PL448602A1 - Sposób otrzymywania 4-jodo-5′-fenylo-1,1′:3′,1′′-terfenylu - Google Patents
Sposób otrzymywania 4-jodo-5′-fenylo-1,1′:3′,1′′-terfenyluInfo
- Publication number
- PL448602A1 PL448602A1 PL448602A PL44860224A PL448602A1 PL 448602 A1 PL448602 A1 PL 448602A1 PL 448602 A PL448602 A PL 448602A PL 44860224 A PL44860224 A PL 44860224A PL 448602 A1 PL448602 A1 PL 448602A1
- Authority
- PL
- Poland
- Prior art keywords
- terphenyl
- phenyl
- iodo
- obtaining
- hours
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 2
- NLKNQRATVPKPDG-UHFFFAOYSA-M potassium iodide Chemical compound [K+].[I-] NLKNQRATVPKPDG-UHFFFAOYSA-M 0.000 abstract 3
- 239000011541 reaction mixture Substances 0.000 abstract 2
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000004440 column chromatography Methods 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract 1
- 239000011707 mineral Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000002244 precipitate Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 235000010288 sodium nitrite Nutrition 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C25/00—Compounds containing at least one halogen atom bound to a six-membered aromatic ring
- C07C25/18—Polycyclic aromatic halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C15/00—Cyclic hydrocarbons containing only six-membered aromatic rings as cyclic parts
- C07C15/12—Polycyclic non-condensed hydrocarbons
- C07C15/14—Polycyclic non-condensed hydrocarbons all phenyl groups being directly linked
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C245/00—Compounds containing chains of at least two nitrogen atoms with at least one nitrogen-to-nitrogen multiple bond
- C07C245/02—Azo compounds, i.e. compounds having the free valencies of —N=N— groups attached to different atoms, e.g. diazohydroxides
- C07C245/06—Azo compounds, i.e. compounds having the free valencies of —N=N— groups attached to different atoms, e.g. diazohydroxides with nitrogen atoms of azo groups bound to carbon atoms of six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/06—Luminescent, e.g. electroluminescent, chemiluminescent materials containing organic luminescent materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Przedmiotem wynalazku jest sposób otrzymywania 4-jodo-5'-fenylo-1,1':3',1"-terfenylu o wzorze 1, charakteryzujący się tym, że mieszaninę 5'-fenylo-[1,1':3',1-terfenylo]-4-aminy i azotynu sodu w wodnym roztworze kwasu mineralnego w stosunku molowym 1:5, miesza się przez 2 h w temperaturze pokojowej, po czym do mieszaniny reakcyjnej dodaje się jodek potasu i mieszanie kontynuowane jest przez 2 godziny w temperaturze pokojowej a uzyskany osad wydziela się z mieszaniny reakcyjnej na drodze ekstrakcji, zaś czysty produkt wyodrębnia się na drodze chromatografii kolumnowej.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL448602A PL448602A1 (pl) | 2024-05-17 | 2024-05-17 | Sposób otrzymywania 4-jodo-5′-fenylo-1,1′:3′,1′′-terfenylu |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL448602A PL448602A1 (pl) | 2024-05-17 | 2024-05-17 | Sposób otrzymywania 4-jodo-5′-fenylo-1,1′:3′,1′′-terfenylu |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL448602A1 true PL448602A1 (pl) | 2024-12-16 |
Family
ID=93895000
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL448602A PL448602A1 (pl) | 2024-05-17 | 2024-05-17 | Sposób otrzymywania 4-jodo-5′-fenylo-1,1′:3′,1′′-terfenylu |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL448602A1 (pl) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0586006A (ja) * | 1991-09-24 | 1993-04-06 | Mita Ind Co Ltd | アゾ系化合物およびジアゾニウム塩 |
-
2024
- 2024-05-17 PL PL448602A patent/PL448602A1/pl unknown
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0586006A (ja) * | 1991-09-24 | 1993-04-06 | Mita Ind Co Ltd | アゾ系化合物およびジアゾニウム塩 |
Non-Patent Citations (2)
| Title |
|---|
| EWA DROZD-SZCZYGIEŁ ET AL: "Uniwersytet Medyczny im. Piastów Śląskich we Wrocławiu Wydział Farmaceutyczny z Oddziałem Analityki Medycznej Katedra i Zakład Chemii Organicznej, 2014", PREPARATYKA ORGANICZNA * |
| UJ - COLLEGIUM MEDICUM, KCHO: "Pracownia chemii organicznej, 02.2019", DIAZOWANIE * |
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