SG11201601069PA - Method for producing methacrolein and the conditioning/draining thereof for direct oxidative esterification - Google Patents

Method for producing methacrolein and the conditioning/draining thereof for direct oxidative esterification

Info

Publication number
SG11201601069PA
SG11201601069PA SG11201601069PA SG11201601069PA SG11201601069PA SG 11201601069P A SG11201601069P A SG 11201601069PA SG 11201601069P A SG11201601069P A SG 11201601069PA SG 11201601069P A SG11201601069P A SG 11201601069PA SG 11201601069P A SG11201601069P A SG 11201601069PA
Authority
SG
Singapore
Prior art keywords
draining
conditioning
oxidative esterification
producing methacrolein
direct oxidative
Prior art date
Application number
SG11201601069PA
Other languages
English (en)
Inventor
Steffen Krill
Matthias Grömping
Alexander Lygin
Torsten Balduf
Rudolf Burghardt
Original Assignee
Evonik Roehm Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Roehm Gmbh filed Critical Evonik Roehm Gmbh
Publication of SG11201601069PA publication Critical patent/SG11201601069PA/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78Separation; Purification; Stabilisation; Use of additives
    • C07C45/80Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78Separation; Purification; Stabilisation; Use of additives
    • C07C45/81Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C07C45/84Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation by azeotropic distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/39Preparation of carboxylic acid esters by oxidation of groups which are precursors for the acid moiety of the ester
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/52Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/72Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups
    • C07C45/75Reactions with formaldehyde
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78Separation; Purification; Stabilisation; Use of additives
    • C07C45/81Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00Compounds having —CHO groups
    • C07C47/20Unsaturated compounds having —CHO groups bound to acyclic carbon atoms
    • C07C47/21Unsaturated compounds having —CHO groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C47/22Acryaldehyde; Methacryaldehyde
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54Acrylic acid esters; Methacrylic acid esters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
SG11201601069PA 2013-09-26 2014-08-27 Method for producing methacrolein and the conditioning/draining thereof for direct oxidative esterification SG11201601069PA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP13186137 2013-09-26
PCT/EP2014/068171 WO2015043861A1 (de) 2013-09-26 2014-08-27 Verfahren zur herstellung von methacrolein und dessen konditionierung/entwässerung für die direkte oxidative veresterung

Publications (1)

Publication Number Publication Date
SG11201601069PA true SG11201601069PA (en) 2016-03-30

Family

ID=49231361

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201601069PA SG11201601069PA (en) 2013-09-26 2014-08-27 Method for producing methacrolein and the conditioning/draining thereof for direct oxidative esterification

Country Status (12)

Country Link
US (1) US9580374B2 (zh)
EP (1) EP3049385B1 (zh)
JP (1) JP6355723B2 (zh)
KR (1) KR102282531B1 (zh)
CN (1) CN105683148B (zh)
BR (1) BR112016006509B1 (zh)
MY (1) MY192947A (zh)
RU (1) RU2645214C2 (zh)
SA (1) SA516370808B1 (zh)
SG (1) SG11201601069PA (zh)
TW (1) TWI633082B (zh)
WO (1) WO2015043861A1 (zh)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2998284A1 (de) * 2014-09-18 2016-03-23 Evonik Röhm GmbH Optimiertes Verfahren zur Herstellung von Methacrolein
EP3144291A1 (de) * 2015-09-16 2017-03-22 Evonik Röhm GmbH Synthese von methacrylsäure aus auf methacrolein basierenden alkylmethacrylat
RU2019137896A (ru) * 2017-05-09 2021-05-25 Рём ГмбХ Способ окислительной эстерификации альдегидов до сложных эфиров карбоновых кислот
CN110678439B (zh) * 2017-05-25 2022-11-01 罗门哈斯公司 用于制备甲基丙烯醛的方法
BR112019023830B1 (pt) 2017-05-25 2023-02-28 Rohm And Haas Company Processo para preparar metacroleína
EP3587390A1 (de) * 2018-06-26 2020-01-01 Röhm GmbH Verfahren zur herstellung von mma in hohen ausbeuten
EP3613726A1 (en) * 2018-08-21 2020-02-26 Röhm GmbH Continuous process for preparing methacrolein
CN111233667A (zh) * 2018-11-29 2020-06-05 中国科学院大连化学物理研究所 一种改进制备甲基丙烯酸甲酯的方法
KR102417077B1 (ko) * 2019-01-18 2022-07-04 주식회사 엘지화학 메틸메타크릴레이트의 제조 방법
US11414371B2 (en) * 2019-06-28 2022-08-16 Asahi Kasei Kabushiki Kaisha Method for producing methyl methacrylate
EP3786147A1 (de) 2019-08-30 2021-03-03 Röhm GmbH Verfahren zur herstellung von methacrolein aus formaldehyd und propionaldehyd sowie herstellanlage hierfür
EP3786146A1 (de) 2019-08-30 2021-03-03 Röhm GmbH Verfahren zur herstellung von methacrolein aus formaldehyd und propionaldehyd sowie herstellanlage hierfür
EP3798202A1 (de) * 2019-09-25 2021-03-31 Röhm GmbH Verfahren zur aufreinigung von methylmethacrylat von leichtsiedenden komponenten
JP2024520502A (ja) 2021-05-28 2024-05-24 レーム・ゲーエムベーハー アルキル(メタ)アクリレートを製造するための反応器および方法
JP2024520503A (ja) 2021-05-28 2024-05-24 レーム・ゲーエムベーハー アルキルメタクリレートを製造するための反応器および方法
WO2023083869A1 (de) * 2021-11-12 2023-05-19 Röhm Gmbh Verfahren zur eliminierung störender nebenprodukte in der direkten oxidativen veresterung von methacrolein

