PL3137418T3 - Sposób oczyszczania surowego kwasu fosforowego (np. kwasu mga) poprzez dodanie popiołów pochodzących ze spalarni odpadów, obejmujący produkcję czystego kwasu fosforowego, siarczanu wapnia, rozpuszczalnych w wodzie wodorosforanów wapnia oraz roztworu soli metali - Google Patents
Sposób oczyszczania surowego kwasu fosforowego (np. kwasu mga) poprzez dodanie popiołów pochodzących ze spalarni odpadów, obejmujący produkcję czystego kwasu fosforowego, siarczanu wapnia, rozpuszczalnych w wodzie wodorosforanów wapnia oraz roztworu soli metaliInfo
- Publication number
- PL3137418T3 PL3137418T3 PL14727160.5T PL14727160T PL3137418T3 PL 3137418 T3 PL3137418 T3 PL 3137418T3 PL 14727160 T PL14727160 T PL 14727160T PL 3137418 T3 PL3137418 T3 PL 3137418T3
- Authority
- PL
- Poland
- Prior art keywords
- phosphoric acid
- acid
- production
- metal salt
- salt solution
- Prior art date
Links
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 title 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 title 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 title 2
- 235000002918 Fraxinus excelsior Nutrition 0.000 title 1
- 239000002253 acid Substances 0.000 title 1
- 239000002956 ash Substances 0.000 title 1
- FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical class [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 title 1
- 235000019700 dicalcium phosphate Nutrition 0.000 title 1
- 229910052751 metal Chemical class 0.000 title 1
- 239000002184 metal Chemical class 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 239000012266 salt solution Substances 0.000 title 1
- 238000004056 waste incineration Methods 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/18—Phosphoric acid
- C01B25/234—Purification; Stabilisation; Concentration
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/32—Phosphates of magnesium, calcium, strontium, or barium
- C01B25/324—Preparation from a reaction solution obtained by acidifying with an acid other than orthophosphoric acid
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/46—Sulfates
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/42—Treatment of water, waste water, or sewage by ion-exchange
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
- C02F1/5245—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents using basic salts, e.g. of aluminium and iron
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/30—Aerobic and anaerobic processes
- C02F3/302—Nitrification and denitrification treatment
- C02F3/305—Nitrification and denitrification treatment characterised by the denitrification
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B1/00—Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
- C05B1/04—Double-superphosphate; Triple-superphosphate; Other fertilisers based essentially on monocalcium phosphate
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B17/00—Other phosphatic fertilisers, e.g. soft rock phosphates, bone meal
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/42—Treatment of water, waste water, or sewage by ion-exchange
- C02F2001/425—Treatment of water, waste water, or sewage by ion-exchange using cation exchangers
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/105—Phosphorus compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2303/00—Specific treatment goals
- C02F2303/16—Regeneration of sorbents, filters
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W10/00—Technologies for wastewater treatment
