SU1192611A3 - Способ получени 2-метокси-2,6-диметил-9-( @ -изопропилфенил)нонана - Google Patents
Способ получени 2-метокси-2,6-диметил-9-( @ -изопропилфенил)нонана Download PDFInfo
- Publication number
- SU1192611A3 SU1192611A3 SU813327707A SU3327707A SU1192611A3 SU 1192611 A3 SU1192611 A3 SU 1192611A3 SU 813327707 A SU813327707 A SU 813327707A SU 3327707 A SU3327707 A SU 3327707A SU 1192611 A3 SU1192611 A3 SU 1192611A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- chloride
- dimethyl
- formula
- methoxy
- producing
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 7
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 5
- KXZJHVJKXJLBKO-UHFFFAOYSA-N chembl1408157 Chemical compound N=1C2=CC=CC=C2C(C(=O)O)=CC=1C1=CC=C(O)C=C1 KXZJHVJKXJLBKO-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims description 2
- AUHZEENZYGFFBQ-UHFFFAOYSA-N mesitylene Substances CC1=CC(C)=CC(C)=C1 AUHZEENZYGFFBQ-UHFFFAOYSA-N 0.000 claims description 2
- 125000001827 mesitylenyl group Chemical group [H]C1=C(C(*)=C(C([H])=C1C([H])([H])[H])C([H])([H])[H])C([H])([H])[H] 0.000 claims description 2
- 238000009835 boiling Methods 0.000 claims 2
- SKEIFHHBXILYJQ-UHFFFAOYSA-N 8-methoxy-4,8-dimethyl-2-[(4-propan-2-ylphenyl)methyl]nonanenitrile Chemical compound COC(C)(C)CCCC(C)CC(C#N)CC1=CC=C(C(C)C)C=C1 SKEIFHHBXILYJQ-UHFFFAOYSA-N 0.000 claims 1
- KEAYESYHFKHZAL-UHFFFAOYSA-N Sodium Chemical compound [Na] KEAYESYHFKHZAL-UHFFFAOYSA-N 0.000 claims 1
- KCXMKQUNVWSEMD-UHFFFAOYSA-N benzyl chloride Chemical compound ClCC1=CC=CC=C1 KCXMKQUNVWSEMD-UHFFFAOYSA-N 0.000 claims 1
- 229940073608 benzyl chloride Drugs 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims 1
- SUSQOBVLVYHIEX-UHFFFAOYSA-N phenylacetonitrile Chemical compound N#CCC1=CC=CC=C1 SUSQOBVLVYHIEX-UHFFFAOYSA-N 0.000 claims 1
- -1 methylenedioxy Chemical group 0.000 abstract description 6
- 230000029936 alkylation Effects 0.000 abstract description 2
- 238000005804 alkylation reaction Methods 0.000 abstract description 2
- 125000000229 (C1-C4)alkoxy group Chemical group 0.000 abstract 1
- 125000006527 (C1-C5) alkyl group Chemical group 0.000 abstract 1
- 125000006734 (C2-C20) alkoxyalkyl group Chemical group 0.000 abstract 1
- 125000006755 (C2-C20) alkyl group Chemical group 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical group [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 125000004183 alkoxy alkyl group Chemical group 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 238000007333 cyanation reaction Methods 0.000 abstract 1
- 238000007255 decyanation reaction Methods 0.000 abstract 1
- 229910052739 hydrogen Chemical group 0.000 abstract 1
- 239000001257 hydrogen Chemical group 0.000 abstract 1
- 125000001997 phenyl group Chemical class [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 8
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 6
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical group CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- 238000010992 reflux Methods 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- 229910052708 sodium Inorganic materials 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 2
- 238000005481 NMR spectroscopy Methods 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- WVDDGKGOMKODPV-UHFFFAOYSA-N hydroxymethyl benzene Natural products OCC1=CC=CC=C1 WVDDGKGOMKODPV-UHFFFAOYSA-N 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 235000019445 benzyl alcohol Nutrition 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 230000035800 maturation Effects 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- XKBGEWXEAPTVCK-UHFFFAOYSA-M methyltrioctylammonium chloride Chemical compound [Cl-].CCCCCCCC[N+](C)(CCCCCCCC)CCCCCCCC XKBGEWXEAPTVCK-UHFFFAOYSA-M 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
