RU2018118547A - Устойчивое к щелочам покрытие для легких металлов, в частности алюминия - Google Patents

Устойчивое к щелочам покрытие для легких металлов, в частности алюминия Download PDF

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RU2018118547A
RU2018118547A RU2018118547A RU2018118547A RU2018118547A RU 2018118547 A RU2018118547 A RU 2018118547A RU 2018118547 A RU2018118547 A RU 2018118547A RU 2018118547 A RU2018118547 A RU 2018118547A RU 2018118547 A RU2018118547 A RU 2018118547A
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light metal
aluminum
alkyl
substrate
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RU2018118547A3 (ru
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Этругрул АРПАДЖ
Хайке ШНАЙДЕР
Гюнтер ХОЙЕР
Ральф КОКЛЕР
Сандра АРЕНД
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ИПиДжи (ЭНДЖИНИЭРД НАНОПРОДАКТС ДЖЕРМАНИ) АГ
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D1/00—Processes for applying liquids or other fluent materials
    • B05D1/02—Processes for applying liquids or other fluent materials performed by spraying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
    • B05D3/02—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by baking
    • B05D3/0254—After-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D7/00—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
    • B05D7/14—Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials to metal, e.g. car bodies
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04—Polyurethanes
    • C09D175/06—Polyurethanes from polyesters
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D4/00—Coating compositions, e.g. paints, varnishes or lacquers, based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; Coating compositions, based on monomers of macromolecular compounds of groups C09D183/00 - C09D183/16
    • C09D4/06—Organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond in combination with a macromolecular compound other than an unsaturated polymer of groups C09D159/00 - C09D187/00
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/02—Emulsion paints including aerosols
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08—Anti-corrosive paints
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/1208—Oxides, e.g. ceramics
    • C23C18/1216—Metal oxides
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/122—Inorganic polymers, e.g. silanes, polysilazanes, polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1229—Composition of the substrate
    • C23C18/1241—Metallic substrates
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125—Process of deposition of the inorganic material
    • C23C18/1254—Sol or sol-gel processing
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
    • C25D11/02—Anodisation
    • C25D11/04—Anodisation of aluminium or alloys based thereon
    • C25D11/16—Pretreatment, e.g. desmutting
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
    • C25D11/02—Anodisation
    • C25D11/04—Anodisation of aluminium or alloys based thereon
    • C25D11/18—After-treatment, e.g. pore-sealing
    • C25D11/24—Chemical after-treatment
    • C25D11/246—Chemical after-treatment for sealing layers
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
    • C25D11/02—Anodisation
    • C25D11/04—Anodisation of aluminium or alloys based thereon
    • C25D11/06—Anodisation of aluminium or alloys based thereon characterised by the electrolytes used
    • C25D11/08—Anodisation of aluminium or alloys based thereon characterised by the electrolytes used containing inorganic acids

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  • Chemical Kinetics & Catalysis (AREA)
  • Metallurgy (AREA)
  • General Chemical & Material Sciences (AREA)
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  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Electrochemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Ceramic Engineering (AREA)
  • Paints Or Removers (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Glass Compositions (AREA)
  • Chemical Treatment Of Metals (AREA)

Claims (42)

1. Способ получения покрытой подложки из легкого металла, в частности из алюминия, включающий стадии
а) жидкостного химического нанесения композиции покрытия на подложку из легкого металла и
b) термического отверждения композиции покрытия,
причем композиция покрытия содержит золь-гель-материал, полученный из
А. одного или более частично гидролизованных алкоксисиланов формулы (I)
(R1O)nSiR2 3-nR3 (I),
причем символы и индексы имеют следующие значения:
R1 представляет собой C1-C6-алкил или C1-C10-арил,
R2 представляет собой C1-C4-алкил, C2-C4-алкенил или C2-C4-алкинил, C6-C10-арил, C6-C10-арилалкил или C6-C10-алкиларил,
R3 представляет собой эпоксидную функциональную группу, и
n равен 1, 2 или 3;
B. одного или более алкоксидов металлов формулы (II)
M+(4-m)(X)4-m (II),
причем символы и индексы имеют следующие значения:
M представляет собой металл 3-ей или 4-ой главной или побочной подгруппы с EN<1,5, предпочтительно Al, Zr, Ti или B, особенно предпочтительно Al;
X представляет собой (OR4), галоген, NH3 или первичный, вторичный или третичный (C1-C4)-алкиламин,
R4 представляет собой C1-C6-алкил или C6-C10-арил, и
m равен 0 или 1, предпочтительно 1,
в сочетании с одним или более комплексообразователями из группы 1,3-дикарбонильных соединений;
C. одного или более олигомерных или полимерных полиолов и
D. необязательно, одного или более блокированных полиизоцианатов.
2. Способ по п.1, причем символы и индексы в формуле (I) имеют следующие значения:
R1 представляет собой С1-С4-алкил;
R3 представляет собой 3-глицидилоксипропил, и
n равен 3.
3. Способ по п. 1 или 2, причем соединение (I) выбрано из 3-глицидилоксипропилтриметоксисилана и 3-глицидилоксипропилтриэтоксисилана.
4. Способ по любому из пп. 1-3, причем проводят частичный гидролиз соединения формулы (I) добавлением от 0,13 до 1,5 моля воды, в расчете на 1 моль соединения (I).
5. Способ по любому из пп. 1-4, причем символы и индексы в формуле (II) имеют следующие значения:
M представляет собой Al, Zr, Ti или B;
X представляет собой OR4;
R4 представляет собой C1-C6-алкил, и
m равен 0 или 1.
6. Способ по любому из пп. 1-5, причем соединение (II) представляет собой трис-втор-бутоксид алюминия.
7. Способ по любому из пп. 1-6, причем комплексообразователь компонента В выбран из ацетилацетона и этилацетоацетата.
8. Способ по любому из пп. 1-7, причем в качестве компонента С используют разветвленный сложный полиэфирполиол.
9. Способ по любому из пп. 1-8, причем компонент D присутствует, и в качестве компонента D используют один или более блокированных полиизоцианатов на основе изофорондиизоцианата или гексаметилендиизоцианата.
10. Способ по любому из пп. 1-9, причем жидкостное химическое нанесение на стадии а) выполняют напылением.
11. Способ по любому из пп. 1-10, причем термическое отверждение на стадии b) выполняют при температуре в диапазоне от 130°С до 200°С.
12. Способ по любому из пп. 1-11, причем подложка из легкого металла, в частности алюминиевая подложка, представляет собой подножку или молдинг.
13. Подложка из легкого металла, в частности алюминиевая подложка, покрытая способом по любому из пп. 1-11.
14. Подложка из легкого металла, покрытая композицией покрытия, описанной в любом из пп. 1-9.
15. Применение композиции покрытия, описанной в любом из пп. 1-9, для нанесения покрытия на подложки из легких металлов, в частности алюминиевые подложки.
RU2018118547A 2015-10-22 2016-10-21 Устойчивое к щелочам покрытие для легких металлов, в частности алюминия RU2719888C2 (ru)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP15191132 2015-10-22
EP15191132.8 2015-10-22
PCT/EP2016/001745 WO2017067666A1 (de) 2015-10-22 2016-10-21 Alkaliresistente beschichtung für leichtmetalle, insbesondere aluminium

