SE465932B - Foerfarande foer rening av tallharts genom avlaegsnande av fria fettsyror daeri samt tallharts fritt fraan fria fettsyror erhaallet genom detta foerfarande - Google Patents
Foerfarande foer rening av tallharts genom avlaegsnande av fria fettsyror daeri samt tallharts fritt fraan fria fettsyror erhaallet genom detta foerfarandeInfo
- Publication number
- SE465932B SE465932B SE9001015A SE9001015A SE465932B SE 465932 B SE465932 B SE 465932B SE 9001015 A SE9001015 A SE 9001015A SE 9001015 A SE9001015 A SE 9001015A SE 465932 B SE465932 B SE 465932B
- Authority
- SE
- Sweden
- Prior art keywords
- resin
- acids
- fatty acids
- free
- acid
- Prior art date
Links
- 239000002253 acid Substances 0.000 title claims description 58
- 150000007513 acids Chemical class 0.000 title claims description 37
- 238000000034 method Methods 0.000 title claims description 18
- 235000021588 free fatty acids Nutrition 0.000 title claims description 7
- 238000000746 purification Methods 0.000 title 1
- 229920005989 resin Polymers 0.000 claims description 107
- 239000011347 resin Substances 0.000 claims description 107
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 56
- 229930195729 fatty acid Natural products 0.000 claims description 56
- 239000000194 fatty acid Substances 0.000 claims description 56
- 150000004665 fatty acids Chemical class 0.000 claims description 55
- 235000008331 Pinus X rigitaeda Nutrition 0.000 claims description 30
- 235000011613 Pinus brutia Nutrition 0.000 claims description 30
- 241000018646 Pinus brutia Species 0.000 claims description 30
- 230000032050 esterification Effects 0.000 claims description 24
- 238000005886 esterification reaction Methods 0.000 claims description 24
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 238000004821 distillation Methods 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 239000011261 inert gas Substances 0.000 claims description 4
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000003860 storage Methods 0.000 claims description 3
- 239000003760 tallow Substances 0.000 claims description 3
- 238000009835 boiling Methods 0.000 claims description 2
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- 150000005846 sugar alcohols Polymers 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims 1
- 239000008107 starch Substances 0.000 claims 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 15
- 238000006243 chemical reaction Methods 0.000 description 10
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- 150000002148 esters Chemical class 0.000 description 7
- 239000002994 raw material Substances 0.000 description 7
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
- 238000009826 distribution Methods 0.000 description 4
- 239000011521 glass Substances 0.000 description 4
- 238000000926 separation method Methods 0.000 description 4
- 150000001298 alcohols Chemical class 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- 229910001873 dinitrogen Inorganic materials 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 239000010665 pine oil Substances 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 2
- 238000010276 construction Methods 0.000 description 2
- 239000010408 film Substances 0.000 description 2
- 239000003292 glue Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000007937 lozenge Substances 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 239000005011 phenolic resin Substances 0.000 description 2
- 229920001568 phenolic resin Polymers 0.000 description 2
- 229920005862 polyol Polymers 0.000 description 2
- 150000003077 polyols Chemical class 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- 238000010561 standard procedure Methods 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000003784 tall oil Substances 0.000 description 2
- -1 trinetylolpropane Chemical compound 0.000 description 2
- BTXXTMOWISPQSJ-UHFFFAOYSA-N 4,4,4-trifluorobutan-2-one Chemical compound CC(=O)CC(F)(F)F BTXXTMOWISPQSJ-UHFFFAOYSA-N 0.000 description 1
- BQACOLQNOUYJCE-FYZZASKESA-N Abietic acid Natural products CC(C)C1=CC2=CC[C@]3(C)[C@](C)(CCC[C@@]3(C)C(=O)O)[C@H]2CC1 BQACOLQNOUYJCE-FYZZASKESA-N 0.000 description 1
- 241001164374 Calyx Species 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- QUUCYKKMFLJLFS-UHFFFAOYSA-N Dehydroabietan Natural products CC1(C)CCCC2(C)C3=CC=C(C(C)C)C=C3CCC21 QUUCYKKMFLJLFS-UHFFFAOYSA-N 0.000 description 1
