SU124123A1 - Method of producing titanium trichloride, titanium lower chlorides and titanium metal - Google Patents
Method of producing titanium trichloride, titanium lower chlorides and titanium metalInfo
- Publication number
- SU124123A1 SU124123A1 SU619889A SU619889A SU124123A1 SU 124123 A1 SU124123 A1 SU 124123A1 SU 619889 A SU619889 A SU 619889A SU 619889 A SU619889 A SU 619889A SU 124123 A1 SU124123 A1 SU 124123A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- titanium
- metal
- producing
- trichloride
- chlorides
- Prior art date
Links
Landscapes
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Description
При нззестных способах получени лгеталлического титана и его .НИЗШИХ хлоридов дл восстановлени водорода используют алюлмшии, лагний, натрий и др. ВосстанОЗле1 не четыреххлормстого титана про ,извод т при температурах в интервале 150-800° С. Полученный таким способом металл требует дополнптелыюй очистки от восстановителей.In situ methods of producing metallic titanium and its. LOW chlorides, aluminum is used for the reduction of hydrogen. They are lagged, sodium, etc. The non-tetrachlorite titanium is reduced and is removed at temperatures in the range of 150-800 ° C. The metal thus obtained requires additional cleaning from reducing agents .
Восста1ювление четыреххлористого титана по предлагаемо.:у способу производ т в вакууме или в атмосфере инертного газа путем воздействи ионизирующей радиации у-излучени радиоактивного кобальта 60 на раствор четыреххлористого титана в углеводороде при температуре 20° С.Reduction of titanium tetrachloride by the proposed method: the method is produced in vacuum or in an inert gas atmosphere by exposing the y-radiation of radioactive cobalt 60 to a solution of titanium tetrachloride in a hydrocarbon at a temperature of 20 ° C.
Образующиес из углеводородов свободные радикалы восстанавливают четыреххлористый титан до его низших хлоридов или металла. При этом металлический титан и его субхлориды выпадают в осадок, после чего их легко отдел ют от продуктов радиолнза.Free radicals formed from hydrocarbons reduce titanium tetrachloride to its lower chlorides or metal. In this case, metallic titanium and its subchlorides precipitate, after which they are easily separated from the radio wave products.
Облучение раствора, содержащего 66,6 об. /о тетрахлорида титана в сухом октане, лучалш кобальта 60 активностью 1440 г-же радн при мощности дозы 0,72 мли. р/час дало положительиые результаты.Irradiation of a solution containing 66.6 vol. / o titanium tetrachloride in dry octane, cobalt luchalsh 60 with an activity of 1,440 Ms. glad with a dose rate of 0.72 ml. p / hour gave positive results.
Предмет зобретени Subject matter
Способ получени низших хлоридов титана и металлического титана из его тетрахлорида, отличающийс тем, что, с целью упрощени технологического процесса, исходный раствор тетрахлорида титана в углеводородах обрабатывают радиоактивными луча.ми.A method of producing lower titanium chlorides and titanium metal from its tetrachloride, characterized in that, in order to simplify the technological process, the initial solution of titanium tetrachloride in hydrocarbons is treated with radioactive rays.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU619889A SU124123A1 (en) | 1959-02-18 | 1959-02-18 | Method of producing titanium trichloride, titanium lower chlorides and titanium metal |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
SU619889A SU124123A1 (en) | 1959-02-18 | 1959-02-18 | Method of producing titanium trichloride, titanium lower chlorides and titanium metal |
Publications (1)
Publication Number | Publication Date |
---|---|
SU124123A1 true SU124123A1 (en) | 1959-11-30 |
Family
ID=48395619
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
SU619889A SU124123A1 (en) | 1959-02-18 | 1959-02-18 | Method of producing titanium trichloride, titanium lower chlorides and titanium metal |
Country Status (1)
Country | Link |
---|---|
SU (1) | SU124123A1 (en) |
-
1959
- 1959-02-18 SU SU619889A patent/SU124123A1/en active
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