SU598560A3 - Способ получени замещенных 2-хлор-4-алкиламино-6цианоалкиламино-1,3,5триазинов - Google Patents
Способ получени замещенных 2-хлор-4-алкиламино-6цианоалкиламино-1,3,5триазиновInfo
- Publication number
- SU598560A3 SU598560A3 SU742017401A SU2017401A SU598560A3 SU 598560 A3 SU598560 A3 SU 598560A3 SU 742017401 A SU742017401 A SU 742017401A SU 2017401 A SU2017401 A SU 2017401A SU 598560 A3 SU598560 A3 SU 598560A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- acetone
- mol
- product
- aqueous solution
- solution
- Prior art date
Links
- 238000000034 method Methods 0.000 title description 10
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 30
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 16
- 239000000047 product Substances 0.000 description 14
- 239000007864 aqueous solution Substances 0.000 description 13
- 239000011541 reaction mixture Substances 0.000 description 12
- 239000000243 solution Substances 0.000 description 12
- 238000001816 cooling Methods 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 8
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 description 8
- 239000000203 mixture Substances 0.000 description 8
- 150000002576 ketones Chemical class 0.000 description 7
- MZZBPDKVEFVLFF-UHFFFAOYSA-N Cyanazine Natural products CCNC1=NC(Cl)=NC(NC(C)(C)C#N)=N1 MZZBPDKVEFVLFF-UHFFFAOYSA-N 0.000 description 6
- 235000011121 sodium hydroxide Nutrition 0.000 description 5
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 4
- -1 alkali metal cyanide Chemical class 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- 229910052783 alkali metal Inorganic materials 0.000 description 3
- 150000003863 ammonium salts Chemical class 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000001953 recrystallisation Methods 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 235000019270 ammonium chloride Nutrition 0.000 description 2
- KXZJHVJKXJLBKO-UHFFFAOYSA-N chembl1408157 Chemical compound N=1C2=CC=CC=C2C(C(=O)O)=CC=1C1=CC=C(O)C=C1 KXZJHVJKXJLBKO-UHFFFAOYSA-N 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- IUCVBFHDSFSEIK-UHFFFAOYSA-N 2-{[4-chloro-6-(ethylamino)-1,3,5-triazin-2-yl]amino}-2-methylbutanenitrile Chemical compound CCNC1=NC(Cl)=NC(NC(C)(CC)C#N)=N1 IUCVBFHDSFSEIK-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 150000003973 alkyl amines Chemical class 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- ICAIHGOJRDCMHE-UHFFFAOYSA-O ammonium cyanide Chemical compound [NH4+].N#[C-] ICAIHGOJRDCMHE-UHFFFAOYSA-O 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 229940088623 biologically active substance Drugs 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 230000002363 herbicidal effect Effects 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- JJWLVOIRVHMVIS-UHFFFAOYSA-N isopropylamine Chemical compound CC(C)N JJWLVOIRVHMVIS-UHFFFAOYSA-N 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
- A01N43/66—1,3,5-Triazines, not hydrogenated and not substituted at the ring nitrogen atoms
- A01N43/68—1,3,5-Triazines, not hydrogenated and not substituted at the ring nitrogen atoms with two or three nitrogen atoms directly attached to ring carbon atoms
- A01N43/70—Diamino—1,3,5—triazines with only one oxygen, sulfur or halogen atom or only one cyano, thiocyano (—SCN), cyanato (—OCN) or azido (—N3) group directly attached to a ring carbon atom
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Dentistry (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Plural Heterocyclic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| HUNO000172 HU167030B (enExample) | 1973-04-09 | 1973-04-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU598560A3 true SU598560A3 (ru) | 1978-03-15 |
Family
ID=11000028
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU742017401A SU598560A3 (ru) | 1973-04-09 | 1974-04-08 | Способ получени замещенных 2-хлор-4-алкиламино-6цианоалкиламино-1,3,5триазинов |