- C07C15/02—Monocyclic hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/14—Preparation of carboxylic acid nitriles by reaction of cyanides with halogen-containing compounds with replacement of halogen atoms by cyano groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C43/00—Ethers; Compounds having groups, groups or groups
- C07C43/02—Ethers
- C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
- C07C43/14—Unsaturated ethers
- C07C43/164—Unsaturated ethers containing six-membered aromatic rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Toxicology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US18450680A | 1980-09-05 | 1980-09-05 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU1192611A3 true SU1192611A3 (ru) | 1985-11-15 |
Family
ID=22677158
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU813327707A SU1192611A3 (ru) | 1980-09-05 | 1981-09-04 | Способ получени 2-метокси-2,6-диметил-9-( @ -изопропилфенил)нонана |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP0047562B1 (enExample) |
| JP (1) | JPS5780330A (enExample) |
| KR (1) | KR850000568B1 (enExample) |
| BR (1) | BR8105710A (enExample) |
| CA (1) | CA1174686A (enExample) |
| DE (1) | DE3161507D1 (enExample) |
| HU (1) | HU189532B (enExample) |
| IL (1) | IL63743A0 (enExample) |
| SU (1) | SU1192611A3 (enExample) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3341306A1 (de) * | 1983-11-15 | 1985-05-23 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von in 2-stellung aromatisch oder heterocyclisch substituierten acetonitrilen |
| JP2551649Y2 (ja) * | 1992-03-13 | 1997-10-27 | 日本軽金属株式会社 | アルミニウム製折り畳み式コンテナ |
| RU2384560C1 (ru) * | 2008-08-27 | 2010-03-20 | Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран | Способ получения 1-алкокси-1-фенилэтанов |
| RU2384559C1 (ru) * | 2008-08-27 | 2010-03-20 | Учреждение Российской Академии Наук Институт Нефтехимии И Катализа Ран | Способ получения 1-алкокси-1-фенилэтанов |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1668034A1 (de) * | 1967-10-21 | 1971-07-22 | Bayer Ag | Verfahren zur Herstellung von Benzylcyaniden und deren Homologen |
| US4002769A (en) * | 1974-08-16 | 1977-01-11 | The United States Of America As Represented By The Secretary Of Agriculture | Insect maturation inhibitors |
-
1981
- 1981-08-31 JP JP56135649A patent/JPS5780330A/ja active Granted
- 1981-08-31 KR KR1019810003221A patent/KR850000568B1/ko not_active Expired
- 1981-09-02 CA CA000385032A patent/CA1174686A/en not_active Expired
- 1981-09-03 EP EP81200987A patent/EP0047562B1/en not_active Expired
- 1981-09-03 DE DE8181200987T patent/DE3161507D1/de not_active Expired
- 1981-09-04 SU SU813327707A patent/SU1192611A3/ru active
- 1981-09-04 IL IL63743A patent/IL63743A0/xx unknown
- 1981-09-04 BR BR8105710A patent/BR8105710A/pt unknown
- 1981-09-04 HU HU812570A patent/HU189532B/hu not_active IP Right Cessation
Non-Patent Citations (1)
| Title |
|---|
| Патент US № 4002769, кл. 424339, опублик. 1970. * |
Also Published As
| Publication number | Publication date |
|---|---|
| KR830006150A (ko) | 1983-09-17 |
| JPS5780330A (en) | 1982-05-19 |
| CA1174686A (en) | 1984-09-18 |
| EP0047562B1 (en) | 1983-11-23 |
| KR850000568B1 (ko) | 1985-04-29 |
| IL63743A0 (en) | 1981-12-31 |
| HU189532B (en) | 1986-07-28 |
| EP0047562A1 (en) | 1982-03-17 |
| JPS6259096B2 (enExample) | 1987-12-09 |
| DE3161507D1 (en) | 1983-12-29 |
| BR8105710A (pt) | 1982-05-25 |
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