PL84923B3 - Cyclic process for preparing and working up a hydroxylammonium salt solution [gb1283894a] - Google Patents
Cyclic process for preparing and working up a hydroxylammonium salt solution [gb1283894a] Download PDFInfo
- Publication number
- PL84923B3 PL84923B3 PL1971146111A PL14611171A PL84923B3 PL 84923 B3 PL84923 B3 PL 84923B3 PL 1971146111 A PL1971146111 A PL 1971146111A PL 14611171 A PL14611171 A PL 14611171A PL 84923 B3 PL84923 B3 PL 84923B3
- Authority
- PL
- Poland
- Prior art keywords
- gb1283894a
- oxime
- solution
- salt solution
- preparing
- Prior art date
Links
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical class ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 title abstract description 20
- 238000004519 manufacturing process Methods 0.000 title abstract description 4
- 239000012266 salt solution Substances 0.000 title description 3
- 125000004122 cyclic group Chemical group 0.000 title 1
- 229910017920 NH3OH Inorganic materials 0.000 claims 2
- 230000015572 biosynthetic process Effects 0.000 abstract description 23
- 238000003786 synthesis reaction Methods 0.000 abstract description 21
- 239000007788 liquid Substances 0.000 abstract description 16
- VEZUQRBDRNJBJY-UHFFFAOYSA-N cyclohexanone oxime Chemical compound ON=C1CCCCC1 VEZUQRBDRNJBJY-UHFFFAOYSA-N 0.000 abstract description 14
- IOVCWXUNBOPUCH-UHFFFAOYSA-N Nitrous acid Chemical compound ON=O IOVCWXUNBOPUCH-UHFFFAOYSA-N 0.000 abstract description 13
- 238000000034 method Methods 0.000 abstract description 12
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 abstract description 3
- 239000000356 contaminant Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 description 11
- 239000007789 gas Substances 0.000 description 11
- 239000000243 solution Substances 0.000 description 11
- 150000002923 oximes Chemical class 0.000 description 10
- GQPLMRYTRLFLPF-UHFFFAOYSA-N nitrous oxide Inorganic materials [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 description 9
- 238000010438 heat treatment Methods 0.000 description 8
- 229910002651 NO3 Inorganic materials 0.000 description 7
- 238000010521 absorption reaction Methods 0.000 description 7
- 150000002576 ketones Chemical class 0.000 description 7
- -1 nitrate ions Chemical class 0.000 description 7
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 6
- 239000003054 catalyst Substances 0.000 description 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 4
- 238000000354 decomposition reaction Methods 0.000 description 4
- 238000007254 oxidation reaction Methods 0.000 description 4
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- 239000003929 acidic solution Substances 0.000 description 3
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 229910052763 palladium Inorganic materials 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 239000012429 reaction media Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 101000983970 Conus catus Alpha-conotoxin CIB Proteins 0.000 description 1
- SZUKPSUMNNWOCI-UHFFFAOYSA-N NOO Chemical compound NOO SZUKPSUMNNWOCI-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000012295 chemical reaction liquid Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 125000002243 cyclohexanonyl group Chemical group *C1(*)C(=O)C(*)(*)C(*)(*)C(*)(*)C1(*)* 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-M hydrogensulfate Chemical compound OS([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-M 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 150000002826 nitrites Chemical class 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1418—Preparation by catalytic reduction of nitrogen oxides or nitrates with hydrogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL7001905A NL7001905A (en, 2012) | 1970-02-11 | 1970-02-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL84923B3 true PL84923B3 (en) | 1976-04-30 |
Family
ID=19809297
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL1971146111A PL84923B3 (en) | 1970-02-11 | 1971-02-09 | Cyclic process for preparing and working up a hydroxylammonium salt solution [gb1283894a] |
Country Status (11)
| Country | Link |
|---|---|
| BE (1) | BE762596R (en, 2012) |
| BG (1) | BG18847A3 (en, 2012) |
| CH (1) | CH584191A5 (en, 2012) |
| DE (1) | DE2106384C3 (en, 2012) |
| ES (1) | ES388142A2 (en, 2012) |
| FR (1) | FR2080977B2 (en, 2012) |
| GB (1) | GB1283894A (en, 2012) |
| IT (1) | IT994009B (en, 2012) |
| NL (1) | NL7001905A (en, 2012) |
| PL (1) | PL84923B3 (en, 2012) |
| ZA (1) | ZA71775B (en, 2012) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3997607A (en) * | 1974-04-26 | 1976-12-14 | Stamicarbon B.V. | Recycling process for the preparation of cyclohexanone oxime |
| DE2921649A1 (de) * | 1979-05-28 | 1980-12-11 | Basf Ag | Verfahren zur behandlung von cyclohexanon und cyclohexanonoxim enthaltenden ammoniumhydrogensulfatloesungen |
| US4349520A (en) * | 1981-08-24 | 1982-09-14 | Allied Corporation | Continuous hydrolysis of ketoxime |
-
1970
- 1970-02-11 NL NL7001905A patent/NL7001905A/xx not_active Application Discontinuation
-
1971
- 1971-02-05 BE BE762596A patent/BE762596R/xx active
- 1971-02-08 ZA ZA710775A patent/ZA71775B/xx unknown
- 1971-02-09 PL PL1971146111A patent/PL84923B3/pl unknown
- 1971-02-10 IT IT48307/71A patent/IT994009B/it active
- 1971-02-10 ES ES388142A patent/ES388142A2/es not_active Expired
- 1971-02-11 FR FR7104585A patent/FR2080977B2/fr not_active Expired
- 1971-02-11 DE DE2106384A patent/DE2106384C3/de not_active Expired
- 1971-02-11 CH CH203171A patent/CH584191A5/xx not_active IP Right Cessation
- 1971-02-11 BG BG016783A patent/BG18847A3/xx unknown
- 1971-04-19 GB GB21605/71A patent/GB1283894A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE2106384C3 (de) | 1981-01-08 |
| BG18847A3 (bg) | 1975-03-20 |
| BE762596R (fr) | 1971-08-05 |
| ES388142A2 (es) | 1976-01-01 |
| ZA71775B (en) | 1971-10-27 |
| GB1283894A (en) | 1972-08-02 |
| DE2106384A1 (en, 2012) | 1971-08-26 |
| FR2080977A2 (en, 2012) | 1971-11-26 |
| NL7001905A (en, 2012) | 1971-08-13 |
| FR2080977B2 (en, 2012) | 1976-01-16 |
| DE2106384B2 (de) | 1980-04-24 |
| CH584191A5 (en, 2012) | 1977-01-31 |
| IT994009B (it) | 1975-10-20 |
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