RU2020107716A - Способ получения кремнийсодержащих гетероциклов - Google Patents
Способ получения кремнийсодержащих гетероциклов Download PDFInfo
- Publication number
- RU2020107716A RU2020107716A RU2020107716A RU2020107716A RU2020107716A RU 2020107716 A RU2020107716 A RU 2020107716A RU 2020107716 A RU2020107716 A RU 2020107716A RU 2020107716 A RU2020107716 A RU 2020107716A RU 2020107716 A RU2020107716 A RU 2020107716A
- Authority
- RU
- Russia
- Prior art keywords
- magnesium
- calcium
- paragraphs
- general formula
- residue
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 claims 13
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims 6
- -1 methylene, ethylene, 1,3-propylene, 2-methyl-1,3-propylene Chemical group 0.000 claims 5
- 125000000217 alkyl group Chemical group 0.000 claims 4
- 229910052739 hydrogen Inorganic materials 0.000 claims 4
- 239000001257 hydrogen Substances 0.000 claims 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims 3
- 239000003054 catalyst Substances 0.000 claims 3
- 125000005842 heteroatom Chemical group 0.000 claims 3
- 239000000203 mixture Substances 0.000 claims 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims 3
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims 2
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 2
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 claims 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims 2
- 125000002947 alkylene group Chemical group 0.000 claims 2
- VSGNNIFQASZAOI-UHFFFAOYSA-L calcium acetate Chemical compound [Ca+2].CC([O-])=O.CC([O-])=O VSGNNIFQASZAOI-UHFFFAOYSA-L 0.000 claims 2
- 238000006243 chemical reaction Methods 0.000 claims 2
- 239000003795 chemical substances by application Substances 0.000 claims 2
- NEHMKBQYUWJMIP-UHFFFAOYSA-N chloromethane Chemical compound ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 claims 2
- 125000000623 heterocyclic group Chemical group 0.000 claims 2
- 150000002431 hydrogen Chemical class 0.000 claims 2
- 239000011968 lewis acid catalyst Substances 0.000 claims 2
- UEGPKNKPLBYCNK-UHFFFAOYSA-L magnesium acetate Chemical compound [Mg+2].CC([O-])=O.CC([O-])=O UEGPKNKPLBYCNK-UHFFFAOYSA-L 0.000 claims 2
- 229910052710 silicon Inorganic materials 0.000 claims 2
- 239000010703 silicon Substances 0.000 claims 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 claims 1
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims 1
- BCZXFFBUYPCTSJ-UHFFFAOYSA-L Calcium propionate Chemical compound [Ca+2].CCC([O-])=O.CCC([O-])=O BCZXFFBUYPCTSJ-UHFFFAOYSA-L 0.000 claims 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims 1
- 239000004593 Epoxy Substances 0.000 claims 1
- NHTMVDHEPJAVLT-UHFFFAOYSA-N Isooctane Chemical compound CC(C)CC(C)(C)C NHTMVDHEPJAVLT-UHFFFAOYSA-N 0.000 claims 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims 1
- YSVZGWAJIHWNQK-UHFFFAOYSA-N [3-(hydroxymethyl)-2-bicyclo[2.2.1]heptanyl]methanol Chemical compound C1CC2C(CO)C(CO)C1C2 YSVZGWAJIHWNQK-UHFFFAOYSA-N 0.000 claims 1
- CIUQDSCDWFSTQR-UHFFFAOYSA-N [C]1=CC=CC=C1 Chemical compound [C]1=CC=CC=C1 CIUQDSCDWFSTQR-UHFFFAOYSA-N 0.000 claims 1
- 239000000654 additive Substances 0.000 claims 1
- 230000000996 additive effect Effects 0.000 claims 1
- 239000002318 adhesion promoter Substances 0.000 claims 1
- 125000003277 amino group Chemical group 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- 150000005840 aryl radicals Chemical class 0.000 claims 1
- 239000011230 binding agent Substances 0.000 claims 1
- 229910052791 calcium Inorganic materials 0.000 claims 1
