RU2011112045A - Способ соединения деталей из углеродного материала пайкой тугоплавким припоем - Google Patents
Способ соединения деталей из углеродного материала пайкой тугоплавким припоем Download PDFInfo
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Abstract
1. Способ соединения по меньшей мере двух деталей из углеродного материала с размером частиц менее 10 мкм, включающий, по меньшей мере, следующие шаги: ! a) размещение соединяемых деталей из углеродного материала и кремниевого элемента, в частности, имеющего вид полоски кремния, таким образом, что указанный элемент находится между указанными деталями, и ! b) выдерживание сборной детали, сцепленной из указанных элементов, под давлением с нагревом в инертной атмосфере до температуры выше 1410°С, что ведет к расплавлению кремния и формированию шва, содержащего по меньшей мере одну перемычку из карбида кремния на границе раздела указанных деталей, и ! c) нагрев сборной детали, полученной после шага b), до температуры, превышающей температуру шага b) с расходованием всего расплавленного кремния и формирования шва из карбида кремния по всей поверхности раздела указанных деталей из углеродного материала. ! 2. Способ по п.1, отличающийся тем, что припой, полученный после шага с), совершенно не содержит остаточного кремния в твердом состоянии. ! 3. Способ по любому из пп.1 или 2, в котором детали из углеродного материала имеют открытую пористость от 0% до 40% по объему. ! 4. Способ по любому из пп.1 или 2, в котором размер частиц углеродного материала составляет от 1 мкм до 5 мкм. ! 5. Способ по любому из пп.1 или 2, в котором шов, образовавшийся на границе раздела двух соединяемых деталей, имеет толщину от 10 мкм до 40 мкм, предпочтительно от 20 мкм до 30 мкм. ! 6. Способ по любому из пп.1 или 2, в котором шаг b) включает в себя нагрев в инертной атмосфере при температуре от 1410°С до 1600°С, предпочтительно от 1450°С до 1550°С, в течение предпочтительно от 10 мин до 1 �
Claims (8)
1. Способ соединения по меньшей мере двух деталей из углеродного материала с размером частиц менее 10 мкм, включающий, по меньшей мере, следующие шаги:
a) размещение соединяемых деталей из углеродного материала и кремниевого элемента, в частности, имеющего вид полоски кремния, таким образом, что указанный элемент находится между указанными деталями, и
b) выдерживание сборной детали, сцепленной из указанных элементов, под давлением с нагревом в инертной атмосфере до температуры выше 1410°С, что ведет к расплавлению кремния и формированию шва, содержащего по меньшей мере одну перемычку из карбида кремния на границе раздела указанных деталей, и
c) нагрев сборной детали, полученной после шага b), до температуры, превышающей температуру шага b) с расходованием всего расплавленного кремния и формирования шва из карбида кремния по всей поверхности раздела указанных деталей из углеродного материала.
2. Способ по п.1, отличающийся тем, что припой, полученный после шага с), совершенно не содержит остаточного кремния в твердом состоянии.
3. Способ по любому из пп.1 или 2, в котором детали из углеродного материала имеют открытую пористость от 0% до 40% по объему.
4. Способ по любому из пп.1 или 2, в котором размер частиц углеродного материала составляет от 1 мкм до 5 мкм.
5. Способ по любому из пп.1 или 2, в котором шов, образовавшийся на границе раздела двух соединяемых деталей, имеет толщину от 10 мкм до 40 мкм, предпочтительно от 20 мкм до 30 мкм.
6. Способ по любому из пп.1 или 2, в котором шаг b) включает в себя нагрев в инертной атмосфере при температуре от 1410°С до 1600°С, предпочтительно от 1450°С до 1550°С, в течение предпочтительно от 10 мин до 1 ч или даже от 20 до 40 мин.
7. Способ по любому из пп.1 или 2, в котором шаг b) выполняют при температуре от 1410°С до 1500°С, предпочтительно от 1430°С до 1500°С в течение предпочтительно от 10 мин до 1 ч или даже от 10 до 40 мин, и шаг с) выполняют при температуре от 1500°С до 1750°С, предпочтительно от 1600°С до 1700°С в течение предпочтительно от 3 до 8 ч или даже от 3 до 6 ч.