- NFWKVWVWBFBAOV-UHFFFAOYSA-N Dehydroabietic acid Natural products OC(=O)C1(C)CCCC2(C)C3=CC=C(C(C)C)C=C3CCC21 NFWKVWVWBFBAOV-UHFFFAOYSA-N 0.000 description 1
- 241000287227 Fringillidae Species 0.000 description 1
- OGRZPYBWAVRXFO-UHFFFAOYSA-N [C].CC(O)CO Chemical compound [C].CC(O)CO OGRZPYBWAVRXFO-UHFFFAOYSA-N 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000004873 anchoring Methods 0.000 description 1
- 210000001367 artery Anatomy 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000004020 conductor Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- NFWKVWVWBFBAOV-MISYRCLQSA-N dehydroabietic acid Chemical compound OC(=O)[C@]1(C)CCC[C@]2(C)C3=CC=C(C(C)C)C=C3CC[C@H]21 NFWKVWVWBFBAOV-MISYRCLQSA-N 0.000 description 1
- 229940118781 dehydroabietic acid Drugs 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 150000002009 diols Chemical class 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000000976 ink Substances 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 210000002445 nipple Anatomy 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000000422 nocturnal effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 235000010603 pastilles Nutrition 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000001577 simple distillation Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09F—NATURAL RESINS; FRENCH POLISH; DRYING-OILS; OIL DRYING AGENTS, i.e. SICCATIVES; TURPENTINE
- C09F1/00—Obtaining purification, or chemical modification of natural resins, e.g. oleo-resins
- C09F1/02—Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE9001015A SE465932B (sv) | 1990-03-21 | 1990-03-21 | Foerfarande foer rening av tallharts genom avlaegsnande av fria fettsyror daeri samt tallharts fritt fraan fria fettsyror erhaallet genom detta foerfarande |
| PCT/SE1991/000209 WO1991014748A1 (fr) | 1990-03-21 | 1991-03-19 | Procede de purification |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE9001015A SE465932B (sv) | 1990-03-21 | 1990-03-21 | Foerfarande foer rening av tallharts genom avlaegsnande av fria fettsyror daeri samt tallharts fritt fraan fria fettsyror erhaallet genom detta foerfarande |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| SE9001015D0 SE9001015D0 (sv) | 1990-03-21 |
| SE9001015A SE9001015A (fr) | 1991-09-22 |
| SE465932B true SE465932B (sv) | 1991-11-18 |
Family
ID=20378936
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SE9001015A SE465932B (sv) | 1990-03-21 | 1990-03-21 | Foerfarande foer rening av tallharts genom avlaegsnande av fria fettsyror daeri samt tallharts fritt fraan fria fettsyror erhaallet genom detta foerfarande |
Country Status (2)
| Country | Link |
|---|---|
| SE (1) | SE465932B (fr) |
| WO (1) | WO1991014748A1 (fr) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2746582B1 (fr) * | 1996-03-28 | 1998-05-22 | Courau Claude | Procede de traitement de la resine, dispositif pour la mise en oeuvre de ce procede et colophane obtenue |
| FI122689B (fi) * | 2003-06-05 | 2012-05-31 | Forchem Oy | Menetelmä uuteaineiden poistamiseksi selluloosamassasta |
| FI123107B (fi) * | 2005-10-31 | 2012-11-15 | Metso Paper Inc | Menetelmä ja laitteisto uuteaineiden poistamiseksi kuitupitoisesta suspensiosta |
| CN100564468C (zh) * | 2007-03-20 | 2009-12-02 | 陆让先 | 一种松脂脂液净化锅及脂液净化工艺过程 |
| CA2895979C (fr) * | 2012-12-21 | 2018-08-07 | Sunpine Ab | Bioraffinage de tallol brut |
| EP3064558B1 (fr) * | 2013-10-29 | 2020-03-11 | Arakawa Chemical Industries, Ltd. | Procédé pour produire une colophane de tall oil et un ester de colophane de tall oil de couleur claire raffinés et colophane de tall oil et ester de colophane de tall oil de couleur claire raffinés obtenus par ledit procédé |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2572035A (en) * | 1948-08-14 | 1951-10-23 | Gen Mills Inc | Plastic tall oil rosin fraction |
| US3859270A (en) * | 1972-02-22 | 1975-01-07 | Azs Corp | Refining of fatty acids |
| US4548746A (en) * | 1984-05-14 | 1985-10-22 | Westvaco Corporation | Rosin pentaerythritol ester preparation improvement |
-
1990
- 1990-03-21 SE SE9001015A patent/SE465932B/sv not_active IP Right Cessation
-
1991
- 1991-03-19 WO PCT/SE1991/000209 patent/WO1991014748A1/fr unknown
Also Published As
| Publication number | Publication date |
|---|---|
| WO1991014748A1 (fr) | 1991-10-03 |
| SE9001015D0 (sv) | 1990-03-21 |
| SE9001015A (fr) | 1991-09-22 |
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| NAL | Patent in force |
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