SU617005A3 - Способ получени 2-(6-карбометоксигексил)4-( )-оксициклопентенона-2 - Google Patents
Способ получени 2-(6-карбометоксигексил)4-( )-оксициклопентенона-2Info
- Publication number
- SU617005A3 SU617005A3 SU731975423A SU1975423A SU617005A3 SU 617005 A3 SU617005 A3 SU 617005A3 SU 731975423 A SU731975423 A SU 731975423A SU 1975423 A SU1975423 A SU 1975423A SU 617005 A3 SU617005 A3 SU 617005A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- carbomethoxyhexyl
- oxycyclopentenone
- obtaining
- acetic acid
- reaction mixture
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 2
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 7
- -1 6-carbomethoxyhexyl Chemical group 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical class [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 239000011541 reaction mixture Substances 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- PIBGGWWVVJELOD-UHFFFAOYSA-N 2-hex-5-enoxyacetic acid Chemical compound OC(=O)COCCCCC=C PIBGGWWVVJELOD-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- ZAFNJMIOTHYJRJ-UHFFFAOYSA-N Diisopropyl ether Chemical compound CC(C)OC(C)C ZAFNJMIOTHYJRJ-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229940125585 NDV-HXP-S Drugs 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 238000005804 alkylation reaction Methods 0.000 description 1
- 125000005605 benzo group Chemical group 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- 239000006188 syrup Substances 0.000 description 1
- 235000020357 syrup Nutrition 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/66—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
- C07C69/73—Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of unsaturated acids
- C07C69/738—Esters of keto-carboxylic acids or aldehydo-carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C405/00—Compounds containing a five-membered ring having two side-chains in ortho position to each other, and having oxygen atoms directly attached to the ring in ortho position to one of the side-chains, one side-chain containing, not directly attached to the ring, a carbon atom having three bonds to hetero atoms with at the most one bond to halogen, and the other side-chain having oxygen atoms attached in gamma-position to the ring, e.g. prostaglandins ; Analogues or derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US30976672A | 1972-11-27 | 1972-11-27 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU617005A3 true SU617005A3 (ru) | 1978-07-25 |
Family
ID=23199601
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU731975423A SU617005A3 (ru) | 1972-11-27 | 1973-11-26 | Способ получени 2-(6-карбометоксигексил)4-( )-оксициклопентенона-2 |
Country Status (25)
| Country | Link |
|---|---|
| JP (1) | JPS5328908B2 (bs) |
| AR (1) | AR198543A1 (bs) |
| AT (1) | AT330143B (bs) |
| AU (1) | AU459800B2 (bs) |
| BE (1) | BE807825A (bs) |
| BG (1) | BG21204A3 (bs) |
| CA (1) | CA1034139A (bs) |
| CH (1) | CH599098A5 (bs) |
| CS (1) | CS170480B2 (bs) |
| DD (1) | DD108516A5 (bs) |
| DE (1) | DE2358781C3 (bs) |
| ES (1) | ES420855A1 (bs) |
| FR (1) | FR2207905B1 (bs) |
| GB (1) | GB1440108A (bs) |
| HU (1) | HU169638B (bs) |
| IE (1) | IE38497B1 (bs) |
| IL (1) | IL43597A (bs) |
| NL (1) | NL7316147A (bs) |
| NO (1) | NO138905C (bs) |
| PH (1) | PH10276A (bs) |
| PL (1) | PL91162B1 (bs) |
| RO (1) | RO63011A (bs) |
| SE (1) | SE406462B (bs) |
| SU (1) | SU617005A3 (bs) |