- Y02W10/40—Valorisation of by-products of wastewater, sewage or sludge processing
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Geology (AREA)
- Biodiversity & Conservation Biology (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Processing Of Solid Wastes (AREA)
- Fertilizers (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Removal Of Specific Substances (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102014006278.3A DE102014006278B3 (de) | 2014-05-02 | 2014-05-02 | Verfahren zur Reinigung von Roh-Phosphorsäure (z.B. MGA-Säure) durch Zugabe von Aschen aus Abfall-Verbrennungsanlagen umfassend die Gewinnung von reiner Phosphorsäure, Kalziumsulfat, wasserlöslichen Kalziumhydrogenphosphaten und Metallsalz-Lösung |
| PCT/EP2014/001360 WO2015165481A1 (de) | 2014-05-02 | 2014-05-20 | Verfahren zur reinigung von roh-phosphorsäure (z.b. mga-säure) durch zugabe von aschen aus abfall-verbrennungsanlagen umfassend die gewinnung von reiner phosphorsäure, kalziumsulfat, wasserlöslichen kalziumhydrogenphosphaten und metallsalz-lösung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL3137418T3 true PL3137418T3 (pl) | 2023-10-30 |
Family
ID=50842228
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL14727160.5T PL3137418T3 (pl) | 2014-05-02 | 2014-05-20 | Sposób oczyszczania surowego kwasu fosforowego (np. kwasu mga) poprzez dodanie popiołów pochodzących ze spalarni odpadów, obejmujący produkcję czystego kwasu fosforowego, siarczanu wapnia, rozpuszczalnych w wodzie wodorosforanów wapnia oraz roztworu soli metali |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US10329153B2 (pl) |
| EP (1) | EP3137418B1 (pl) |
| JP (2) | JP6397565B2 (pl) |
| AU (1) | AU2014392293B2 (pl) |
| CA (1) | CA2947190C (pl) |
| DE (1) | DE102014006278B3 (pl) |
| EA (1) | EA032870B1 (pl) |
| ES (1) | ES2956671T3 (pl) |
| PL (1) | PL3137418T3 (pl) |
| RS (1) | RS64525B1 (pl) |
| WO (1) | WO2015165481A1 (pl) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL449304A1 (pl) * | 2024-07-24 | 2026-01-26 | Politechnika Krakowska im. Tadeusza Kościuszki | Sposób wytwarzania nawozów fosforowych typu superfosfat potrójny |
| PL449301A1 (pl) * | 2024-07-24 | 2026-01-26 | Politechnika Krakowska im. Tadeusza Kościuszki | Sposób wytwarzania nawozów fosforowych typu superfosfat potrójny |
Families Citing this family (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2934215C (en) | 2013-12-20 | 2020-07-28 | Ecophos S.A. | Method for recovering ash from waste incineration |
| DE102014006278B3 (de) * | 2014-05-02 | 2015-02-26 | Remondis Aqua Gmbh & Co. Kg | Verfahren zur Reinigung von Roh-Phosphorsäure (z.B. MGA-Säure) durch Zugabe von Aschen aus Abfall-Verbrennungsanlagen umfassend die Gewinnung von reiner Phosphorsäure, Kalziumsulfat, wasserlöslichen Kalziumhydrogenphosphaten und Metallsalz-Lösung |
| CN105884077A (zh) * | 2016-04-13 | 2016-08-24 | 四川绵竹市盘龙矿物质有限责任公司 | 在饲料级磷酸氢钙生产工艺中实现废水全封闭循环的方法 |
| DE102016212242B4 (de) * | 2016-07-05 | 2019-02-07 | Technische Universität Bergakademie Freiberg | Verfahren zur Herstellung von Phosphorsäure aus phosphorhaltigen Primär- und Sekundärrohstoffen |
| DE102016010861A1 (de) | 2016-09-07 | 2018-03-08 | Patrick Herr | Verfahren und Vorrichtung zur Rückgewinnung von Phosphor aus phosphorhaltiger Klärschlammasche |
| DE102016122869B4 (de) | 2016-11-28 | 2018-07-05 | Chemische Fabrik Budenheim Kg | Gesamtverfahren zur Aufbereitung von biologischen Abfällen |
| CN107098529B (zh) * | 2017-04-26 | 2025-12-12 | 西可林控制系统(上海)有限公司 | 一种盐酸酸洗废液的无排放处理方法及其装置 |
