SU741780A3 - Способ регенерации ванадийникельсодержащего катализатора - Google Patents
Способ регенерации ванадийникельсодержащего катализатора Download PDFInfo
- Publication number
- SU741780A3 SU741780A3 SU752182547A SU2182547A SU741780A3 SU 741780 A3 SU741780 A3 SU 741780A3 SU 752182547 A SU752182547 A SU 752182547A SU 2182547 A SU2182547 A SU 2182547A SU 741780 A3 SU741780 A3 SU 741780A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- catalyst
- vanadium
- nickel
- catalysts
- deactivated
- Prior art date
Links
- 239000003054 catalyst Substances 0.000 title abstract description 110
- 238000000034 method Methods 0.000 title abstract description 10
- HBVFXTAPOLSOPB-UHFFFAOYSA-N nickel vanadium Chemical compound [V].[Ni] HBVFXTAPOLSOPB-UHFFFAOYSA-N 0.000 title description 3
- 230000001172 regenerating effect Effects 0.000 title 1
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract description 67
- 229910052720 vanadium Inorganic materials 0.000 abstract description 51
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 abstract description 48
- 229910052759 nickel Inorganic materials 0.000 abstract description 35
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract description 12
- 239000003921 oil Substances 0.000 abstract description 12
- 230000000694 effects Effects 0.000 abstract description 10
- 239000001257 hydrogen Substances 0.000 abstract description 5
- 229910052739 hydrogen Inorganic materials 0.000 abstract description 5
- 239000004215 Carbon black (E152) Substances 0.000 abstract description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract description 4
- 239000007864 aqueous solution Substances 0.000 abstract description 4
- 229930195733 hydrocarbon Natural products 0.000 abstract description 4
- 150000002430 hydrocarbons Chemical class 0.000 abstract description 4
- 229910052750 molybdenum Inorganic materials 0.000 abstract description 4
- 238000011084 recovery Methods 0.000 abstract description 4
- 239000000377 silicon dioxide Substances 0.000 abstract description 4
- 239000000243 solution Substances 0.000 abstract description 4
- 229910052751 metal Inorganic materials 0.000 abstract description 3
- 239000002184 metal Substances 0.000 abstract description 3
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical class O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 2
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 2
- 239000011707 mineral Substances 0.000 abstract 2
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 150000002431 hydrogen Chemical class 0.000 abstract 1
- 150000002739 metals Chemical class 0.000 abstract 1
- 229910052721 tungsten Inorganic materials 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 38
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 22
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 15
- 238000000605 extraction Methods 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 229920006395 saturated elastomer Polymers 0.000 description 7
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 5
- 229910052717 sulfur Inorganic materials 0.000 description 5
- 239000011593 sulfur Substances 0.000 description 5
- 238000001035 drying Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 230000008929 regeneration Effects 0.000 description 4
- 238000011069 regeneration method Methods 0.000 description 4
- 229910052814 silicon oxide Inorganic materials 0.000 description 4
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
- 238000001354 calcination Methods 0.000 description 3