8. Детали, соединенные швом из карбида кремния, проходящим по всей поверхности раздела указанных деталей, полученным способом, раскрытым в пп.1-7.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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FR0855970 | 2008-09-05 | ||
FR0855970A FR2935622B1 (fr) | 2008-09-05 | 2008-09-05 | Procede d'assemblage de pieces carbonees par brasage refractaire |
PCT/FR2009/051665 WO2010026341A2 (fr) | 2008-09-05 | 2009-09-03 | Procede d'assemblage de pieces carbonees par brasage refractaire |
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RU2011112045A true RU2011112045A (ru) | 2012-10-10 |
RU2480434C2 RU2480434C2 (ru) | 2013-04-27 |
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RU2011112045/03A RU2480434C2 (ru) | 2008-09-05 | 2009-09-03 | Способ соединения деталей из углеродного материала пайкой тугоплавким припоем |
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US (1) | US8956481B2 (ru) |
EP (1) | EP2326606B1 (ru) |
JP (1) | JP5654993B2 (ru) |
KR (1) | KR101338256B1 (ru) |
CN (1) | CN102143926B (ru) |
BR (1) | BRPI0919146A2 (ru) |
ES (1) | ES2730075T3 (ru) |
FR (1) | FR2935622B1 (ru) |
RU (1) | RU2480434C2 (ru) |
WO (1) | WO2010026341A2 (ru) |
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CN104220400B (zh) * | 2011-11-29 | 2018-04-03 | 康宁股份有限公司 | 处理陶瓷组件中接头的方法 |
EP2963002A4 (en) * | 2013-02-27 | 2016-10-26 | Kyocera Corp | CERAMICLY CONNECTED BODY AND CHANNEL BODY |
CN103143809B (zh) * | 2013-03-21 | 2016-03-09 | 光驰科技(上海)有限公司 | 一种同时焊接多条焊缝的方法和焊接辅助工具 |
RU2623395C2 (ru) * | 2015-08-11 | 2017-06-26 | Общество с ограниченной ответственностью "Керамические технологии" | Способ соединения деталей из карбида кремния |
FR3045846B1 (fr) * | 2015-12-22 | 2018-09-28 | Centre National De La Recherche Scientifique | Dispositif electro-optique pour la detection de la modification locale d’un champ electrique. |
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US5079195A (en) * | 1988-01-15 | 1992-01-07 | Massachusetts Institute Of Technology | Method of preparing refractory silicon carbide composites and coatings |
US5021107A (en) * | 1988-01-19 | 1991-06-04 | Holko Kenneth H | Process for joining or coating carbon-carbon composite components |
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DE3907913A1 (de) * | 1989-03-11 | 1990-09-27 | Bayer Ag | Graphitkleber und verfahren zur herstellung von klebeverbindungen zwischen graphitteilen |
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JPH07257981A (ja) * | 1994-03-17 | 1995-10-09 | Nippon Steel Corp | 炭素含有耐火物の接合体およびその製造方法 |
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US5972157A (en) * | 1995-11-20 | 1999-10-26 | Alliedsignal Inc. | Joining of rough carbon-carbon composites with high joint strength |
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DE102006009388B4 (de) * | 2006-03-01 | 2009-02-26 | Audi Ag | Vorrichtung zur Silicierung von kohlenstoffhaltigen Werkstoffen und darin durchführbares Verfahren |
JP5322382B2 (ja) * | 2006-11-30 | 2013-10-23 | 株式会社東芝 | セラミックス複合部材とその製造方法 |
-
2008
- 2008-09-05 FR FR0855970A patent/FR2935622B1/fr active Active
-
2009
- 2009-09-03 US US13/062,394 patent/US8956481B2/en not_active Expired - Fee Related
- 2009-09-03 ES ES09741362T patent/ES2730075T3/es active Active
- 2009-09-03 WO PCT/FR2009/051665 patent/WO2010026341A2/fr active Application Filing
- 2009-09-03 BR BRPI0919146A patent/BRPI0919146A2/pt not_active IP Right Cessation
- 2009-09-03 JP JP2011525596A patent/JP5654993B2/ja not_active Expired - Fee Related
- 2009-09-03 EP EP09741362.9A patent/EP2326606B1/fr active Active
- 2009-09-03 RU RU2011112045/03A patent/RU2480434C2/ru not_active IP Right Cessation
- 2009-09-03 KR KR1020117007355A patent/KR101338256B1/ko not_active IP Right Cessation
- 2009-09-03 CN CN200980134950.0A patent/CN102143926B/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP2326606A2 (fr) | 2011-06-01 |
CN102143926A (zh) | 2011-08-03 |
WO2010026341A2 (fr) | 2010-03-11 |
CN102143926B (zh) | 2015-12-02 |
RU2480434C2 (ru) | 2013-04-27 |
BRPI0919146A2 (pt) | 2015-12-08 |
EP2326606B1 (fr) | 2019-04-03 |
ES2730075T3 (es) | 2019-11-08 |
FR2935622B1 (fr) | 2017-02-03 |
KR20110066925A (ko) | 2011-06-17 |
US20110229711A1 (en) | 2011-09-22 |
JP5654993B2 (ja) | 2015-01-14 |
FR2935622A1 (fr) | 2010-03-12 |
KR101338256B1 (ko) | 2013-12-06 |
WO2010026341A3 (fr) | 2010-06-17 |
US8956481B2 (en) | 2015-02-17 |
JP2012501851A (ja) | 2012-01-26 |
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