Country Status (10)
| Country | Link |
|---|---|
| CS (1) | CS203971B2 (enExample) |
| DE (1) | DE2416930C2 (enExample) |
| ES (1) | ES447118A1 (enExample) |
| FR (1) | FR2224467A1 (enExample) |
| HU (1) | HU167030B (enExample) |
| PL (1) | PL99093B1 (enExample) |
| RO (2) | RO63907A (enExample) |
| SU (1) | SU598560A3 (enExample) |
| TR (1) | TR17906A (enExample) |
| YU (2) | YU39918B (enExample) |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH550546A (de) * | 1971-08-05 | 1974-06-28 | Ciba Geigy Ag | Herbizides mittel. |
-
1973
- 1973-04-09 HU HUNO000172 patent/HU167030B/hu not_active IP Right Cessation
-
1974
- 1974-04-05 YU YU95474A patent/YU39918B/xx unknown
- 1974-04-05 FR FR7412077A patent/FR2224467A1/fr active Granted
- 1974-04-08 DE DE19742416930 patent/DE2416930C2/de not_active Expired
- 1974-04-08 CS CS251874A patent/CS203971B2/cs unknown
- 1974-04-08 SU SU742017401A patent/SU598560A3/ru active
- 1974-04-09 RO RO7835674A patent/RO63907A/ro unknown
- 1974-04-09 TR TR1790674A patent/TR17906A/xx unknown
- 1974-04-09 RO RO7484992A patent/RO70194A/ro unknown
- 1974-04-09 PL PL18347274A patent/PL99093B1/pl unknown
-
1976
- 1976-04-15 ES ES447118A patent/ES447118A1/es not_active Expired
-
1980
- 1980-04-01 YU YU90380A patent/YU40071B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| RO63907A (fr) | 1978-09-15 |
| DE2416930C2 (de) | 1984-08-30 |
| RO70194A (ro) | 1980-12-30 |
| PL99093B1 (pl) | 1978-06-30 |
| YU90380A (en) | 1983-02-28 |
| DE2416930A1 (de) | 1974-10-24 |
| HU167030B (enExample) | 1975-07-28 |
| YU95474A (en) | 1982-06-30 |
| TR17906A (tr) | 1976-11-01 |
| CS203971B2 (en) | 1981-03-31 |
| FR2224467A1 (en) | 1974-10-31 |
| YU39918B (en) | 1985-06-30 |
| FR2224467B1 (enExample) | 1978-01-13 |
| YU40071B (en) | 1985-06-30 |
| ES447118A1 (es) | 1977-06-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| SU453830A3 (ru) | Способ получения соответственно замещенного фенацетилгуанидина | |
| US3016403A (en) | 1-aryl-3-hydroxypropyl sulfones and processes | |
| SU622399A3 (ru) | Способ получени солей арилсульфониламидоалкиламинов | |
| US2455894A (en) | Production of 1-mono-and 1, 2-disubstituted-3-cyanoguanidines | |
| SU950188A3 (ru) | Способ получени производных 4(5)-меркаптометилимидазолов | |
| US3328395A (en) | 6-halo-2-amino substituted-4-sulfanilamido-pyrimidine compounds | |
| US3320255A (en) | Production of thioethers | |
| JP2578797B2 (ja) | Ｎ−（スルホニルメチル）ホルムアミド類の製造法 | |
| US3029239A (en) | Basic substituted 1-and 7-alkylxanthines or salts thereof | |
| US2659733A (en) | Process of producing butyrolactones | |
| US3226379A (en) | Novel 1,3-bis(polyhydroxyalkyl)-2-imidazolidinones and 1,3-bis(polyhydroxyalkyl)-imidazolidine-2-thiones | |
| US2917545A (en) | Preparation of n-substituted hydrazine derivatives | |
| Mukaiyama et al. | Reactions of the Iodomethylate of N, N-Dimethylthiobenzamide with Nucleophilic Reagents | |
| NO133892B (enExample) | ||
| KR920004137B1 (ko) | 이미다졸 유도체의 제조방법 | |
| US3494921A (en) | 1,4-disubstituted pyridazino(4,5-d) pyridazines | |
| SU650504A3 (ru) | Способ получени метил-(2-хиноксалинилметилен)-карбазат-диоксида | |
| DK141531B (da) | Analogifremgangsmåde til fremstilling af 1-metyl-9,10-dihydro-d-lysergsyreallylamid eller syreadditionssalte deraf. | |
| US3597444A (en) | Method of synthesizing selenoureas from thioureas | |
| SU845781A3 (ru) | Способ получени производных пирида-зиНОНА или иХ СОлЕй | |
| SU503522A3 (ru) | Способ получени карбаматных производных 2,4-диоксиметилтиазола | |
| SU437764A1 (ru) | Способ получени 5 (4)-тиопроизводных имидазола | |
| US2676175A (en) | Process for manufacturing thiamine | |
| SU436057A1 (ru) | СПОСОБ ПОЛУЧЕНИЯ ИЗОПРОПИЛИДЕНОВЫХ ПРОИЗВОДНЫХ ПИРИДОКСИНАВ ПТ5ФОНЯ mmim | |
| US3317521A (en) | Process for the manufacture of n-(5'-nitro-2'-furfurylidene)-1-aminohydantoin |