SU416355A1 - - Google Patents
Info
- Publication number
- SU416355A1 SU416355A1 SU1698519A SU1698519A SU416355A1 SU 416355 A1 SU416355 A1 SU 416355A1 SU 1698519 A SU1698519 A SU 1698519A SU 1698519 A SU1698519 A SU 1698519A SU 416355 A1 SU416355 A1 SU 416355A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- water
- trichloroquinolyl
- mercaptide
- reaction
- propiolactone
- Prior art date
Links
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims description 9
- 238000006243 chemical reaction Methods 0.000 claims description 9
- 229960000380 propiolactone Drugs 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 7
- 230000003197 catalytic effect Effects 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 150000003512 tertiary amines Chemical class 0.000 claims description 3
- 229910052739 hydrogen Inorganic materials 0.000 claims description 2
- 239000001257 hydrogen Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 claims description 2
- 239000003960 organic solvent Substances 0.000 claims description 2
- 235000019260 propionic acid Nutrition 0.000 claims description 2
- 150000004672 propanoic acids Chemical class 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 239000002244 precipitate Substances 0.000 description 6
- 239000000706 filtrate Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- -1 4-mercapto-5,7,8-trichloroquinolylpropionic acid Chemical compound 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 3
- RMVRSNDYEFQCLF-UHFFFAOYSA-N thiophenol Chemical compound SC1=CC=CC=C1 RMVRSNDYEFQCLF-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 2
- 238000001953 recrystallisation Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- ROYCCMJSURLMLI-UHFFFAOYSA-N 1h-quinoline-4-thione Chemical class C1=CC=C2C(S)=CC=NC2=C1 ROYCCMJSURLMLI-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1698519A SU416355A1 (enrdf_load_stackoverflow) | 1971-09-13 | 1971-09-13 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1698519A SU416355A1 (enrdf_load_stackoverflow) | 1971-09-13 | 1971-09-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU416355A1 true SU416355A1 (enrdf_load_stackoverflow) | 1974-02-25 |
Family
ID=20488313
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1698519A SU416355A1 (enrdf_load_stackoverflow) | 1971-09-13 | 1971-09-13 |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU416355A1 (enrdf_load_stackoverflow) |
-
1971
- 1971-09-13 SU SU1698519A patent/SU416355A1/ru active
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