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RU2018118547A3 RU2018118547A3 (ru) 2020-02-14
RU2719888C2 RU2719888C2 (ru) 2020-04-23

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US (1) US11407903B2 (ru)
EP (1) EP3365476B1 (ru)
DK (1) DK3365476T3 (ru)
ES (1) ES2754591T3 (ru)
HR (1) HRP20191906T1 (ru)
HU (1) HUE046287T2 (ru)
PL (1) PL3365476T3 (ru)
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US10184054B2 (en) * 2016-06-07 2019-01-22 Raytheon Company Coating for the mitigation of metal whiskers
RS63860B1 (sr) 2020-02-20 2023-01-31 Epg F Ukrasna i zaštitna supstanca obloge za supstrate metala, stakla i plastike

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DE4338361A1 (de) 1993-11-10 1995-05-11 Inst Neue Mat Gemein Gmbh Verfahren zur Herstellung von Zusammensetzungen auf der Basis von Epoxidgruppen-haltigen Silanen
DE102004008772A1 (de) * 2004-02-23 2005-09-08 Institut für Neue Materialien Gemeinnützige GmbH Abriebbeständige und alkalibeständige Beschichtungen oder Formkörper mit Niedrigenergieoberfläche
US20080127859A1 (en) * 2004-11-10 2008-06-05 Thomas Kolberg Method for Coating Metallic Surfaces with an Aqueous Multi-Component Composition
DE102007003761B4 (de) * 2007-01-19 2016-01-28 Airbus Operations Gmbh Beschichtete Substrate mit heterogenen Oberflächeneigenschaften
DE102008026923A1 (de) * 2008-06-05 2009-12-10 Henniges Automotive Gmbh & Co. Kg Verfahren zur Anordnung und Befestigung einer Zierleiste im Bereich eines Fensters eines Kraftfahrzeugs
DE102008063160A1 (de) 2008-12-24 2010-07-01 Epg (Engineered Nanoproducts Germany) Ag Alkalibeständige, abriebfeste und spülmaschinenfeste Beschichtung auf einem Substrat
DE102012022731A1 (de) 2012-11-21 2014-05-22 Epg (Engineered Nanoproducts Germany) Ag Hochabriebfeste Antikalkschichten mit hoher chemischer Beständigkeit
DE102013017217A1 (de) 2013-10-17 2015-04-23 Hsm Techconsult Gmbh Beschichtete optische Formkörper aus transparenten Substraten und Verfahren zu ihrer Herstellung und zu ihrer Verwendung.

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US20180305557A1 (en) 2018-10-25
WO2017067666A1 (de) 2017-04-27
PL3365476T3 (pl) 2020-05-18
US11407903B2 (en) 2022-08-09
DK3365476T3 (da) 2019-11-04
HUE046287T2 (hu) 2020-02-28
PT3365476T (pt) 2019-11-06
RU2018118547A3 (ru) 2020-02-14
TWI751984B (zh) 2022-01-11
ES2754591T3 (es) 2020-04-20
EP3365476A1 (de) 2018-08-29
EP3365476B1 (de) 2019-07-31
HRP20191906T1 (hr) 2020-02-07
TW201728709A (zh) 2017-08-16

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