- 239000010779 crude oil Substances 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000011733 molybdenum Substances 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 239000010703 silicon Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 239000000446 fuel Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- KBJMLQFLOWQJNF-UHFFFAOYSA-N nickel(ii) nitrate Chemical compound [Ni+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O KBJMLQFLOWQJNF-UHFFFAOYSA-N 0.000 description 2
- 125000000101 thioether group Chemical group 0.000 description 2
- 150000003568 thioethers Chemical group 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 101100492805 Caenorhabditis elegans atm-1 gene Proteins 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 1
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 1
- LXASOGUHMSNFCR-UHFFFAOYSA-D [V+5].[V+5].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O Chemical compound [V+5].[V+5].[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O.[O-]C(=O)C([O-])=O LXASOGUHMSNFCR-UHFFFAOYSA-D 0.000 description 1
- 238000005266 casting Methods 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000005504 petroleum refining Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- -1 vanadyl nickel oxalate nitrate Chemical compound 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/90—Regeneration or reactivation
- B01J23/92—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/20—Obtaining niobium, tantalum or vanadium
- C22B34/22—Obtaining vanadium
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Catalysts (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB44604/74A GB1526927A (en) | 1974-10-15 | 1974-10-15 | Process for recovering vanadium from deactivated catalyst |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU741780A3 true SU741780A3 (ru) | 1980-06-15 |
Family
ID=10434046
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU752182547A SU741780A3 (ru) | 1974-10-15 | 1975-10-13 | Способ регенерации ванадийникельсодержащего катализатора |
Country Status (15)
| Country | Link |
|---|---|
| JP (1) | JPS6012908B2 (enExample) |
| AR (1) | AR224854A1 (enExample) |
| AU (1) | AU498495B2 (enExample) |
| BE (1) | BE834257A (enExample) |
| CA (1) | CA1071413A (enExample) |
| DE (1) | DE2545787A1 (enExample) |
| FR (1) | FR2288154A1 (enExample) |
| GB (1) | GB1526927A (enExample) |
| IT (1) | IT1043322B (enExample) |
| MX (1) | MX3049E (enExample) |
| NL (1) | NL186587C (enExample) |
| NO (1) | NO143521C (enExample) |
| SE (1) | SE410474B (enExample) |
| SU (1) | SU741780A3 (enExample) |
| ZA (1) | ZA756443B (enExample) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL7703181A (nl) * | 1977-03-24 | 1978-09-26 | Shell Int Research | Verbeterde werkwijze voor het winnen van vanadium van gedesactiveerde katalysatoren. |
| NL7703180A (nl) * | 1977-03-24 | 1978-09-26 | Shell Int Research | Verbeterde werkwijze voor het winnen van vanadium van gedesactiveerde katalysatoren. |
| US4272401A (en) | 1978-09-01 | 1981-06-09 | Exxon Research & Engineering Co. | Regeneration of spent hydrodesulfurization catalyst with heteropoly acids |
| CA1163810A (en) * | 1980-02-20 | 1984-03-20 | Petrus J.W.M. Van Den Bosch | Process for the removal of vanadium-containing acid from an acid-extracted deactivated demetallization catalyst |
| NL8103964A (nl) | 1981-08-26 | 1983-03-16 | Shell Int Research | Werkwijze voor het winnen van vijfwaardige vanadium verbindingen uit zure katalysator extracten. |
| US4595666A (en) * | 1981-11-02 | 1986-06-17 | Hri, Inc. | Catalyst rejuvenation process for removal of metal contaminants |
| US4454240A (en) * | 1981-11-02 | 1984-06-12 | Hri, Inc. | Catalyst regeneration process including metal contaminants removal |
| EP0122249B1 (en) * | 1983-04-01 | 1986-05-21 | Monsanto Company | Recovery of vanadium and copper from adipic acid production |
| DD239348A5 (de) * | 1985-07-19 | 1986-09-24 | ��������@�����������@�@������������@���������@����@����������@���k�� | Verfahren zur verarbeitung von vanadinhaltigen altkatalysatoren |
