RU2007125572A - METAL SURFACE TREATMENT COMPOSITION, ACTIVE SURFACE TREATMENT LIQUID, SURFACE TREATMENT METHOD AND SURFACE TREATED METAL MATERIAL - Google Patents

METAL SURFACE TREATMENT COMPOSITION, ACTIVE SURFACE TREATMENT LIQUID, SURFACE TREATMENT METHOD AND SURFACE TREATED METAL MATERIAL Download PDF

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RU2007125572A
RU2007125572A RU2007125572/02A RU2007125572A RU2007125572A RU 2007125572 A RU2007125572 A RU 2007125572A RU 2007125572/02 A RU2007125572/02 A RU 2007125572/02A RU 2007125572 A RU2007125572 A RU 2007125572A RU 2007125572 A RU2007125572 A RU 2007125572A
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acid
surface treatment
metal material
zinc
compound
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RU2007125572/02A
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RU2395622C2 (en
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Масаюки ЙОШИДА (JP)
Масаюки ЙОШИДА
Катсуюки КАВАКАМИ (JP)
Катсуюки КАВАКАМИ
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Хенкель Коммандитгезелльшафт Ауф Акциен (DE)
Хенкель Коммандитгезелльшафт ауф Акциен
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    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/82—After-treatment
    • C23C22/83—Chemical after-treatment
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/34—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 containing fluorides or complex fluorides
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/48—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 not containing phosphates, hexavalent chromium compounds, fluorides or complex fluorides, molybdates, tungstates, vanadates or oxalates
    • C23C22/50—Treatment of iron or alloys based thereon
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/06—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6
    • C23C22/48—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous acidic solutions with pH less than 6 not containing phosphates, hexavalent chromium compounds, fluorides or complex fluorides, molybdates, tungstates, vanadates or oxalates
    • C23C22/53—Treatment of zinc or alloys based thereon
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D5/00—Electroplating characterised by the process; Pretreatment or after-treatment of workpieces
    • C25D5/34—Pretreatment of metallic surfaces to be electroplated
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D9/00—Electrolytic coating other than with metals
    • C25D9/04—Electrolytic coating other than with metals with inorganic materials
    • C25D9/08—Electrolytic coating other than with metals with inorganic materials by cathodic processes
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D9/00—Electrolytic coating other than with metals
    • C25D9/04—Electrolytic coating other than with metals with inorganic materials
    • C25D9/08—Electrolytic coating other than with metals with inorganic materials by cathodic processes
    • C25D9/10—Electrolytic coating other than with metals with inorganic materials by cathodic processes on iron or steel

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Electrochemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Other Surface Treatments For Metallic Materials (AREA)

Claims (15)

