RU2014112447A - OIL WASTE PROCESSING METHOD - Google Patents

OIL WASTE PROCESSING METHOD Download PDF

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Publication number
RU2014112447A
RU2014112447A RU2014112447/05A RU2014112447A RU2014112447A RU 2014112447 A RU2014112447 A RU 2014112447A RU 2014112447/05 A RU2014112447/05 A RU 2014112447/05A RU 2014112447 A RU2014112447 A RU 2014112447A RU 2014112447 A RU2014112447 A RU 2014112447A
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RU
Russia
Prior art keywords
liquid hydrocarbons
reactor
water
gas
flue gases
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Application number
RU2014112447/05A
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Russian (ru)
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RU2566407C9 (en
RU2566407C1 (en
Inventor
Алексей Сергеевич Градов
Евгений Сергеевич Сусеков
Original Assignee
Общество С Ограниченной Ответственностью "Научно-Производственное Объединение Инноватех"
Алексей Сергеевич Градов
Евгений Сергеевич Сусеков
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Application filed by Общество С Ограниченной Ответственностью "Научно-Производственное Объединение Инноватех", Алексей Сергеевич Градов, Евгений Сергеевич Сусеков filed Critical Общество С Ограниченной Ответственностью "Научно-Производственное Объединение Инноватех"
Priority to RU2014112447/05A priority Critical patent/RU2566407C9/en
Priority to PCT/RU2015/000186 priority patent/WO2015152768A1/en
Publication of RU2014112447A publication Critical patent/RU2014112447A/en
Application granted granted Critical
Publication of RU2566407C1 publication Critical patent/RU2566407C1/en
Publication of RU2566407C9 publication Critical patent/RU2566407C9/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G9/00—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G15/00—Cracking of hydrocarbon oils by electric means, electromagnetic or mechanical vibrations, by particle radiation or with gases superheated in electric arcs
    • C10G15/08—Cracking of hydrocarbon oils by electric means, electromagnetic or mechanical vibrations, by particle radiation or with gases superheated in electric arcs by electric means or by electromagnetic or mechanical vibrations
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G31/00—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for
    • C10G31/06—Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for by heating, cooling, or pressure treatment
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G33/00—Dewatering or demulsification of hydrocarbon oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G51/00—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more cracking processes only
    • C10G51/02—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more cracking processes only plural serial stages only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G55/00—Treatment of hydrocarbon oils, in the absence of hydrogen, by at least one refining process and at least one cracking process
    • C10G55/02—Treatment of hydrocarbon oils, in the absence of hydrogen, by at least one refining process and at least one cracking process plural serial stages only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G55/00—Treatment of hydrocarbon oils, in the absence of hydrogen, by at least one refining process and at least one cracking process
    • C10G55/02—Treatment of hydrocarbon oils, in the absence of hydrogen, by at least one refining process and at least one cracking process plural serial stages only
    • C10G55/04—Treatment of hydrocarbon oils, in the absence of hydrogen, by at least one refining process and at least one cracking process plural serial stages only including at least one thermal cracking step
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G5/00—Incineration of waste; Incinerator constructions; Details, accessories or control therefor
    • F23G5/006—General arrangement of incineration plant, e.g. flow sheets
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G5/00—Incineration of waste; Incinerator constructions; Details, accessories or control therefor
    • F23G5/008—Incineration of waste; Incinerator constructions; Details, accessories or control therefor adapted for burning two or more kinds, e.g. liquid and solid, of waste being fed through separate inlets
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G5/00—Incineration of waste; Incinerator constructions; Details, accessories or control therefor
    • F23G5/02—Incineration of waste; Incinerator constructions; Details, accessories or control therefor with pretreatment
    • F23G5/027—Incineration of waste; Incinerator constructions; Details, accessories or control therefor with pretreatment pyrolising or gasifying stage
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G5/00—Incineration of waste; Incinerator constructions; Details, accessories or control therefor
    • F23G5/02—Incineration of waste; Incinerator constructions; Details, accessories or control therefor with pretreatment
    • F23G5/04—Incineration of waste; Incinerator constructions; Details, accessories or control therefor with pretreatment drying
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F23—COMBUSTION APPARATUS; COMBUSTION PROCESSES
    • F23G—CREMATION FURNACES; CONSUMING WASTE PRODUCTS BY COMBUSTION
    • F23G7/00—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals
    • F23G7/05—Incinerators or other apparatus for consuming industrial waste, e.g. chemicals of waste oils

