SU688131A3 - Способ выделени стабилизированных оксиметиленовых сополимеров - Google Patents
Способ выделени стабилизированных оксиметиленовых сополимеровInfo
- Publication number
- SU688131A3 SU688131A3 SU772480277A SU2480277A SU688131A3 SU 688131 A3 SU688131 A3 SU 688131A3 SU 772480277 A SU772480277 A SU 772480277A SU 2480277 A SU2480277 A SU 2480277A SU 688131 A3 SU688131 A3 SU 688131A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- copolymer
- temperature
- cooling
- polymer
- water
- Prior art date
Links
- 229920001577 copolymer Polymers 0.000 title claims description 30
- 238000000605 extraction Methods 0.000 title 1
- 239000000203 mixture Substances 0.000 claims description 66
- 239000000725 suspension Substances 0.000 claims description 35
- 238000001816 cooling Methods 0.000 claims description 31
- 238000005245 sintering Methods 0.000 claims description 30
- GBMDVOWEEQVZKZ-UHFFFAOYSA-N methanol;hydrate Chemical compound O.OC GBMDVOWEEQVZKZ-UHFFFAOYSA-N 0.000 claims description 19
- 239000002245 particle Substances 0.000 claims description 19
- 239000006185 dispersion Substances 0.000 claims description 13
- 238000000034 method Methods 0.000 claims description 13
- 238000002156 mixing Methods 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- 230000001376 precipitating effect Effects 0.000 claims description 2
- 230000003134 recirculating effect Effects 0.000 claims 1
- 239000002002 slurry Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 229920000642 polymer Polymers 0.000 description 63
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Substances OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 46
- 239000000047 product Substances 0.000 description 27
- 239000000243 solution Substances 0.000 description 26
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 24
- 239000002826 coolant Substances 0.000 description 20
- -1 hydroxymethylene Chemical group 0.000 description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 239000007788 liquid Substances 0.000 description 11
- 125000005704 oxymethylene group Chemical group [H]C([H])([*:2])O[*:1] 0.000 description 11
- 239000000126 substance Substances 0.000 description 9
- 239000000155 melt Substances 0.000 description 7
- 239000002904 solvent Substances 0.000 description 7
- BGJSXRVXTHVRSN-UHFFFAOYSA-N 1,3,5-trioxane Chemical compound C1OCOCO1 BGJSXRVXTHVRSN-UHFFFAOYSA-N 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 6
- 229920006324 polyoxymethylene Polymers 0.000 description 6
- 239000012716 precipitator Substances 0.000 description 6
- 238000005119 centrifugation Methods 0.000 description 5
- 238000002844 melting Methods 0.000 description 5
- 230000008018 melting Effects 0.000 description 5
- 239000012299 nitrogen atmosphere Substances 0.000 description 5
- 239000002270 dispersing agent Substances 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000004815 dispersion polymer Substances 0.000 description 3
- 239000011261 inert gas Substances 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000007858 starting material Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical compound C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 description 2
- 229910052756 noble gas Inorganic materials 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000012265 solid product Substances 0.000 description 2
- XNWFRZJHXBZDAG-UHFFFAOYSA-N 2-METHOXYETHANOL Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 description 1
- XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 1
- 229930040373 Paraformaldehyde Natural products 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- 239000000539 dimer Substances 0.000 description 1
