercihen agirlikça %0,01 ila 1,0 olarak kullanilir.
Bulusa göre sivi ajanlarin özel avantaji, bunlarin, yükseltilen sicakliklar esnasinda dahi
çok iyi depolanma stabilitesinde olmasi ve ayni zamanda, O°C'nin altindaki
sicakliklarda dahi kristalize olmamasidir. Buna ek olarak, formülasyonlarin, depolama
esnasinda sadece düsük olarak renk degistirdigi ve ayni zamanda, korunacak olan
teknik malzemeye yönelik olarak en basit sekilde nüfuz edebildigi bulunmustur. Ayrica,
bulusa göre ajanlar, formülasyonun, beklenmedik sekilde, daha yüksek IPBC ve NOIT
etken madde konsantrasyonlarina imkan verir.
Örnekler
6.7 9 Rhodiasolv DIB (glutarik, süksinik ve adipik asidin izobütil diesterlerinin bir
polioksietilen blok kopolimerizati, CAS No. 9038-95-3)lden olusan bir solusyon, IPBC
ve NOIT (agirlik orani 5:3) ile, daha fazla çözülemeyene kadar oda sicakliginda
karistirilir. Meydana gelen solusyon, ve
57,95 9 (toplam solusyona göre %49,9) IPBC ihtiva eder. Oda sicakliginda, bir hafta
içinde, hiçbir çökelme gözlenmez.
NOIT (agirlik orani 5:3) ile, oda sicakliginda, daha fazla çözünmeyene kadar karistirilir.
Meydana gelen solusyon, 25, ve 43,6 g
(toplam solusyona göre %50,0) lPBC ihtiva eder. Oda sicakliginda, bir hafta içinde,
hiçbir çökelme gözlenmez.
ile, oda sicakliginda,
daha fazla çözünmeyene kadar karistirilir. Meydana gelen solusyon, 25,8 9 NOIT
eder. Oda sicakliginda, bir hafta içinde, hiçbir çökelme gözlenmez.
Örnekler 4 ila 6
Tabloda bildirilen solusyonlar, karistirma vasitasiyla üretilir, 54°C'de 2 hafta depolanir
ve bunun akabinde analitik ve optik olarak degerlendirilir.
- \ Örnek No. 4 5 6
Rhodiasolv DIB” 13,40 - 13,40
Antarox B 500 5,0 5,0 5,0
akabinde)
- \ Örnek No. 4 5 6
akabinde)
Dis görünüs (54°Cide 2 Berrak, açik sari Berrak, açik sari Berrak, açik sari
hafta akabinde) solusyon solusyon solusyon
Dis görünüs (- 4°C'de bir Berrak, renksiz Berrak, renksiz Berrak, renksiz
hafta akabinde) solusyon solusyon solusyon
Bilesenlerin tüm verileri, agirlikça % halinde
Örnek 7 (Karsilastirmaya yönelik olarak)
Solvent, oda sicakliginda hazirlanir ve bir tortu olusuncaya kadar IPBC ilave edilir. 12
saat daha karistirilir, kati madde santrifüje edilir ve geri kalan üstteki sivi, HPLC
vasitasiyla analiz edilir. Bu baglamda, lPBClnin, Rhodiasolv DIB içinde, agirlikça
Claims (1)
- ISTEMLER Sivi ajan olup en azindan asagidakileri ihtiva eder 3-iyotpropargilbütilkarbamat (IPBC) n-oktilizotiyazolinon (NOIT) standart basinca göre, 250°C veya daha fazla bir kaynama noktasina sahip ve eter, ester veya amid veya alkol gruplarindan seçilen en az iki fonksiyonel gruplari ihtiva eden bir solvent, özelligi solventin, polietilenglikol, polipropilenglikol, dialkiladipat, dialkilsüksinat ve dialkilglutarat gruplarindan ve ayni zamanda yukarida belirtilen solventlerin karisimlarindan seçilmesi ve sivi ajanlarin, standart basinca göre, 250°C'den daha düsük bir kaynama noktasina, agirlikça %0 ila 3”e sahip solventlerin agirlik oranina sahip olmasi lPBC ve NOlT etken madde içeriginin toplaminin, agirlikça %30 ila 80 olmasidir. istem 1'e göre sivi ajan olup, özelligi, solvent içeriginin, agirlik olarak %40 ila 48 olmasi ile karakterize edilmesidir. Istemler 1 veya 2lden herhangi birine göre sivi ajan olup, özelligi, bunun, ek olarak, en az bir emülgatör içermesi ile karakterize edilmesidir. istem 3te göre sivi ajan olup, özelligi, en az bir emülgatör içeriginin, agirlik olarak, %0,001 ila 10 olmasi ile karakterize edilmesidir. Istemler 1 ila 4'ten herhangi birine göre sivi ajan olup, özelligi, bunun, ek olarak, hiçbir diger etken madde içermemesi ile karakterize edilmesidir. . istemler 1 ila 5'ten