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Electromagnetism (AREA)
  • Processing Of Solid Wastes (AREA)
  • Gasification And Melting Of Waste (AREA)

Abstract

1. Способ переработки нефтяных отходов, включающий подачу отходов в реактор, обогрев реактора высокотемпературными дымовыми газами, подачу перегретого водяного пара в реактор, отделение горючего газа от жидких углеводородов и пара путем охлаждения в теплообменнике, разделение жидких углеводородов и воды, использование горючего газа и жидких углеводородов для производства высокотемпературных дымовых газов, вывод из реактора твердого остатка, отличающийся тем, что производство высокотемпературных дымовых газов осуществляют путем совместного сжигания горючих газов, жидких углеводородов и воды, при этом подачу водяного пара в реактор осуществляют в смеси с высокотемпературными дымовыми газами при массовом соотношении 1:(0,1÷0,5), в теплообменнике горючие газы, жидкие углеводороды и водяной пар охлаждают до температуры 20÷100°C путем теплообмена с теплоносителем, который далее используют для сушки исходных отходов, причем жидкие углеводороды отделяют от воды частично и устанавливают массовое соотношение жидких углеводородов и воды в смеси в пределах 1:(0,1÷4,0).2. Способ переработки нефтяных отходов по п.1, отличающийся тем, что твердый остаток выводят из реактора при температуре 400÷600°C и подают в газогенератор, в котором получают генераторный газ, сжигают данный газ, а продукты сгорания используют для обогрева реактора.3. Способ переработки нефтяных отходов по пп.1 и 2, отличающийся тем, что смесь воды и жидких углеводородов подвергают кавитационному воздействию путем наложения ультразвука с частотой в пределах 20÷200 кГц и интенсивностью колебаний 1,0÷5,0 Вт/см.1. A method of processing oil waste, including supplying waste to the reactor, heating the reactor with high temperature flue gases, supplying superheated water vapor to the reactor, separating combustible gas from liquid hydrocarbons and steam by cooling in a heat exchanger, separating liquid hydrocarbons and water, using combustible gas and liquid hydrocarbons for the production of high temperature flue gases, the conclusion of the solid residue from the reactor, characterized in that the production of high temperature flue gases is carried out by burning combustible gases, liquid hydrocarbons and water, while the steam is supplied to the reactor in a mixture with high-temperature flue gases at a mass ratio of 1: (0.1 ÷ 0.5), in the heat exchanger combustible gases, liquid hydrocarbons and water vapor are cooled to a temperature of 20 ÷ 100 ° C by heat exchange with a coolant, which is then used to dry the initial waste, moreover, liquid hydrocarbons are partially separated from water and the mass ratio of liquid hydrocarbons and water in the mixture is set within 1: (0.1 ÷ 4.0) .2. The method of processing oil waste according to claim 1, characterized in that the solid residue is removed from the reactor at a temperature of 400 ÷ 600 ° C and fed to the gas generator, in which the generating gas is obtained, this gas is burned, and the combustion products are used to heat the reactor. A method of processing oil waste according to claims 1 and 2, characterized in that the mixture of water and liquid hydrocarbons is subjected to cavitation by applying ultrasound with a frequency in the range of 20 ÷ 200 kHz and an oscillation intensity of 1.0 ÷ 5.0 W / cm.

Claims (3)