- 239000011575 calcium Substances 0.000 claims 1
- 235000011092 calcium acetate Nutrition 0.000 claims 1
- 239000001639 calcium acetate Substances 0.000 claims 1
- 229960005147 calcium acetate Drugs 0.000 claims 1
- 235000010237 calcium benzoate Nutrition 0.000 claims 1
- 239000004301 calcium benzoate Substances 0.000 claims 1
- RCPKXZJUDJSTTM-UHFFFAOYSA-L calcium;2,2,2-trifluoroacetate Chemical compound [Ca+2].[O-]C(=O)C(F)(F)F.[O-]C(=O)C(F)(F)F RCPKXZJUDJSTTM-UHFFFAOYSA-L 0.000 claims 1
- URRFTBGSJHOMEG-UHFFFAOYSA-L calcium;2,2-difluoroacetate Chemical compound [Ca+2].[O-]C(=O)C(F)F.[O-]C(=O)C(F)F URRFTBGSJHOMEG-UHFFFAOYSA-L 0.000 claims 1
- GFQBEGBGISQEDF-UHFFFAOYSA-L calcium;2,2-dimethylpropanoate Chemical compound [Ca+2].CC(C)(C)C([O-])=O.CC(C)(C)C([O-])=O GFQBEGBGISQEDF-UHFFFAOYSA-L 0.000 claims 1
- BVTQVYBMHFSYPL-UHFFFAOYSA-L calcium;2-methylpropanoate Chemical compound [Ca+2].CC(C)C([O-])=O.CC(C)C([O-])=O BVTQVYBMHFSYPL-UHFFFAOYSA-L 0.000 claims 1
- WUGPBVBHNMMSPD-UHFFFAOYSA-L calcium;cyclohexanecarboxylate Chemical compound [Ca+2].[O-]C(=O)C1CCCCC1.[O-]C(=O)C1CCCCC1 WUGPBVBHNMMSPD-UHFFFAOYSA-L 0.000 claims 1
- HZQXCUSDXIKLGS-UHFFFAOYSA-L calcium;dibenzoate;trihydrate Chemical compound O.O.O.[Ca+2].[O-]C(=O)C1=CC=CC=C1.[O-]C(=O)C1=CC=CC=C1 HZQXCUSDXIKLGS-UHFFFAOYSA-L 0.000 claims 1
- QKIIAXWPNQIENK-UHFFFAOYSA-L calcium;methyl carbonate Chemical compound [Ca+2].COC([O-])=O.COC([O-])=O QKIIAXWPNQIENK-UHFFFAOYSA-L 0.000 claims 1
- FOCAUTSVDIKZOP-UHFFFAOYSA-M chloroacetate Chemical compound [O-]C(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-M 0.000 claims 1
- 229940089960 chloroacetate Drugs 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 125000000753 cycloalkyl group Chemical group 0.000 claims 1
- JVSWJIKNEAIKJW-UHFFFAOYSA-N dimethyl-hexane Natural products CCCCCC(C)C JVSWJIKNEAIKJW-UHFFFAOYSA-N 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
- 239000000835 fiber Substances 0.000 claims 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims 1
- 229940069446 magnesium acetate Drugs 0.000 claims 1
- 235000011285 magnesium acetate Nutrition 0.000 claims 1
- 239000011654 magnesium acetate Substances 0.000 claims 1
- PJJZFXPJNUVBMR-UHFFFAOYSA-L magnesium benzoate Chemical compound [Mg+2].[O-]C(=O)C1=CC=CC=C1.[O-]C(=O)C1=CC=CC=C1 PJJZFXPJNUVBMR-UHFFFAOYSA-L 0.000 claims 1
- CQQJGTPWCKCEOQ-UHFFFAOYSA-L magnesium dipropionate Chemical compound [Mg+2].CCC([O-])=O.CCC([O-])=O CQQJGTPWCKCEOQ-UHFFFAOYSA-L 0.000 claims 1
- WNBKPRWWMIPBSH-UHFFFAOYSA-L magnesium;2,2,2-trifluoroacetate Chemical compound [Mg+2].[O-]C(=O)C(F)(F)F.[O-]C(=O)C(F)(F)F WNBKPRWWMIPBSH-UHFFFAOYSA-L 0.000 claims 1
- CBUZSVKDOHZQRF-UHFFFAOYSA-L magnesium;2,2-dimethylpropanoate Chemical compound [Mg+2].CC(C)(C)C([O-])=O.CC(C)(C)C([O-])=O CBUZSVKDOHZQRF-UHFFFAOYSA-L 0.000 claims 1
- LFDKGAGSXQRVIR-UHFFFAOYSA-L magnesium;2-fluoroacetate Chemical compound [Mg+2].[O-]C(=O)CF.[O-]C(=O)CF LFDKGAGSXQRVIR-UHFFFAOYSA-L 0.000 claims 1
- VDUQUWCVENWCNL-UHFFFAOYSA-L magnesium;2-methylpropanoate Chemical compound [Mg+2].CC(C)C([O-])=O.CC(C)C([O-])=O VDUQUWCVENWCNL-UHFFFAOYSA-L 0.000 claims 1
- HQILXKLDWMKFEC-UHFFFAOYSA-L magnesium;cyclohexanecarboxylate Chemical compound [Mg+2].[O-]C(=O)C1CCCCC1.[O-]C(=O)C1CCCCC1 HQILXKLDWMKFEC-UHFFFAOYSA-L 0.000 claims 1
- CHKVEDLTACTUAS-UHFFFAOYSA-L magnesium;methyl carbonate Chemical compound [Mg+2].COC([O-])=O.COC([O-])=O CHKVEDLTACTUAS-UHFFFAOYSA-L 0.000 claims 1
