SU313834A1 - - Google Patents

Info

Publication number

SU313834A1

SU313834A1 SU1349286A SU1349286A SU313834A1 SU 313834 A1 SU313834 A1 SU 313834A1 SU 1349286 A SU1349286 A SU 1349286A SU 1349286 A SU1349286 A SU 1349286A SU 313834 A1 SU313834 A1 SU 313834A1

Authority

SU

USSR - Soviet Union

Prior art keywords

flask

product

yield

toluene

degradation

Prior art date

Links

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• YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
• 238000000034 method Methods 0.000 description 7
• -1 polymethylphenylsiloxane Polymers 0.000 description 6
• 239000007788 liquid Substances 0.000 description 5
• 230000015556 catabolic process Effects 0.000 description 4
• 238000006731 degradation reaction Methods 0.000 description 4
• 239000000047 product Substances 0.000 description 4
• CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 3
• FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 3
• 230000003197 catalytic effect Effects 0.000 description 3
• OSXYHAQZDCICNX-UHFFFAOYSA-N dichloro(diphenyl)silane Chemical compound C=1C=CC=CC=1[Si](Cl)(Cl)C1=CC=CC=C1 OSXYHAQZDCICNX-UHFFFAOYSA-N 0.000 description 3
• LIKFHECYJZWXFJ-UHFFFAOYSA-N dimethyldichlorosilane Chemical compound C[Si](C)(Cl)Cl LIKFHECYJZWXFJ-UHFFFAOYSA-N 0.000 description 3
• 239000000203 mixture Substances 0.000 description 3
• 238000010992 reflux Methods 0.000 description 3
• 238000003756 stirring Methods 0.000 description 3
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
• WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 2
• 239000003054 catalyst Substances 0.000 description 2
• 235000002639 sodium chloride Nutrition 0.000 description 2
• 239000011780 sodium chloride Substances 0.000 description 2
• 239000000243 solution Substances 0.000 description 2
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
• 239000002253 acid Substances 0.000 description 1
• 230000002378 acidificating effect Effects 0.000 description 1
• 239000007864 aqueous solution Substances 0.000 description 1
• 230000001174 ascending effect Effects 0.000 description 1
• 239000004927 clay Substances 0.000 description 1
• 239000007857 degradation product Substances 0.000 description 1
• KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 1
• 238000001914 filtration Methods 0.000 description 1
• 239000012530 fluid Substances 0.000 description 1
• UQEAIHBTYFGYIE-UHFFFAOYSA-N hexamethyldisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)C UQEAIHBTYFGYIE-UHFFFAOYSA-N 0.000 description 1
• 238000011068 loading method Methods 0.000 description 1
• 238000004519 manufacturing process Methods 0.000 description 1
• 229920001921 poly-methyl-phenyl-siloxane Polymers 0.000 description 1
• 238000002360 preparation method Methods 0.000 description 1
• 230000008707 rearrangement Effects 0.000 description 1
• 239000012047 saturated solution Substances 0.000 description 1
• 238000000926 separation method Methods 0.000 description 1
• 235000017550 sodium carbonate Nutrition 0.000 description 1
• 229910000029 sodium carbonate Inorganic materials 0.000 description 1
• 238000007711 solidification Methods 0.000 description 1
• 230000008023 solidification Effects 0.000 description 1