RO80924B - Procedeu pentru prepararea 2, 3-dihidro-2, 2-dimetil-7-hidroxibenzofuranului - Google Patents
Procedeu pentru prepararea 2, 3-dihidro-2, 2-dimetil-7-hidroxibenzofuranuluiInfo
- Publication number
- RO80924B RO80924B RO102783A RO10278380A RO80924B RO 80924 B RO80924 B RO 80924B RO 102783 A RO102783 A RO 102783A RO 10278380 A RO10278380 A RO 10278380A RO 80924 B RO80924 B RO 80924B
- Authority
- RO
- Romania
- Prior art keywords
- hydroxybenzofuran
- dihydro
- dimethyl
- preparation
- ortho
- Prior art date
Links
- WJGPNUBJBMCRQH-UHFFFAOYSA-N 2,2-dimethyl-2,3-dihydro-1-benzofuran-7-ol Chemical compound C1=CC(O)=C2OC(C)(C)CC2=C1 WJGPNUBJBMCRQH-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- AAXBKJXGVXNSHI-UHFFFAOYSA-N 2-(2-methylprop-2-enoxy)phenol Chemical compound CC(=C)COC1=CC=CC=C1O AAXBKJXGVXNSHI-UHFFFAOYSA-N 0.000 abstract 2
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- DUEPRVBVGDRKAG-UHFFFAOYSA-N carbofuran Chemical compound CNC(=O)OC1=CC=CC2=C1OC(C)(C)C2 DUEPRVBVGDRKAG-UHFFFAOYSA-N 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000002917 insecticide Substances 0.000 abstract 1
- 238000003786 synthesis reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/77—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D307/78—Benzo [b] furans; Hydrogenated benzo [b] furans
- C07D307/86—Benzo [b] furans; Hydrogenated benzo [b] furans with an oxygen atom directly attached in position 7
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Furan Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Plural Heterocyclic Compounds (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
Abstract
Inventia se refera la un procedeu pentru prepararea 2,3-dihidro-2,2-dimetil-7-hidroxibenzofuranului prin încalzirea O-metilpirocatechinei sa o-metiloxifenolului la temperaturi cuprinse între 100 si 200 degree C, în prezenta de izopropilat de aluminiu, crezolat de aluminiu, eventual în prezenta unui solvent organic inert ales dintre hidrocarburi aromatice alfatice, alifatice clorurate, cicloalifatice, eteri alifatici sau armoatici, metilizobutilcetona, alcanoli inferiori, fenol.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7930645A FR2470768A1 (fr) | 1979-12-07 | 1979-12-07 | Procede de preparation de derives de benzofuranne |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RO80924A RO80924A (ro) | 1983-02-15 |
| RO80924B true RO80924B (ro) | 1983-02-28 |
Family
ID=9232755
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RO102783A RO80924B (ro) | 1979-12-07 | 1980-12-05 | Procedeu pentru prepararea 2, 3-dihidro-2, 2-dimetil-7-hidroxibenzofuranului |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US4324731A (ro) |
| EP (1) | EP0030511B1 (ro) |
| JP (1) | JPS5697279A (ro) |
| KR (1) | KR840001020B1 (ro) |
| AT (1) | ATE6424T1 (ro) |
| BG (1) | BG35188A3 (ro) |
| BR (1) | BR8007966A (ro) |
| CA (1) | CA1157875A (ro) |
| DD (1) | DD155067A5 (ro) |
| DE (1) | DE3066770D1 (ro) |
| DK (1) | DK154140C (ro) |
| ES (1) | ES497479A0 (ro) |
| FR (1) | FR2470768A1 (ro) |
| HU (1) | HU185804B (ro) |
| IE (1) | IE51695B1 (ro) |
| IL (1) | IL61424A (ro) |
| PL (1) | PL136260B1 (ro) |
| PT (1) | PT72175B (ro) |
| RO (1) | RO80924B (ro) |
| SU (1) | SU1153828A3 (ro) |
| YU (1) | YU41369B (ro) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5821676A (ja) * | 1981-07-29 | 1983-02-08 | Otsuka Chem Co Ltd | 2,3−ジハイドロ−2,2−ジメチル−7−ハイドロオキシベンゾフランの製造方法 |
| JPS5835180A (ja) * | 1981-08-24 | 1983-03-01 | Otsuka Chem Co Ltd | 2,3−ジハイドロ−2,2−ジメチル−7−ハイドロオキシペンゾフランの製造法 |
| JPS5839679A (ja) * | 1981-09-01 | 1983-03-08 | Otsuka Chem Co Ltd | 2,3−ジハイドロ−2,2−ジメチル−7−ハイドロオキシベンゾフランの製法 |
| US4380654A (en) * | 1982-02-18 | 1983-04-19 | Fmc Corporation | Process for preparation of 2,3-dihydro-2,2-dimethyl-7-hydroxybenzofuran |
| FR2536395A1 (fr) * | 1982-11-18 | 1984-05-25 | Rhone Poulenc Agrochimie | Procede de preparation du dihydro-2,3 dimethyl-2,2 hydroxy-7 benzofuranne |
