SU182155A1 - - Google Patents

Info

Publication number

SU182155A1

SU182155A1 SU1001569A SU1001569A SU182155A1 SU 182155 A1 SU182155 A1 SU 182155A1 SU 1001569 A SU1001569 A SU 1001569A SU 1001569 A SU1001569 A SU 1001569A SU 182155 A1 SU182155 A1 SU 182155A1

Authority

SU

USSR - Soviet Union

Prior art keywords

acid

mol

yield

heated

hypophosphorous acid

Prior art date

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• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 5
• ACVYVLVWPXVTIT-UHFFFAOYSA-N phosphinic acid Chemical compound O[PH2]=O ACVYVLVWPXVTIT-UHFFFAOYSA-N 0.000 description 5
• 239000002253 acid Substances 0.000 description 4
• 238000000034 method Methods 0.000 description 3
• VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
• 150000007513 acids Chemical class 0.000 description 2
• 239000000538 analytical sample Substances 0.000 description 2
• 238000009835 boiling Methods 0.000 description 2
• 239000012442 inert solvent Substances 0.000 description 2
• 230000003993 interaction Effects 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• 239000002904 solvent Substances 0.000 description 2
• 239000000126 substance Substances 0.000 description 2
• HFFLGKNGCAIQMO-UHFFFAOYSA-N trichloroacetaldehyde Chemical compound ClC(Cl)(Cl)C=O HFFLGKNGCAIQMO-UHFFFAOYSA-N 0.000 description 2
• -1 -halo aldehyde Chemical class 0.000 description 1
• RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
• 102000020897 Formins Human genes 0.000 description 1
• 108091022623 Formins Proteins 0.000 description 1
• 239000012736 aqueous medium Substances 0.000 description 1
• RNFNDJAIBTYOQL-UHFFFAOYSA-N chloral hydrate Chemical compound OC(O)C(Cl)(Cl)Cl RNFNDJAIBTYOQL-UHFFFAOYSA-N 0.000 description 1
• 229960002327 chloral hydrate Drugs 0.000 description 1
• 238000001816 cooling Methods 0.000 description 1
• 239000013078 crystal Substances 0.000 description 1
• 238000002844 melting Methods 0.000 description 1
• 230000008018 melting Effects 0.000 description 1
• XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
• 238000002360 preparation method Methods 0.000 description 1
• 238000001953 recrystallisation Methods 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 238000005406 washing Methods 0.000 description 1