1. Водная композиция для обработки поверхности металлов, содержащих железо и/или цинк, включающая приведенные далее компоненты (А):1. An aqueous composition for surface treatment of metals containing iron and / or zinc, including the following components (A): (A) соединение, содержащее по крайней мере один элемент, выбираемый из группы, включающей титан, цирконий, гафний и кремний,(A) a compound containing at least one element selected from the group consisting of titanium, zirconium, hafnium and silicon, (Б) соединение, содержащее иттрий и/или лантанидный элемент и(B) a compound containing yttrium and / or lanthanide element and (B) азотная кислота и/или соединение азотной кислоты,(B) nitric acid and / or a nitric acid compound, при этом отношение общей выраженной в единицах массы концентрации Б, относящейся к названным выше иттрию и/или лантанидным элементам, содержащимся в названной выше компоненте (Б), к общей выраженной в единицах массы концентрации А, относящейся к названным выше элементам, входящим в состав названной выше компоненты (А), или К1=Б/А, лежит в пределах: 0,05≤К1≤50, а отношение общей выраженной в единицах массы концентрации В атомов азота, содержащихся в названной выше компоненте (В) и относящихся к концентрации нитратных ионов, к общей выраженной в единицах массы концентрации А, или К2=В/А, лежит в пределах: 0,01≤К2≤200, и названная выше общая концентрация А, выраженная в единицах массы, лежит в пределах: 10 частей на миллион ≤А≤10000 частей на миллион.the ratio of the total concentration expressed in units of mass of B related to the above yttrium and / or lanthanide elements contained in the above component (B) to the total concentration expressed in units of mass of A related to the above elements included in the named above the component (A), or K1 = B / A, lies in the range: 0.05≤K1≤50, and the ratio of the total expressed in units of mass concentration of nitrogen atoms contained in the above component (B) and related to the concentration of nitrate ions, to the total expressed in e in terms of mass concentration A, or K2 = B / A, lies in the range: 0.01≤K2≤200, and the above total concentration A, expressed in units of mass, lies in the range: 10 parts per million ≤A≤10000 parts per million. 2. Водная композиция для обработки поверхности по п.1, содержащая дополнительно по крайней мере одно фторсодержащее соединение в качестве компоненты (Г).2. The aqueous composition for surface treatment according to claim 1, additionally containing at least one fluorine-containing compound as component (D). 3. Водная композиция для обработки поверхности по п.2, содержащая свободные ионы фтора компоненты Г в концентрации в пределах: 0,001 частей на миллион ≤Г≤300 частей на миллион.3. The aqueous composition for surface treatment according to claim 2, containing free fluorine ions of component G at a concentration in the range of: 0.001 ppm ≤G≤300 ppm. 4. Водная композиция для обработки поверхности по п.1, значение рН которой не превышает 6,0.4. The aqueous composition for surface treatment according to claim 1, the pH of which does not exceed 6.0. 5. Водная композиция для обработки поверхности по п.1, содержащая дополнительно по крайней мере одно соединение, выбираемое из группы, включающей соляную кислоту, серную кислоту, хлорноватую кислоту (HClO3), бромноватую кислоту (HBrO3), азотистую кислоту, марганцевую кислоту (HMnO4), ванадиевую кислоту (VHO3), пероксид водорода, вольфрамовую кислоту, молибденовую кислоту и их соли в концентрации в пределах от 10 до 20000 частей на миллион.5. The aqueous composition for surface treatment according to claim 1, containing additionally at least one compound selected from the group comprising hydrochloric acid, sulfuric acid, perchloric acid (HClO 3 ), bromic acid (HBrO 3 ), nitrous acid, manganese acid (HMnO 4 ), vanadium acid (VHO 3 ), hydrogen peroxide, tungsten acid, molybdenum acid and their salts in a concentration ranging from 10 to 20,000 parts per million. 6. Водная композиция для обработки поверхности по п.1, содержащая дополнительно по крайней мере одно соединение, выбираемое из группы, включающей этилендиаминтетрауксусную кислоту, глюконовую кислоту, гептоглюконовую кислоту, гликолевую кислоту, лимонную кислоту, янтарную кислоту, фумаровую кислоту, аспарагиновую кислоту, винную кислоту, малоновую кислоту, яблочную кислоту, салициловую кислоту и их соли в концентрации в пределах от 1 до 10000 частей на миллион.6. The aqueous surface treatment composition according to claim 1, further comprising at least one compound selected from the group consisting of ethylenediaminetetraacetic acid, gluconic acid, heptogluconic acid, glycolic acid, citric acid, succinic acid, fumaric acid, aspartic acid, tartaric acid acid, malonic acid, malic acid, salicylic acid and their salts in concentrations ranging from 1 to 10,000 ppm. 7. Водная композиция для обработки поверхности по п.1, содержащая дополнительно растворимое в воде полимерное соединение и/или диспергируемое в воде полимерное соединение.7. The aqueous surface treatment composition according to claim 1, further comprising a water-soluble polymer compound and / or a water-dispersible polymer compound. 