| CN107512843B (zh) * | 2017-07-17 | 2020-10-30 | 中山大学 | 一种基于循环盐液渗析的污泥脱水系统及其脱水方法 |
| EP3665124B1 (fr) * | 2017-08-11 | 2021-09-29 | Prayon S.A. | Procede d'attaque acide d'une source phosphatee |
| EP3707102A4 (en) * | 2017-11-10 | 2021-07-21 | Reticle, Inc. | WATER TREATMENT PROCESSES TO REMOVE CONTAMINANTS AND WATER TREATMENT PLANTS FOR THEIR IMPLEMENTATION |
| US11834382B2 (en) * | 2018-02-01 | 2023-12-05 | Pontes Pabuli Gmbh | Pedosphere-improving granulate, method for producing same, and use thereof |
| EP3947321A1 (de) * | 2019-03-26 | 2022-02-09 | Pontes pabuli GmbH | Schwermetallabgereicherte düngergranulate aus sekundärphosphat und verfahren zu deren herstellung |
| EP4015452A1 (en) | 2020-12-21 | 2022-06-22 | Técnicas Reunidas, S.A. | Process for producing technical grade phosphoric acid from sewage sludge ash |
| DE112022001097A5 (de) | 2021-02-15 | 2024-02-15 | Remondis Aqua Gmbh & Co. Kg | Verfahren zur kombinierten Rückgewinnung von Phosphat und Stickstoff aus Klärschlamm und gegebenenfalls biologischen Abfällen |
| DE102021000786A1 (de) | 2021-02-16 | 2022-08-18 | Remondis Aqua Gmbh & Co. Kg | Verfahren zur kombinierten Rückgewinnung von Phosphat und Stickstoff aus Klärschlamm und gegebenenfalls biologischen Abfällen |
| CN115215310B (zh) * | 2022-06-28 | 2023-10-27 | 新希望化工投资有限公司 | 一种粗磷酸的除杂回收方法 |
| DE102023100413A1 (de) | 2023-01-10 | 2024-07-11 | Remondis Aqua Gmbh & Co. Kg | Verfahren zur Gewinnung und Aufreinigung von Phosphorsäure aus Asche |
| FR3151032A1 (fr) * | 2023-07-12 | 2025-01-17 | Universite Mohammed VI Polytechnique | Procédé d’élimination de métaux lourds contenus dans les solutions d’acide phosphorique |
| WO2025047870A1 (ja) * | 2023-08-30 | 2025-03-06 | 学校法人近畿大学 | カルシウム塩の製造方法 |
| WO2025047869A1 (ja) * | 2023-08-30 | 2025-03-06 | 学校法人近畿大学 | リン酸の製造方法 |
| CN117623248B (zh) * | 2023-12-13 | 2025-09-19 | 东北大学 | 一种转炉渣和污泥焚烧灰联合处理及回收磷的方法 |
| DE102024119483A1 (de) | 2024-07-09 | 2026-01-15 | Remondis Aqua Gmbh & Co. Kg | Verbessertes Verfahren zur Gewinnung und Aufreinigung von Phosphorsäure aus Asche |
Family Cites Families (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3006754A (en) * | 1959-04-15 | 1961-10-31 | Anaconda Co | Production of superphosphate fertilizers |
| DE1289036B (de) * | 1967-02-10 | 1969-02-13 | Kloeckner Humboldt Deutz Ag | Verfahren zur Reinigung einer Phosphorsaeure-Aufschlussloesung |
| US3607016A (en) * | 1967-11-29 | 1971-09-21 | Sir Soc Italiana Resine Spa | Process for recovering sodium fluosilicate in the production of phosphoric acid |
| JPS4834797A (pl) * | 1971-09-08 | 1973-05-22 | ||
| JPS5375196A (en) * | 1976-12-15 | 1978-07-04 | Central Glass Co Ltd | Removing method for heavy metals from phosphoric acid solution |
| JPS54123469A (en) * | 1978-03-10 | 1979-09-25 | Mitsubishi Chem Ind | Production of granulated basic phosphatic fertilizer |
| SE418845B (sv) * | 1979-05-10 | 1981-06-29 | Boliden Ab | Forfarande for rening av vatprocessfosforsyra |
| DE3134847A1 (de) * | 1981-09-03 | 1983-03-17 | Hoechst Ag, 6000 Frankfurt | "verfahren zur gewinnung cadmium-freier rohphosphorsaeure" |
| US4389380A (en) * | 1982-01-12 | 1983-06-21 | Agrico Chemical Company | Multiple-stage thermal beneficiation process for phosphate ores |
| US4479923A (en) * | 1982-01-12 | 1984-10-30 | Pennzoil Company | Production of phosphoric acid and additional products from phosphate ore |