- WCYWZMWISLQXQU-UHFFFAOYSA-N methyl Chemical compound [CH3] WCYWZMWISLQXQU-UHFFFAOYSA-N 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- 125000000325 methylidene group Chemical group [H]C([H])=* 0.000 claims 1
- 239000000178 monomer Substances 0.000 claims 1
- 238000005580 one pot reaction Methods 0.000 claims 1
- 229920000642 polymer Polymers 0.000 claims 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims 1
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims 1
- JOYRKODLDBILNP-UHFFFAOYSA-N urethane group Chemical group NC(=O)OCC JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- 239000008096 xylene Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
- C07F7/1872—Preparation; Treatments not provided for in C07F7/20
- C07F7/1892—Preparation; Treatments not provided for in C07F7/20 by reactions not provided for in C07F7/1876 - C07F7/1888
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
- C07F7/1872—Preparation; Treatments not provided for in C07F7/20
- C07F7/1876—Preparation; Treatments not provided for in C07F7/20 by reactions involving the formation of Si-C linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP17182575 | 2017-07-21 | ||
| EP17182575.5 | 2017-07-21 | ||
| PCT/EP2018/053739 WO2019015809A1 (en) | 2017-07-21 | 2018-02-15 | PROCESS FOR THE PREPARATION OF HETEROCYCLES CONTAINING SILICON |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2020107716A3 RU2020107716A3 (https=) | 2021-08-23 |
| RU2020107716A true RU2020107716A (ru) | 2021-08-23 |
Family
ID=59501180
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2020107716A RU2020107716A (ru) | 2017-07-21 | 2018-02-15 | Способ получения кремнийсодержащих гетероциклов |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US11306109B2 (https=) |
| EP (1) | EP3655411A1 (https=) |
| JP (1) | JP2020527584A (https=) |
| CA (1) | CA3070493A1 (https=) |
| RU (1) | RU2020107716A (https=) |
| WO (1) | WO2019015809A1 (https=) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2020527640A (ja) * | 2017-07-21 | 2020-09-10 | ヘンケル・アクチェンゲゼルシャフト・ウント・コムパニー・コマンディットゲゼルシャフト・アウフ・アクチェンＨｅｎｋｅｌ ＡＧ ＆ Ｃｏ． ＫＧａＡ | シリル化ポリウレタンおよびその製造方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1143748A1 (ru) | 1983-10-11 | 1985-03-07 | Иркутский институт органической химии СО АН СССР | Способ получени 2,2-диалкил-1,3-диокса-6-(2-оксиалкил)-6-аза-2-силациклооктанов |
| US4794192A (en) | 1987-07-06 | 1988-12-27 | General Electric Company | Cyclic aminoalkylsilanes and their use as adhesion promoters in room temperature vulcanizable polydiorganosiloxane compositions |
| JP5835116B2 (ja) | 2012-06-15 | 2015-12-24 | 信越化学工業株式会社 | アミノ基と保護された水酸基を有する有機ケイ素化合物及びその製造方法 |
| JP2016040233A (ja) * | 2014-08-12 | 2016-03-24 | 信越化学工業株式会社 | ビシクロアミノオルガノキシシラン化合物及びその製造方法 |
| KR101838565B1 (ko) * | 2017-04-28 | 2018-03-14 | 제이에스아이실리콘주식회사 | 알콕시알킬아미노실란 및 에폭시 화합물의 반응에 의한 2-옥사-5-아자-1-실라사이클로옥탄 및 이의 제조방법 |
-
2018
- 2018-02-15 RU RU2020107716A patent/RU2020107716A/ru unknown
- 2018-02-15 CA CA3070493A patent/CA3070493A1/en not_active Abandoned
- 2018-02-15 EP EP18704034.0A patent/EP3655411A1/en active Pending
- 2018-02-15 JP JP2020502700A patent/JP2020527584A/ja active Pending
- 2018-02-15 WO PCT/EP2018/053739 patent/WO2019015809A1/en not_active Ceased
-
2020
- 2020-01-17 US US16/745,609 patent/US11306109B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| JP2020527584A (ja) | 2020-09-10 |
| RU2020107716A3 (https=) | 2021-08-23 |
| WO2019015809A1 (en) | 2019-01-24 |
| CA3070493A1 (en) | 2019-01-24 |
| EP3655411A1 (en) | 2020-05-27 |
| US11306109B2 (en) | 2022-04-19 |
| US20200148708A1 (en) | 2020-05-14 |
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