- NKDDWNXOKDWJAK-UHFFFAOYSA-N dimethoxymethane Chemical compound COCOC NKDDWNXOKDWJAK-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000001746 injection moulding Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 description 1
- 125000005702 oxyalkylene group Chemical group 0.000 description 1
- 125000000075 primary alcohol group Chemical group 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000005029 sieve analysis Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000011550 stock solution Substances 0.000 description 1
- 238000010408 sweeping Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2/00—Addition polymers of aldehydes or cyclic oligomers thereof or of ketones; Addition copolymers thereof with less than 50 molar percent of other substances
- C08G2/18—Copolymerisation of aldehydes or ketones
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2/00—Addition polymers of aldehydes or cyclic oligomers thereof or of ketones; Addition copolymers thereof with less than 50 molar percent of other substances
- C08G2/38—Block or graft polymers prepared by polymerisation of aldehydes or ketones on to macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2359/00—Characterised by the use of polyacetals containing polyoxymethylene sequences only
- C08J2359/02—Copolyoxymethylenes
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyoxymethylene Polymers And Polymers With Carbon-To-Carbon Bonds (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Artificial Filaments (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Polyethers (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2620017A DE2620017C3 (de) | 1976-05-06 | 1976-05-06 | Verfahren zur Herstellung von grobkörnigen Oxymethylenpolymeren |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU688131A3 true SU688131A3 (ru) | 1979-09-25 |
Family
ID=5977210
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU772480277A SU688131A3 (ru) | 1976-05-06 | 1977-05-06 | Способ выделени стабилизированных оксиметиленовых сополимеров |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US4111912A (enExample) |
| JP (1) | JPS5850616B2 (enExample) |
| AT (1) | AT354733B (enExample) |
| BE (1) | BE854364A (enExample) |
| BR (1) | BR7702897A (enExample) |
| CA (1) | CA1076291A (enExample) |
| CH (1) | CH628657A5 (enExample) |
| DE (1) | DE2620017C3 (enExample) |
| DK (1) | DK199477A (enExample) |
| FR (1) | FR2350364A1 (enExample) |
| GB (1) | GB1573169A (enExample) |
| IT (1) | IT1075531B (enExample) |
| LU (1) | LU77255A1 (enExample) |
| NL (1) | NL180115C (enExample) |
| PL (1) | PL197890A1 (enExample) |
| SE (1) | SE7705211L (enExample) |
| SU (1) | SU688131A3 (enExample) |
| ZA (1) | ZA772686B (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2768143C2 (ru) * | 2017-09-12 | 2022-03-23 | Арланксео Дойчланд Гмбх | Вулканизаты сополимеров для применения в контакте со средой, содержащей оксиметиленовый эфир |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2735946C3 (de) * | 1977-08-10 | 1980-03-06 | Hoechst Ag, 6000 Frankfurt | Körniges Oxymethylenpolymer mit verbesserten mechanischen Eigenschaften und Verfahren zu dessen Herstellung |
| DE4431575A1 (de) * | 1994-09-05 | 1996-03-07 | Hoechst Ag | Verfahren zur Herstellung von Polyacetalcopolymeren |
| DE19843730A1 (de) * | 1998-09-24 | 2000-03-30 | Sueddeutsche Kalkstickstoff | Stabilisierte, wasserlösliche Polymerpulver auf Basis von Polyoxyalkylenglykol-Carboxylaten und Verfahren zu deren Herstellung |
| DE102008018965A1 (de) | 2008-04-16 | 2009-10-22 | Ticona Gmbh | Oxymethylen-Copolymere und deren Verwendung sowie Verfahren zur Herstellung von Oxymethylen-Copolymeren |
| DE102008018967A1 (de) * | 2008-04-16 | 2009-10-22 | Ticona Gmbh | Oxymethylenpolymere, Verfahren zu deren Herstellung und deren Verwendung |