| CA1293380C (en) * | 1985-12-11 | 1991-12-24 | Just Jan Christiaan Jansz | Vanadium recovery process |
| GB8610442D0 (en) * | 1986-04-29 | 1986-06-04 | Shell Int Research | Regeneration of spent alumina-based catalysts |
| FR2614613B1 (fr) * | 1987-04-29 | 1989-06-09 | Rhone Poulenc Chimie | Procede de recuperation du vanadium |
| US5254513A (en) * | 1991-05-20 | 1993-10-19 | Texaco, Inc. | Method for the reactivation of spent alumina-supported hydrotreating catalysts |
| US5230791A (en) * | 1991-07-03 | 1993-07-27 | Texaco Inc. | Process for the reactivation of spent alumina-supported hydrotreating catalysts |
| DE4216798A1 (de) * | 1992-05-21 | 1993-11-25 | Metallgesellschaft Ag | Verfahren zur Aufarbeitung von vanadiumhaltigen Rückständen |
| BR122023003434B1 (pt) | 2016-02-23 | 2024-01-30 | John Crane Uk Ltd | Sistema de vedação mecânica configurado para detectar autonomamente uma perda de lubrificação dentro de uma interface de vedação deslizante de uma vedação mecânica, sistema de vedação mecânica que tem um subsistema de diagnóstico preditivo customizável configurado para ser adaptado para se adequar às necessidades individuais do onsumidor, condições ambientais particulares e/ou aplicações específicas, e sistema de vedação mecânica configurado para detectar condições de operação e fornecer avaliações de integridade em tempo real a um usuário durante a operação |
| CN116920878B (zh) * | 2022-04-06 | 2025-07-04 | 中国石油化工股份有限公司 | 一种失活催化剂的再利用方法 |
| CN116920877B (zh) * | 2022-04-06 | 2025-08-05 | 中国石油化工股份有限公司 | 一种金属沉积失活加氢催化剂的再生方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL106228C (enExample) * | 1956-12-28 | |||
| US3791989A (en) * | 1971-03-12 | 1974-02-12 | Chevron Res | Catalyst rejuvenation with oxalic acid |
| JPS4923447A (enExample) * | 1972-06-27 | 1974-03-01 |
-
1974
- 1974-10-15 GB GB44604/74A patent/GB1526927A/en not_active Expired
-
1975
- 1975-08-15 CA CA233,512A patent/CA1071413A/en not_active Expired
- 1975-10-07 BE BE1006931A patent/BE834257A/xx not_active IP Right Cessation
- 1975-10-13 IT IT28227/75A patent/IT1043322B/it active
- 1975-10-13 JP JP50122575A patent/JPS6012908B2/ja not_active Expired
- 1975-10-13 FR FR7531255A patent/FR2288154A1/fr active Granted
- 1975-10-13 NO NO753452A patent/NO143521C/no unknown
- 1975-10-13 SE SE7511450A patent/SE410474B/xx not_active IP Right Cessation
- 1975-10-13 MX MX100089U patent/MX3049E/es unknown
- 1975-10-13 ZA ZA00756443A patent/ZA756443B/xx unknown
- 1975-10-13 AR AR260772A patent/AR224854A1/es active
- 1975-10-13 NL NLAANVRAGE7511993,A patent/NL186587C/xx not_active IP Right Cessation
- 1975-10-13 SU SU752182547A patent/SU741780A3/ru active
- 1975-10-13 AU AU85669/75A patent/AU498495B2/en not_active Expired
- 1975-10-13 DE DE19752545787 patent/DE2545787A1/de active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| NL186587B (nl) | 1990-08-01 |
| NO143521B (no) | 1980-11-24 |
| DE2545787C2 (enExample) | 1989-08-03 |
| JPS6012908B2 (ja) | 1985-04-04 |
| MX3049E (es) | 1980-03-04 |
| CA1071413A (en) | 1980-02-12 |
| NL186587C (nl) | 1991-01-02 |
| AU8566975A (en) | 1977-04-21 |
| NL7511993A (nl) | 1976-04-21 |
| AR224854A1 (es) | 1982-01-29 |
| NO753452L (enExample) | 1976-04-21 |
| ZA756443B (en) | 1976-09-29 |
| FR2288154B1 (enExample) | 1980-07-25 |
| DE2545787A1 (de) | 1976-04-29 |
| SE410474B (sv) | 1979-10-15 |
| NO143521C (no) | 1981-03-04 |
| JPS5164412A (enExample) | 1976-06-03 |
| AU498495B2 (en) | 1979-03-15 |
| FR2288154A1 (fr) | 1976-05-14 |
| IT1043322B (it) | 1980-02-20 |
| BE834257A (nl) | 1976-04-07 |
| GB1526927A (en) | 1978-10-04 |
| SE7511450L (sv) | 1976-04-20 |
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