herhangi birine göre sivi ajan olup, özelligi, bunun, formik asit, format tuzlari veya format esterleri grubundan epoksitlerden hiçbirini ve stabilizatörlerden hiçbirini içermemesi ile karakterize edilmesidir. . istemler 1 ila 6'dan herhangi birine göre sivi ajan olup, özelligi, bunun, agirlikça agirlikça %1 ila 6 emülgatör içermesi ile karakterize edilmesidir, burada, yukarida belirtilen dört bilesenin toplami, sivi ajanin toplam kütlesine göre %90 ila 100 olur. . istemler 1 ila 7'den herhangi birine göre sivi ajanlarin, teknik malzemelerin korunmasina yönelik olarak kullanilmasidir. . Istem 8'e göre uygulama olup, özelligi, teknik malzemelerin yapistirici madde, tutkal, kagit, karton, deri, ahsap, ahsap esasli malzeme, ahsap-plastik kompozit, boyama maddesi, kaplama maddesi, temizlik, sogutma yaglari maddesi ve isi transfer sivilari olmasi ile karakterize edilmesidir. 10. Teknik malzemelerin, istemler 1 ila 7`den herhangi birine göre bir sivi ajan ile muamele görmesi vasitasiyla elde edilebilen teknik malzemedir. 11.Teknik malzemelerin, mikroorganizmalar tarafindan istila edilmesine ve/veya bozulmasina karsi korunmasina yönelik yöntem olup, özelligi, bulusa göre sivi ajanin, seyreltilmemis veya seyreltilmis sekilde, mikroorganizmanin üzerine veya bunun yasam bölgesine nüfuz ettirilmesinin mümkün olmasi ile karakterize edilmesidir. 12. Polietilenglikol, polipropilenglikol, dialkiladipat, dialkilsüksinat ve dialkilglutarat gruplarindan ve ayni zamanda yukarida belirtilen solventlerin karisimlarindan seçilen NOIT, IPBC ve solventlerin, istemler1 ila 7'den birine göre sivi ajanlarin üretilmesine yönelik olarak kullanilmasidir. 13. Emülgatörlerin, istemler 3 ila 7'den birine göre sivi ajanlarin üretilmesine yönelik olarak kullanilmasidir.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP08161821A EP2153722A1 (de) | 2008-08-05 | 2008-08-05 | Antifungische Flüssigformulierungen enthaltend 3-Iodpropargylbutylcarbamat (IPBC) und N-octylisothiazolinon (NOIT) |
Publications (1)
Publication Number | Publication Date |
---|---|
TR201810157T4 true TR201810157T4 (tr) | 2018-08-27 |
Family
ID=40029183
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
TR2018/10157T TR201810157T4 (tr) | 2008-08-05 | 2009-07-28 | 3-iyotpropargilbütilkarbamat (ıpbc) ve n-oktilizotiyazolinon (noıt) içeren antifungal sıvı formülasyonlar. |
Country Status (11)
Country | Link |
---|---|
US (1) | US8231721B2 (tr) |
EP (2) | EP2153722A1 (tr) |
JP (1) | JP2011529937A (tr) |
KR (1) | KR20110041560A (tr) |
AU (1) | AU2009278082A1 (tr) |
BR (1) | BRPI0916903A2 (tr) |
ES (1) | ES2676294T3 (tr) |
MX (1) | MX2011001271A (tr) |
PL (1) | PL2315523T3 (tr) |
TR (1) | TR201810157T4 (tr) |
WO (1) | WO2010015552A2 (tr) |
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JP5302368B2 (ja) * | 2010-11-04 | 2013-10-02 | ダウ グローバル テクノロジーズ エルエルシー | フルメツラムまたはジクロスラムとイソチアゾロンとの相乗的組み合わせ |
JP5529832B2 (ja) * | 2010-12-22 | 2014-06-25 | ダウ グローバル テクノロジーズ エルエルシー | Dcoitまたはoitまたはbbitの1種と、グリホサート化合物との相乗的組み合わせ |
US8901188B2 (en) | 2011-06-16 | 2014-12-02 | Kimberly-Clark Worldwide, Inc. | Antimicrobial polyurethane foam and process to make the same |
US9326518B2 (en) | 2013-03-28 | 2016-05-03 | Rohm And Haas Company | Synergistic combination of a chlorotoluron compound and OIT for dry film protection |
JP2015003863A (ja) * | 2013-06-19 | 2015-01-08 | 住化エンバイロメンタルサイエンス株式会社 | 木材用抗菌組成物 |
JP6325416B2 (ja) * | 2014-10-23 | 2018-05-16 | ケイ・アイ化成株式会社 | 工業用防腐、殺菌剤 |
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JPH0616506B2 (ja) | 1984-12-26 | 1994-03-02 | 株式会社半導体エネルギー研究所 | 積層体の側周辺に選択的に被膜を形成する方法 |