8. Водная композиция для обработки поверхности по одному из пп.1-7, содержащая дополнительно по крайней мере одно поверхностноактивное вещество, выбираемое из группы, включающей неионогенные поверхностно-активные вещества, анионные поверхностноактивные вещества и катионные поверхностноактивные вещества.8. The aqueous composition for surface treatment according to one of claims 1 to 7, further comprising at least one surfactant selected from the group consisting of nonionic surfactants, anionic surfactants and cationic surfactants. 9. Способ обработки металлических материалов, содержащих железо и/или цинк, включающий процесс контактирования поверхности металлического материала с водной композицией по одному из пп.1-8.9. A method of processing metal materials containing iron and / or zinc, comprising the process of contacting the surface of the metal material with an aqueous composition according to one of claims 1 to 8. 10. Способ по п.9, в соответствии с которым металлический материал, содержащий железо и/или цинк, представлен металлическим материалом, который был очищен в процессе обработки с целью обезжиривания.10. The method according to claim 9, in accordance with which the metal material containing iron and / or zinc, is a metal material that has been cleaned during processing to degrease. 11. Способ по п.9, в соответствии с которым процесс контактирования проводят электролитическим путем с использованием металлического материала, содержащего железо и/или цинк, в качестве катода.11. The method according to claim 9, in accordance with which the contacting process is carried out electrolytically using a metal material containing iron and / or zinc as a cathode. 12. Способ по одному из пп.9-11, в соответствии с которым за процессом контактирования следует обработка металлического материала, содержащего железо и/или цинк, водным раствором, содержащим по крайней мере один элемент, выбираемый из группы, включающей кобальт, никель, олово, медь, титан и цирконий.12. The method according to one of claims 9 to 11, wherein the contacting process is followed by treating the metal material containing iron and / or zinc with an aqueous solution containing at least one element selected from the group consisting of cobalt, nickel, tin, copper, titanium and zirconium. 13. Способ по одному из пп.9-11, в соответствии с которым за процессом контактирования следует обработка металлического материала, содержащего железо и/или цинк, водным раствором, содержащим растворимое в воде полимерное соединение или диспергируемое в воде полимерное соединение.13. The method according to one of claims 9 to 11, wherein the contacting process is followed by treating a metal material containing iron and / or zinc with an aqueous solution containing a water-soluble polymer compound or a water-dispersible polymer compound. 14. Содержащий железо металлический материал с нанесенным на поверхность слоем в виде пленки, образованной на поверхности содержащего железо металлического материала способом по одному из пп.9-13, при этом пленка содержит в связанном состоянии элементы компоненты (А) в количестве более 20 мг/см2.14. The iron-containing metal material with a layer deposited on the surface in the form of a film formed on the surface of the iron-containing metal material by the method according to one of claims 9 to 13, wherein the film contains in a bound state the elements of component (A) in an amount of more than 20 mg / cm 2 . 15. Содержащий цинк металлический материал с нанесенным на поверхность слоем в виде пленки, образованной на поверхности содержащего цинк металлического материала способом по одному из пп.9-13, при этом пленка содержит в связанном состоянии элементы компоненты (А) в количестве более 15 мг/см2. 15. The zinc-containing metal material with a layer deposited on the surface in the form of a film formed on the surface of the zinc-containing metal material by the method according to one of claims 9 to 13, wherein the film contains in a bound state the elements of component (A) in an amount of more than 15 mg / cm 2 .
RU2007125572/02A 2004-12-08 2005-12-02 Composition for treatment of surface of metals, effective liquid for surface treatment, procedure for surface treatment and metal material with treated surface RU2395622C2 (en)

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JP2004356059A JP4242827B2 (en) 2004-12-08 2004-12-08 Metal surface treatment composition, surface treatment liquid, surface treatment method, and surface-treated metal material

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US (1) US20070272900A1 (en)
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JP (1) JP4242827B2 (en)
CN (1) CN101076615B (en)
AU (1) AU2005312758B2 (en)
BR (1) BRPI0518423B1 (en)
CA (1) CA2591214C (en)
ES (1) ES2529318T3 (en)
MX (1) MX2007006729A (en)
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