| ZA (1) | ZA738581B (bs) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU529883B2 (en) * | 1978-09-04 | 1983-06-23 | Australian National University, The | Substituted cyclopentenones |
| JPS56159683U (bs) * | 1980-04-28 | 1981-11-28 | ||
| US5227505A (en) * | 1987-06-16 | 1993-07-13 | Nissan Chemical Industries, Ltd. | Substituted cyclic ketones, substituted cyclic enones, and process for producing the same |
| JP2696933B2 (ja) * | 1987-06-16 | 1998-01-14 | 日産化学工業株式会社 | 置換環状ケトン及び置換環状エノン並びにそれらの製造法 |
| US5254708A (en) * | 1987-06-16 | 1993-10-19 | Nissan Chemical Industries, Ltd. | Substituted cyclic ketones, substituted cyclic enones, and process for producing the same |
| US5231208A (en) * | 1987-06-16 | 1993-07-27 | Nissan Chemical Industries, Ltd. | Substituted cyclic ketones, substituted cyclic enones, and process for producing the same |
-
1973
- 1973-11-07 CA CA185,210A patent/CA1034139A/en not_active Expired
- 1973-11-07 IE IE2003/73A patent/IE38497B1/xx unknown
- 1973-11-08 AU AU62283/73A patent/AU459800B2/en not_active Expired
- 1973-11-08 IL IL43597A patent/IL43597A/en unknown
- 1973-11-08 ZA ZA738581A patent/ZA738581B/xx unknown
- 1973-11-09 GB GB5222073A patent/GB1440108A/en not_active Expired
- 1973-11-15 PH PH15227A patent/PH10276A/en unknown
- 1973-11-16 AR AR251028A patent/AR198543A1/es active
- 1973-11-20 CH CH1628373A patent/CH599098A5/xx not_active IP Right Cessation
- 1973-11-22 AT AT980073A patent/AT330143B/de not_active IP Right Cessation
- 1973-11-22 JP JP13086973A patent/JPS5328908B2/ja not_active Expired
- 1973-11-26 DE DE2358781A patent/DE2358781C3/de not_active Expired
- 1973-11-26 DD DD174893A patent/DD108516A5/xx unknown
- 1973-11-26 BG BG025076A patent/BG21204A3/xx unknown
- 1973-11-26 ES ES420855A patent/ES420855A1/es not_active Expired
- 1973-11-26 SU SU731975423A patent/SU617005A3/ru active
- 1973-11-26 NL NL7316147A patent/NL7316147A/xx unknown
- 1973-11-26 HU HUWI246A patent/HU169638B/hu unknown
- 1973-11-26 BE BE138190A patent/BE807825A/xx not_active IP Right Cessation
- 1973-11-26 FR FR7341997A patent/FR2207905B1/fr not_active Expired
- 1973-11-26 NO NO734495A patent/NO138905C/no unknown
- 1973-11-26 SE SE737315982A patent/SE406462B/sv unknown
- 1973-11-26 RO RO7300076778A patent/RO63011A/ro unknown
- 1973-11-26 PL PL1973166812A patent/PL91162B1/pl unknown
- 1973-11-26 CS CS8114A patent/CS170480B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| SE406462B (sv) | 1979-02-12 |
| JPS5328908B2 (bs) | 1978-08-17 |
| JPS4982649A (bs) | 1974-08-08 |
| AT330143B (de) | 1976-06-10 |
| NO138905B (no) | 1978-08-28 |
| NO138905C (no) | 1978-12-06 |
| AU459800B2 (en) | 1975-04-10 |
| AU6228373A (en) | 1975-04-10 |
| IL43597A0 (en) | 1974-03-14 |
| GB1440108A (en) | 1976-06-23 |
| HU169638B (bs) | 1976-12-28 |
| IE38497L (en) | 1974-05-27 |
| PH10276A (en) | 1976-11-03 |
| ATA980073A (de) | 1975-09-15 |
| CH599098A5 (bs) | 1978-05-12 |
| DD108516A5 (de) | 1974-09-20 |
| DE2358781C3 (de) | 1979-11-08 |
| FR2207905A1 (bs) | 1974-06-21 |
| IE38497B1 (en) | 1978-03-29 |
| IL43597A (en) | 1976-09-30 |
| RO63011A (fr) | 1978-05-15 |
| DE2358781A1 (de) | 1974-06-12 |
| ES420855A1 (es) | 1976-04-01 |
| DE2358781B2 (de) | 1979-01-25 |
| NL7316147A (bs) | 1974-05-29 |
| BG21204A3 (bg) | 1976-03-20 |
| ZA738581B (en) | 1974-09-25 |
| AR198543A1 (es) | 1974-06-28 |
| FR2207905B1 (bs) | 1978-02-24 |
| BE807825A (fr) | 1974-03-15 |
| CS170480B2 (bs) | 1976-08-27 |
| CA1034139A (en) | 1978-07-04 |
| PL91162B1 (en) | 1977-02-28 |
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