1. Способ переработки нефтяных отходов, включающий подачу отходов в реактор, обогрев реактора высокотемпературными дымовыми газами, подачу перегретого водяного пара в реактор, отделение горючего газа от жидких углеводородов и пара путем охлаждения в теплообменнике, разделение жидких углеводородов и воды, использование горючего газа и жидких углеводородов для производства высокотемпературных дымовых газов, вывод из реактора твердого остатка, отличающийся тем, что производство высокотемпературных дымовых газов осуществляют путем совместного сжигания горючих газов, жидких углеводородов и воды, при этом подачу водяного пара в реактор осуществляют в смеси с высокотемпературными дымовыми газами при массовом соотношении 1:(0,1÷0,5), в теплообменнике горючие газы, жидкие углеводороды и водяной пар охлаждают до температуры 20÷100°C путем теплообмена с теплоносителем, который далее используют для сушки исходных отходов, причем жидкие углеводороды отделяют от воды частично и устанавливают массовое соотношение жидких углеводородов и воды в смеси в пределах 1:(0,1÷4,0).1. A method of processing oil waste, including supplying waste to the reactor, heating the reactor with high temperature flue gases, supplying superheated water vapor to the reactor, separating combustible gas from liquid hydrocarbons and steam by cooling in a heat exchanger, separating liquid hydrocarbons and water, using combustible gas and liquid hydrocarbons for the production of high temperature flue gases, the conclusion of the solid residue from the reactor, characterized in that the production of high temperature flue gases is carried out by burning combustible gases, liquid hydrocarbons and water, while the steam is supplied to the reactor in a mixture with high-temperature flue gases at a mass ratio of 1: (0.1 ÷ 0.5), in the heat exchanger combustible gases, liquid hydrocarbons and water vapor are cooled to a temperature of 20 ÷ 100 ° C by heat exchange with a coolant, which is then used to dry the initial waste, moreover, liquid hydrocarbons are partially separated from water and the mass ratio of liquid hydrocarbons and water in the mixture is set within 1: (0.1 ÷ 4.0) . 2. Способ переработки нефтяных отходов по п.1, отличающийся тем, что твердый остаток выводят из реактора при температуре 400÷600°C и подают в газогенератор, в котором получают генераторный газ, сжигают данный газ, а продукты сгорания используют для обогрева реактора.2. The method of processing oil waste according to claim 1, characterized in that the solid residue is removed from the reactor at a temperature of 400 ÷ 600 ° C and fed to the gas generator, in which the generator gas is obtained, this gas is burned, and the combustion products are used to heat the reactor. 3. Способ переработки нефтяных отходов по пп.1 и 2, отличающийся тем, что смесь воды и жидких углеводородов подвергают кавитационному воздействию путем наложения ультразвука с частотой в пределах 20÷200 кГц и интенсивностью колебаний 1,0÷5,0 Вт/см2.3. A method of processing oil waste according to claims 1 and 2, characterized in that the mixture of water and liquid hydrocarbons is subjected to cavitation by applying ultrasound with a frequency in the range of 20 ÷ 200 kHz and an oscillation intensity of 1.0 ÷ 5.0 W / cm 2 .
RU2014112447/05A 2014-03-31 2014-03-31 Method of oil wastes recycling RU2566407C9 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
RU2014112447/05A RU2566407C9 (en) 2014-03-31 2014-03-31 Method of oil wastes recycling
PCT/RU2015/000186 WO2015152768A1 (en) 2014-03-31 2015-03-27 Waste oil processing method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU2014112447/05A RU2566407C9 (en) 2014-03-31 2014-03-31 Method of oil wastes recycling

Publications (3)

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RU2014112447A true RU2014112447A (en) 2015-10-10
RU2566407C1 RU2566407C1 (en) 2015-10-27
RU2566407C9 RU2566407C9 (en) 2016-01-20

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WO (1) WO2015152768A1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2627784C1 (en) * 2016-05-04 2017-08-11 Общество с ограниченной ответственностью "ЭКОЛОГИЧЕСКАЯ ТОПЛИВНО-ЭНЕРГЕТИЧЕСКАЯ КОМПАНИЯ" Device for oil wastes recycling

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU427978A1 (en) * 1972-06-28 1974-05-15 METHOD FOR OBTAINING UNLIMITED HYDROCARBONS
SU917493A1 (en) * 1980-06-19 1985-06-15 Всесоюзный Ордена Трудового Красного Знамени Научно-Исследовательский Институт Железнодорожного Транспорта Installation for thermal decontamination of petroleum slimes
KR0171501B1 (en) * 1996-08-28 1999-03-20 이성래 Apparatus and process for reclaiming waste oil
RU2161176C1 (en) * 2000-06-28 2000-12-27 Закрытое акционерное общество "ПОМ-ТЭК" Method and installation for processing waste petroleum products
EA200200475A1 (en) * 2001-12-07 2002-12-26 Гамлет Алиевич Мирзоев METHOD OF PROCESSING MIXED OIL WASTE AND INSTALLATION FOR ITS IMPLEMENTATION

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RU2566407C9 (en) 2016-01-20
RU2566407C1 (en) 2015-10-27

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