US4964892A (en) * | 1988-12-22 | 1990-10-23 | Rohm And Haas Company | Synergistic microbicidal combinations containing 2-N-octyl-3-isothiazolone and certain commercial biocides |
US5131939A (en) | 1988-12-22 | 1992-07-21 | Rohm And Haas Company | Synergistic microbicidal combinations containing 2-n-octyl-3-isothiazolone and certain commercial biocides |
US5041457A (en) | 1989-03-10 | 1991-08-20 | Rohm And Haas Company | Synergistic microbicidal combinations containing 2-n-octyl-3-isothiazolone and certain commercial biocides |
CA2053807A1 (en) * | 1991-10-15 | 1993-04-16 | Deborah K. Donofrio | Biocidal compositions and use thereof containing a synergistic mixture of 3-iodo-2-propynyl-butyl carbamate and 2-n-octyl-4-isothiazolin-3-one |
JPH0616506A (ja) * | 1992-06-30 | 1994-01-25 | Shinto Paint Co Ltd | 工業用防カビ組成物 |
JPH07133205A (ja) * | 1993-11-08 | 1995-05-23 | Shinto Paint Co Ltd | 木材用防カビ組成物 |
DE10040814A1 (de) | 2000-08-21 | 2002-03-07 | Thor Gmbh | Synergistische Biozidzusammensetzung |
JP2002265310A (ja) * | 2001-03-06 | 2002-09-18 | Nagase Chemtex Corp | 抗微生物剤組成物 |
JP4812205B2 (ja) | 2001-09-28 | 2011-11-09 | 日本エンバイロケミカルズ株式会社 | 安定化された微生物増殖抑制組成物 |
CA2469449C (en) | 2001-12-12 | 2011-03-15 | Isp Investments Inc. | Liquid compositions of ipbc in polyethylene glycol, polypropylene glycol or polypropylene glycol glyceryl esters |
JP2004315507A (ja) * | 2003-04-07 | 2004-11-11 | Rohm & Haas Co | 殺微生物組成物 |
HUE031355T2 (hu) | 2004-08-12 | 2017-07-28 | Troy Tech Ii Inc | Vízben nem oldódó aktív szerves vegyületek kompozíciói |
DE102005044855A1 (de) * | 2005-09-21 | 2007-03-29 | Clariant Produkte (Deutschland) Gmbh | Biozide Zusammensetzungen |
ZA200900482B (en) | 2006-07-25 | 2010-05-26 | Down Global Technologies Inc | Stable, low voc, low viscous biocidal formulations and methods of making such formulations |
EP2046125B1 (en) * | 2006-08-02 | 2011-12-28 | Laboratorios Miret, S.A. | Biocidal composition for leather tanning |
TW200932107A (en) * | 2008-01-18 | 2009-08-01 | Dow Global Technologies Inc | Stable, low VOC, low viscous biocidal formulations and method of making such formulations |
-
2008
- 2008-08-05 EP EP08161821A patent/EP2153722A1/de not_active Withdrawn
-
2009
- 2009-07-28 JP JP2011521532A patent/JP2011529937A/ja not_active Withdrawn
- 2009-07-28 MX MX2011001271A patent/MX2011001271A/es not_active Application Discontinuation
- 2009-07-28 BR BRPI0916903-2A patent/BRPI0916903A2/pt not_active IP Right Cessation
- 2009-07-28 PL PL09781205T patent/PL2315523T3/pl unknown
- 2009-07-28 AU AU2009278082A patent/AU2009278082A1/en not_active Abandoned
- 2009-07-28 EP EP09781205.1A patent/EP2315523B1/de active Active
- 2009-07-28 WO PCT/EP2009/059760 patent/WO2010015552A2/de active Application Filing
- 2009-07-28 TR TR2018/10157T patent/TR201810157T4/tr unknown
- 2009-07-28 KR KR1020117005202A patent/KR20110041560A/ko active IP Right Grant
- 2009-07-28 ES ES09781205.1T patent/ES2676294T3/es active Active
- 2009-07-28 US US13/057,021 patent/US8231721B2/en active Active
Also Published As
Publication number | Publication date |
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JP2011529937A (ja) | 2011-12-15 |
BRPI0916903A2 (pt) | 2015-07-28 |
AU2009278082A1 (en) | 2010-02-11 |
EP2315523B1 (de) | 2018-05-30 |
US20110139033A1 (en) | 2011-06-16 |
KR20110041560A (ko) | 2011-04-21 |
MX2011001271A (es) | 2011-03-15 |
ES2676294T3 (es) | 2018-07-18 |
PL2315523T3 (pl) | 2018-10-31 |
US8231721B2 (en) | 2012-07-31 |
EP2315523A2 (de) | 2011-05-04 |
WO2010015552A2 (de) | 2010-02-11 |
EP2153722A1 (de) | 2010-02-17 |
WO2010015552A3 (de) | 2010-04-08 |
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