| US8840976B2 (en) | 2010-10-14 | 2014-09-23 | Ticona Llc | VOC or compressed gas containment device made from a polyoxymethylene polymer |
| EP2505609B1 (en) | 2011-04-01 | 2015-01-21 | Ticona GmbH | High impact resistant polyoxymethylene for extrusion blow molding |
| WO2013101624A1 (en) | 2011-12-30 | 2013-07-04 | Ticona Llc | Printable molded articles made from a polyoxymethylene polymer composition |
| WO2014105670A1 (en) | 2012-12-27 | 2014-07-03 | Ticona Llc | Impact modified polyoxymethylene composition and articles made therefrom that are stable when exposed to ultraviolet light |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE602869A (enExample) * | 1960-04-21 | |||
| US3219623A (en) * | 1960-04-21 | 1965-11-23 | Celanese Corp | Stabilization of oxymethylene copolymers with an hydroxy containing reactant |
| GB1053119A (enExample) * | 1963-04-24 | |||
| FR1390079A (fr) * | 1963-04-24 | 1965-02-19 | Hoechst Ag | Procédé pour isoler d'une solution un polyoxyméthylène granulaire |
| CH523936A (fr) * | 1970-11-24 | 1972-06-15 | Ebauches Sa | Procédé de préparation d'un polyoxyméthylène, homo- ou copolymère, à chaînes stabilisées, pur |
| NL181204C (nl) * | 1974-11-07 | 1987-07-01 | Hoechst Ag | Werkwijze voor het bereiden van korrelvormige oxymethyleenpolymeren. |
| JPS51126294A (en) * | 1975-02-04 | 1976-11-04 | Hoechst Ag | Grannlar oxymethylene copolymer |
-
1976
- 1976-05-06 DE DE2620017A patent/DE2620017C3/de not_active Expired
-
1977
- 1977-05-02 NL NLAANVRAGE7704795,A patent/NL180115C/xx not_active IP Right Cessation
- 1977-05-03 CH CH551477A patent/CH628657A5/de not_active IP Right Cessation
- 1977-05-04 IT IT23186/77A patent/IT1075531B/it active
- 1977-05-04 JP JP52050857A patent/JPS5850616B2/ja not_active Expired
- 1977-05-04 SE SE7705211A patent/SE7705211L/xx not_active Application Discontinuation
- 1977-05-04 GB GB18661/77A patent/GB1573169A/en not_active Expired
- 1977-05-04 LU LU77255A patent/LU77255A1/xx unknown
- 1977-05-04 US US05/793,859 patent/US4111912A/en not_active Expired - Lifetime
- 1977-05-05 AT AT321077A patent/AT354733B/de not_active IP Right Cessation
- 1977-05-05 PL PL19789077A patent/PL197890A1/xx unknown
- 1977-05-05 BR BR7702897A patent/BR7702897A/pt unknown
- 1977-05-05 ZA ZA00772686A patent/ZA772686B/xx unknown
- 1977-05-05 DK DK199477A patent/DK199477A/da not_active Application Discontinuation
- 1977-05-05 CA CA277,735A patent/CA1076291A/en not_active Expired
- 1977-05-06 SU SU772480277A patent/SU688131A3/ru active
- 1977-05-06 BE BE177360A patent/BE854364A/xx not_active IP Right Cessation
- 1977-05-06 FR FR7713813A patent/FR2350364A1/fr active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2768143C2 (ru) * | 2017-09-12 | 2022-03-23 | Арланксео Дойчланд Гмбх | Вулканизаты сополимеров для применения в контакте со средой, содержащей оксиметиленовый эфир |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2620017B2 (de) | 1978-10-05 |
| GB1573169A (en) | 1980-09-17 |
| CA1076291A (en) | 1980-04-22 |
| BR7702897A (pt) | 1977-11-29 |
| DE2620017A1 (de) | 1977-11-17 |
| FR2350364A1 (fr) | 1977-12-02 |
| NL180115C (nl) | 1987-01-02 |
| CH628657A5 (de) | 1982-03-15 |
| US4111912A (en) | 1978-09-05 |
| DE2620017C3 (de) | 1979-05-31 |
| SE7705211L (sv) | 1977-11-07 |
| NL180115B (nl) | 1986-08-01 |
| ATA321077A (de) | 1979-06-15 |
| IT1075531B (it) | 1985-04-22 |
| JPS52134699A (en) | 1977-11-11 |
| AT354733B (de) | 1979-01-25 |
| PL197890A1 (pl) | 1978-02-13 |
| DK199477A (da) | 1977-11-07 |
| ZA772686B (en) | 1978-04-26 |
| LU77255A1 (enExample) | 1977-12-13 |
| BE854364A (fr) | 1977-11-07 |
| FR2350364B1 (enExample) | 1984-03-30 |
| NL7704795A (nl) | 1977-11-08 |
| JPS5850616B2 (ja) | 1983-11-11 |
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