| IT1199987B (it) * | 1983-02-04 | 1989-01-05 | Brichima Spa | Processo per la produzione di derivati benzofuranici |
| EP0127208A1 (en) * | 1983-04-22 | 1984-12-05 | ENICHIMICA SECONDARIA S.p.A. | Process for preparing substituted 2,3-dihydrobenzofuran |
| CN101418008B (zh) * | 2008-12-05 | 2010-12-08 | 湖南大学 | 二羧酸酚铝及其制备方法与应用 |
| CN103562169B (zh) * | 2011-06-13 | 2016-04-20 | Fmc有限公司 | 对-甲代烯丙基邻苯二酚的纯化方法 |
| CN106673967B (zh) * | 2016-11-14 | 2020-05-22 | 湖南海利株洲精细化工有限公司 | 4-(2-甲基烯丙基)-1,2-苯二酚的制备方法 |
| CN118146071B (zh) * | 2024-03-07 | 2024-09-27 | 江苏三吉利化工股份有限公司 | 一种4-(2-甲基烯丙基)-1,2-苯二酚的合成工艺 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL131921C (ro) * | 1963-06-28 | |||
| US3474171A (en) * | 1964-01-23 | 1969-10-21 | Fmc Corp | 2,2-dimethyl-2,3-dihydrobenzofuranyl-7-n-methylcarbamate |
| US3474170A (en) * | 1964-01-23 | 1969-10-21 | Fmc Corp | Pesticidal carbamates of dihydrobenzofuranols |
| GB1179250A (en) * | 1966-09-16 | 1970-01-28 | Fisons Pest Control Ltd | Benzofuran Derivatives |
| US3927118A (en) * | 1973-12-21 | 1975-12-16 | Crown Zellerbach Corp | Process for monoetherification of polyhydric benzenes |
-
1979
- 1979-12-07 FR FR7930645A patent/FR2470768A1/fr active Granted
-
1980
- 1980-11-06 IL IL61424A patent/IL61424A/xx not_active IP Right Cessation
- 1980-11-07 US US06/204,992 patent/US4324731A/en not_active Expired - Lifetime
- 1980-11-21 YU YU3036/80A patent/YU41369B/xx unknown
- 1980-11-24 KR KR1019800004483A patent/KR840001020B1/ko not_active Expired
- 1980-11-27 BG BG049798A patent/BG35188A3/xx unknown
- 1980-12-01 EP EP80420130A patent/EP0030511B1/fr not_active Expired
- 1980-12-01 DE DE8080420130T patent/DE3066770D1/de not_active Expired
- 1980-12-01 AT AT80420130T patent/ATE6424T1/de not_active IP Right Cessation
- 1980-12-03 IE IE2512/80A patent/IE51695B1/en not_active IP Right Cessation
- 1980-12-03 CA CA000366089A patent/CA1157875A/en not_active Expired
- 1980-12-04 JP JP17143980A patent/JPS5697279A/ja active Granted
- 1980-12-05 RO RO102783A patent/RO80924B/ro unknown
- 1980-12-05 PT PT72175A patent/PT72175B/pt not_active IP Right Cessation
- 1980-12-05 HU HU802918A patent/HU185804B/hu not_active IP Right Cessation
- 1980-12-05 SU SU803213102A patent/SU1153828A3/ru active
- 1980-12-05 DK DK520480A patent/DK154140C/da not_active IP Right Cessation
- 1980-12-05 BR BR8007966A patent/BR8007966A/pt not_active IP Right Cessation
- 1980-12-05 ES ES497479A patent/ES497479A0/es active Granted
- 1980-12-05 DD DD80225766A patent/DD155067A5/de not_active IP Right Cessation
- 1980-12-05 PL PL1980228295A patent/PL136260B1/pl unknown
Also Published As
| Publication number | Publication date |
|---|---|
| YU303680A (en) | 1983-01-21 |
| IE802512L (en) | 1981-06-07 |
| PL136260B1 (en) | 1986-02-28 |
| KR830004282A (ko) | 1983-07-09 |
| IL61424A (en) | 1985-04-30 |
| HU185804B (en) | 1985-04-28 |
| DE3066770D1 (en) | 1984-04-05 |
| IE51695B1 (en) | 1987-02-18 |
| ES8304109A1 (es) | 1982-09-16 |
| RO80924A (ro) | 1983-02-15 |
| EP0030511B1 (fr) | 1984-02-29 |
| PT72175A (fr) | 1981-01-01 |
| EP0030511A1 (fr) | 1981-06-17 |
| ATE6424T1 (de) | 1984-03-15 |
| DK520480A (da) | 1981-06-08 |
| YU41369B (en) | 1987-02-28 |
| FR2470768A1 (fr) | 1981-06-12 |
| CA1157875A (en) | 1983-11-29 |
| JPS5697279A (en) | 1981-08-05 |
| BG35188A3 (en) | 1984-02-15 |
| JPS6135191B2 (ro) | 1986-08-12 |
| PL228295A1 (ro) | 1981-08-07 |
| PT72175B (fr) | 1982-07-05 |
| KR840001020B1 (ko) | 1984-07-20 |
| IL61424A0 (en) | 1980-12-31 |
| DK154140B (da) | 1988-10-17 |
| BR8007966A (pt) | 1981-06-23 |
| US4324731A (en) | 1982-04-13 |
| DD155067A5 (de) | 1982-05-12 |
| SU1153828A3 (ru) | 1985-04-30 |
| FR2470768B1 (ro) | 1983-02-04 |
| ES497479A0 (es) | 1982-09-16 |
| DK154140C (da) | 1989-03-06 |
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