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3210708A1 (de) * 1982-03-24 1983-10-06 Basf Ag Katalysator und seine verwendung zur herstellung von methylmethacrylat
DE3213681A1 (de) 1982-04-14 1983-10-27 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von (alpha)-alkylacroleinen
SG71815A1 (en) * 1997-07-08 2000-04-18 Asahi Chemical Ind Method of producing methyl methacrylate
JP3681285B2 (ja) * 1997-07-08 2005-08-10 旭化成ケミカルズ株式会社 メタクリル酸メチルの製造方法
JP4306559B2 (ja) * 2004-08-06 2009-08-05 宇部興産株式会社 メタクロレインの製造方法
CN100368368C (zh) * 2006-02-28 2008-02-13 中国科学院过程工程研究所 一种甲基丙烯酸甲酯生产中甲基丙烯醛的分离方法
EP1994978A1 (en) * 2007-05-25 2008-11-26 Evonik Röhm GmbH Process for preparation of methyl methacrylate by esterification during oxidation
CN101074192A (zh) 2007-06-20 2007-11-21 天津大学 以甲醛为原料制备甲基丙烯酸甲酯的方法
EP2370393B1 (en) * 2008-12-18 2020-02-26 Lucite International UK Limited A methyl methacrylate purification process
KR20140041529A (ko) * 2011-05-11 2014-04-04 아처 다니엘 미드랜드 캄파니 아크릴형 단량체의 제조방법 및 이로부터 제조된 생성물
JP6092221B2 (ja) * 2011-09-16 2017-03-08 エボニック レーム ゲゼルシャフト ミット ベシュレンクテル ハフツングEvonik Roehm GmbH メタクリル酸およびメタクリル酸エステルの製造方法

Also Published As

Publication number Publication date
TW201524948A (zh) 2015-07-01
RU2645214C2 (ru) 2018-02-19
BR112016006509A2 (pt) 2017-08-01
JP2016536277A (ja) 2016-11-24
KR20160061395A (ko) 2016-05-31
EP3049385A1 (de) 2016-08-03
RU2016110762A (ru) 2017-09-28
CN105683148B (zh) 2017-11-24
TWI633082B (zh) 2018-08-21
US9580374B2 (en) 2017-02-28
EP3049385B1 (de) 2018-01-03
CN105683148A (zh) 2016-06-15
BR112016006509B1 (pt) 2021-11-09
US20160200660A1 (en) 2016-07-14
MY192947A (en) 2022-09-19
WO2015043861A1 (de) 2015-04-02
JP6355723B2 (ja) 2018-07-11
KR102282531B1 (ko) 2021-07-27
SA516370808B1 (ar) 2017-05-18

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