| DE3210575A1 (de) * | 1982-03-23 | 1983-10-06 | Hoechst Ag | Verfahren zur verminderung des schwermetall-gehaltes, insbesondere an cadmiumverbindungen |
| US4554144A (en) * | 1983-03-18 | 1985-11-19 | Occidental Research Corporation | Removal of magnesium and/or aluminum values from impure aqueous phosphoric acid |
| US4851199A (en) * | 1985-01-03 | 1989-07-25 | Union Oil Company Of California | Methods for recovering vanadium from phosphoric acid and vanadium sources |
| DE4011716A1 (de) * | 1990-04-11 | 1991-10-17 | Hoechst Ag | Verfahren zur herstellung von alkaliphosphatloesungen |
| JP3417026B2 (ja) * | 1993-12-27 | 2003-06-16 | 栗田工業株式会社 | 煤塵の処理方法 |
| JP2975571B2 (ja) * | 1996-06-07 | 1999-11-10 | 司郎 吉崎 | 汚泥類から重金属類を除去する方法 |
| JP3705982B2 (ja) * | 1999-08-23 | 2005-10-12 | Ｊｆｅプラント＆サービス株式会社 | リン酸塩回収方法 |
| JP4316946B2 (ja) * | 2003-07-01 | 2009-08-19 | 日本化学工業株式会社 | 高純度リン酸及びその製造方法 |
| JP4417152B2 (ja) * | 2004-03-25 | 2010-02-17 | Ｄｏｗａホールディングス株式会社 | 飛灰の処理方法 |
| JP2008200628A (ja) * | 2007-02-21 | 2008-09-04 | Tosoh Corp | 重金属処理剤及びそれを用いた重金属汚染物の処理法 |
| WO2012165382A1 (ja) * | 2011-05-27 | 2012-12-06 | メタウォーター株式会社 | 焼却灰からのリン抽出方法 |
| CA2934215C (en) * | 2013-12-20 | 2020-07-28 | Ecophos S.A. | Method for recovering ash from waste incineration |
| DE102014006278B3 (de) * | 2014-05-02 | 2015-02-26 | Remondis Aqua Gmbh & Co. Kg | Verfahren zur Reinigung von Roh-Phosphorsäure (z.B. MGA-Säure) durch Zugabe von Aschen aus Abfall-Verbrennungsanlagen umfassend die Gewinnung von reiner Phosphorsäure, Kalziumsulfat, wasserlöslichen Kalziumhydrogenphosphaten und Metallsalz-Lösung |
-
2014
- 2014-05-02 DE DE102014006278.3A patent/DE102014006278B3/de active Active
- 2014-05-20 RS RS20230741A patent/RS64525B1/sr unknown
- 2014-05-20 PL PL14727160.5T patent/PL3137418T3/pl unknown
- 2014-05-20 WO PCT/EP2014/001360 patent/WO2015165481A1/de not_active Ceased
- 2014-05-20 JP JP2017508745A patent/JP6397565B2/ja active Active
- 2014-05-20 AU AU2014392293A patent/AU2014392293B2/en active Active
- 2014-05-20 EA EA201692207A patent/EA032870B1/ru unknown
- 2014-05-20 EP EP14727160.5A patent/EP3137418B1/de active Active
- 2014-05-20 ES ES14727160T patent/ES2956671T3/es active Active
- 2014-05-20 US US15/308,323 patent/US10329153B2/en active Active
- 2014-05-20 CA CA2947190A patent/CA2947190C/en active Active
-
2018
- 2018-08-06 JP JP2018147605A patent/JP6669337B2/ja active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL449304A1 (pl) * | 2024-07-24 | 2026-01-26 | Politechnika Krakowska im. Tadeusza Kościuszki | Sposób wytwarzania nawozów fosforowych typu superfosfat potrójny |
| PL449301A1 (pl) * | 2024-07-24 | 2026-01-26 | Politechnika Krakowska im. Tadeusza Kościuszki | Sposób wytwarzania nawozów fosforowych typu superfosfat potrójny |
Also Published As
| Publication number | Publication date |
|---|---|
| JP6669337B2 (ja) | 2020-03-18 |
| EA032870B1 (ru) | 2019-07-31 |
| ES2956671T3 (es) | 2023-12-26 |
| DE102014006278B3 (de) | 2015-02-26 |
| JP2017518956A (ja) | 2017-07-13 |
| JP6397565B2 (ja) | 2018-09-26 |
| AU2014392293B2 (en) | 2019-03-28 |
| EP3137418B1 (de) | 2023-06-21 |
| EP3137418C0 (de) | 2023-06-21 |
| RS64525B1 (sr) | 2023-09-29 |
| US20170050848A1 (en) | 2017-02-23 |
| EP3137418A1 (de) | 2017-03-08 |
| AU2014392293A1 (en) | 2016-11-17 |
| US10329153B2 (en) | 2019-06-25 |
| WO2015165481A1 (de) | 2015-11-05 |
| JP2018188361A (ja) | 2018-11-29 |
| CA2947190A1 (en) | 2015-11-05 |
| CA2947190C (en) | 2022-02-08 |
| EA201692207A1 (ru) | 2017-02-28 |
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