RU2011112045A - Способ соединения деталей из углеродного материала пайкой тугоплавким припоем - Google Patents

Способ соединения деталей из углеродного материала пайкой тугоплавким припоем Download PDF

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RU2011112045A
RU2011112045A RU2011112045/03A RU2011112045A RU2011112045A RU 2011112045 A RU2011112045 A RU 2011112045A RU 2011112045/03 A RU2011112045/03 A RU 2011112045/03A RU 2011112045 A RU2011112045 A RU 2011112045A RU 2011112045 A RU2011112045 A RU 2011112045A
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parts
carbon material
silicon
temperature
interface
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Жан-Поль ГАРАНДЕ (FR)
Жан-Поль Гаранде
Дени КАМЕЛЬ (FR)
Дени КАМЕЛЬ
Беатрис ДРЕВЕ (FR)
Беатрис ДРЕВЕ
Никола ЭСТАТОПУЛО (FR)
Никола ЭСТАТОПУЛО
Рана ИСРАЭЛЬ (FR)
Рана ИСРАЭЛЬ
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Комиссарья А Л'Энержи Атомик Э Оз Энержи Альтернатив (Fr)
Комиссарья А Л'Энержи Атомик Э Оз Энержи Альтернатив
Энститю Насьональ Политекник Де Гренобль (Fr)
Энститю Насьональ Политекник Де Гренобль
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Abstract

1. Способ соединения по меньшей мере двух деталей из углеродного материала с размером частиц менее 10 мкм, включающий, по меньшей мере, следующие шаги: ! a) размещение соединяемых деталей из углеродного материала и кремниевого элемента, в частности, имеющего вид полоски кремния, таким образом, что указанный элемент находится между указанными деталями, и ! b) выдерживание сборной детали, сцепленной из указанных элементов, под давлением с нагревом в инертной атмосфере до температуры выше 1410°С, что ведет к расплавлению кремния и формированию шва, содержащего по меньшей мере одну перемычку из карбида кремния на границе раздела указанных деталей, и ! c) нагрев сборной детали, полученной после шага b), до температуры, превышающей температуру шага b) с расходованием всего расплавленного кремния и формирования шва из карбида кремния по всей поверхности раздела указанных деталей из углеродного материала. ! 2. Способ по п.1, отличающийся тем, что припой, полученный после шага с), совершенно не содержит остаточного кремния в твердом состоянии. ! 3. Способ по любому из пп.1 или 2, в котором детали из углеродного материала имеют открытую пористость от 0% до 40% по объему. ! 4. Способ по любому из пп.1 или 2, в котором размер частиц углеродного материала составляет от 1 мкм до 5 мкм. ! 5. Способ по любому из пп.1 или 2, в котором шов, образовавшийся на границе раздела двух соединяемых деталей, имеет толщину от 10 мкм до 40 мкм, предпочтительно от 20 мкм до 30 мкм. ! 6. Способ по любому из пп.1 или 2, в котором шаг b) включает в себя нагрев в инертной атмосфере при температуре от 1410°С до 1600°С, предпочтительно от 1450°С до 1550°С, в течение предпочтительно от 10 мин до 1 �

Claims (8)

1. Способ соединения по меньшей мере двух деталей из углеродного материала с размером частиц менее 10 мкм, включающий, по меньшей мере, следующие шаги:
a) размещение соединяемых деталей из углеродного материала и кремниевого элемента, в частности, имеющего вид полоски кремния, таким образом, что указанный элемент находится между указанными деталями, и
b) выдерживание сборной детали, сцепленной из указанных элементов, под давлением с нагревом в инертной атмосфере до температуры выше 1410°С, что ведет к расплавлению кремния и формированию шва, содержащего по меньшей мере одну перемычку из карбида кремния на границе раздела указанных деталей, и
c) нагрев сборной детали, полученной после шага b), до температуры, превышающей температуру шага b) с расходованием всего расплавленного кремния и формирования шва из карбида кремния по всей поверхности раздела указанных деталей из углеродного материала.
2. Способ по п.1, отличающийся тем, что припой, полученный после шага с), совершенно не содержит остаточного кремния в твердом состоянии.
3. Способ по любому из пп.1 или 2, в котором детали из углеродного материала имеют открытую пористость от 0% до 40% по объему.
4. Способ по любому из пп.1 или 2, в котором размер частиц углеродного материала составляет от 1 мкм до 5 мкм.
5. Способ по любому из пп.1 или 2, в котором шов, образовавшийся на границе раздела двух соединяемых деталей, имеет толщину от 10 мкм до 40 мкм, предпочтительно от 20 мкм до 30 мкм.
6. Способ по любому из пп.1 или 2, в котором шаг b) включает в себя нагрев в инертной атмосфере при температуре от 1410°С до 1600°С, предпочтительно от 1450°С до 1550°С, в течение предпочтительно от 10 мин до 1 ч или даже от 20 до 40 мин.
7. Способ по любому из пп.1 или 2, в котором шаг b) выполняют при температуре от 1410°С до 1500°С, предпочтительно от 1430°С до 1500°С в течение предпочтительно от 10 мин до 1 ч или даже от 10 до 40 мин, и шаг с) выполняют при температуре от 1500°С до 1750°С, предпочтительно от 1600°С до 1700°С в течение предпочтительно от 3 до 8 ч или даже от 3 до 6 ч.
8. Детали, соединенные швом из карбида кремния, проходящим по всей поверхности раздела указанных деталей, полученным способом, раскрытым в пп.1-7.
RU2011112045/03A 2008-09-05 2009-09-03 Способ соединения деталей из углеродного материала пайкой тугоплавким припоем RU2480434C2 (ru)

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FR0855970A FR2935622B1 (fr) 2008-09-05 2008-09-05 Procede d'assemblage de pieces carbonees par brasage refractaire
FR0855970 2008-09-05
PCT/FR2009/051665 WO2010026341A2 (fr) 2008-09-05 2009-09-03 Procede d'assemblage de pieces carbonees par brasage refractaire

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RU2480434C2 RU2480434C2 (ru) 2013-04-27

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EP2326606B1 (fr) 2019-04-03
CN102143926A (zh) 2011-08-03
CN102143926B (zh) 2015-12-02
US20110229711A1 (en) 2011-09-22
KR101338256B1 (ko) 2013-12-06
JP2012501851A (ja) 2012-01-26
JP5654993B2 (ja) 2015-01-14
EP2326606A2 (fr) 2011-06-01
WO2010026341A2 (fr) 2010-03-11
FR2935622A1 (fr) 2010-03-12
KR20110066925A (ko) 2011-06-17
ES2730075T3 (es) 2019-11-08
WO2010026341A3 (fr) 2010-06-17
FR2935622B1 (fr) 2017-02-03
US8956481B2 (en) 2015-02-17
BRPI0919146A2 (pt) 2015-12-08
RU2480434C2 (ru) 2013-04-27

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