SU236468A1 - - Google Patents

Info

Publication number

SU236468A1

SU236468A1 SU1183160A SU1183160A SU236468A1 SU 236468 A1 SU236468 A1 SU 236468A1 SU 1183160 A SU1183160 A SU 1183160A SU 1183160 A SU1183160 A SU 1183160A SU 236468 A1 SU236468 A1 SU 236468A1

Authority

SU

USSR - Soviet Union

Prior art keywords

thiophosphoric

synthesis

intermediates

acids

mixture

Prior art date

Links

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• 238000000034 method Methods 0.000 claims description 7
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
• 239000000047 product Substances 0.000 claims description 6
• 239000000203 mixture Substances 0.000 claims description 4
• 230000003197 catalytic effect Effects 0.000 claims description 2
• 150000002148 esters Chemical class 0.000 claims description 2
• 230000003993 interaction Effects 0.000 claims description 2
• 239000013067 intermediate product Substances 0.000 claims description 2
• 150000003839 salts Chemical class 0.000 claims description 2
• 230000015572 biosynthetic process Effects 0.000 claims 7
• 238000003786 synthesis reaction Methods 0.000 claims 7
• 239000000543 intermediate Substances 0.000 claims 6
• 150000003582 thiophosphoric acids Chemical class 0.000 claims 5
• RYYWUUFWQRZTIU-UHFFFAOYSA-N Thiophosphoric acid Chemical compound OP(O)(S)=O RYYWUUFWQRZTIU-UHFFFAOYSA-N 0.000 claims 2
• DJMQXCFMMJCCFN-UHFFFAOYSA-N benzyl-dihydroxy-sulfanylidene-$l^{5}-phosphane Chemical class OP(O)(=S)CC1=CC=CC=C1 DJMQXCFMMJCCFN-UHFFFAOYSA-N 0.000 claims 1
• 238000010438 heat treatment Methods 0.000 claims 1
• 238000002955 isolation Methods 0.000 claims 1
• JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 6
• 239000002253 acid Substances 0.000 description 3
• UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 3
• RMVRSNDYEFQCLF-UHFFFAOYSA-N thiophenol Chemical compound SC1=CC=CC=C1 RMVRSNDYEFQCLF-UHFFFAOYSA-N 0.000 description 3
• 150000001875 compounds Chemical class 0.000 description 2
• 239000007788 liquid Substances 0.000 description 2
• DEWLEGDTCGBNGU-UHFFFAOYSA-N 1,3-dichloropropan-2-ol Chemical compound ClCC(O)CCl DEWLEGDTCGBNGU-UHFFFAOYSA-N 0.000 description 1
• XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 1
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
• OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
• QVMHUALAQYRRBM-UHFFFAOYSA-N [P].[P] Chemical compound [P].[P] QVMHUALAQYRRBM-UHFFFAOYSA-N 0.000 description 1
• 150000007513 acids Chemical class 0.000 description 1
• 125000000217 alkyl group Chemical group 0.000 description 1
• -1 benzyl dithiophosphonates Chemical class 0.000 description 1
• 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 1
• 239000000460 chlorine Substances 0.000 description 1
• 229910052801 chlorine Inorganic materials 0.000 description 1
• 125000001309 chloro group Chemical group Cl* 0.000 description 1
• BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
• IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
• 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
• 239000000575 pesticide Substances 0.000 description 1
• 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
• 229910052698 phosphorus Inorganic materials 0.000 description 1
• 239000011574 phosphorus Substances 0.000 description 1
• 238000002360 preparation method Methods 0.000 description 1
• 239000011541 reaction mixture Substances 0.000 description 1
• 238000010992 reflux Methods 0.000 description 1
• 238000000926 separation method Methods 0.000 description 1
• 239000000126 substance Substances 0.000 description 1
• 238000005406 washing Methods 0.000 description 1