PL2707128T3 - Reaktor do ammoksymacji do wytwarzania oksymu cykloheksanonu - Google Patents

Reaktor do ammoksymacji do wytwarzania oksymu cykloheksanonu

Info

Publication number
PL2707128T3
PL2707128T3 PL12719334T PL12719334T PL2707128T3 PL 2707128 T3 PL2707128 T3 PL 2707128T3 PL 12719334 T PL12719334 T PL 12719334T PL 12719334 T PL12719334 T PL 12719334T PL 2707128 T3 PL2707128 T3 PL 2707128T3
Authority
PL
Poland
Prior art keywords
cyclohexanone oxime
oxime production
ammoximation reactor
ammoximation
reactor
Prior art date
Application number
PL12719334T
Other languages
English (en)
Inventor
Alessandro Del Seppia
Elena GHIRARDO
Original Assignee
Versalis S.P.A.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Versalis S.P.A. filed Critical Versalis S.P.A.
Publication of PL2707128T3 publication Critical patent/PL2707128T3/pl

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
    • B01J8/10—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/005—Separating solid material from the gas/liquid stream
    • B01J8/006—Separating solid material from the gas/liquid stream by filtration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • B01J8/224—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement
    • B01J8/226—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid the particles being subject to a circulatory movement internally, i.e. the particles rotate within the vessel
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/00141—Coils
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/0015—Plates; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00823—Mixing elements
    • B01J2208/00831—Stationary elements
    • B01J2208/0084—Stationary elements inside the bed, e.g. baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00823—Mixing elements
    • B01J2208/00858—Moving elements
    • B01J2208/00867—Moving elements inside the bed, e.g. rotary mixer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00893—Feeding means for the reactants
    • B01J2208/00902—Nozzle-type feeding elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00893—Feeding means for the reactants
    • B01J2208/00911—Sparger-type feeding elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00938—Flow distribution elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00245—Avoiding undesirable reactions or side-effects
    • B01J2219/00247—Fouling of the reactor or the process equipment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
PL12719334T 2011-05-09 2012-04-27 Reaktor do ammoksymacji do wytwarzania oksymu cykloheksanonu PL2707128T3 (pl)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN201110209393.3A CN102773048B (zh) 2011-05-09 2011-05-09 生产环己酮肟的氨肟化反应器
EP12719334.0A EP2707128B1 (en) 2011-05-09 2012-04-27 Ammoximation reactor for cyclohexanone oxime production
PCT/EP2012/057746 WO2012152600A1 (en) 2011-05-09 2012-04-27 Ammoximation reactor for cyclohexanone oxime production

Publications (1)

Publication Number Publication Date
PL2707128T3 true PL2707128T3 (pl) 2020-08-10

Family

ID=46044669

Family Applications (1)

Application Number Title Priority Date Filing Date
PL12719334T PL2707128T3 (pl) 2011-05-09 2012-04-27 Reaktor do ammoksymacji do wytwarzania oksymu cykloheksanonu

Country Status (12)

Country Link
US (1) US10525429B2 (pl)
EP (1) EP2707128B1 (pl)
JP (1) JP6058638B2 (pl)
KR (1) KR101941313B1 (pl)
CN (1) CN102773048B (pl)
BR (1) BR112013028740B1 (pl)
ES (1) ES2786002T3 (pl)
HU (1) HUE049692T2 (pl)
MY (1) MY166458A (pl)
PL (1) PL2707128T3 (pl)
TW (1) TWI538899B (pl)
WO (1) WO2012152600A1 (pl)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103214393B (zh) * 2013-04-27 2014-08-20 湖南百利工程科技股份有限公司 一种酮的肟化方法
CN103551085A (zh) * 2013-11-08 2014-02-05 神马实业股份有限公司 一种用于环己酮氨肟化反应的催化剂分离装置
CN104860842B (zh) * 2015-05-13 2018-02-23 南京工业大学 一种基于膜分布的无溶剂绿色氨肟化工艺
EP3235560A1 (de) 2016-04-22 2017-10-25 Evonik Röhm GmbH Verfahren zur durchführung einer heterogen-katalysierten reaktion
CN106040108B (zh) * 2016-06-30 2018-09-14 湘潭大学 气-液-固三相反应器及连续催化氧化合成草甘膦的方法
CN108530316B (zh) * 2018-05-10 2023-07-04 中国平煤神马集团尼龙科技有限公司 一种固定床热回收式氨肟化反应系统
CN110787766B (zh) * 2019-10-10 2020-06-23 浙江工业大学 一种制备脂肪酸丁酯的塔式反应装置及工艺
CN112174850B (zh) * 2019-10-11 2022-11-22 福建天辰耀隆新材料有限公司 一种环己酮肟制备方法
CN111644121B (zh) * 2020-06-09 2022-02-11 常州市新鸿医药化工技术有限公司 一种三氯丙酮的加氢脱氯装置及其方法
WO2022248328A1 (en) 2021-05-28 2022-12-01 Röhm Gmbh Reactor and process for producing alkyl (meth)acrylates
WO2022248321A1 (en) 2021-05-28 2022-12-01 Röhm Gmbh Reactor and process for producing alkyl methacrylates
CN113877493B (zh) * 2021-08-24 2023-06-27 浙江中巨海锐科技有限公司 一种环十二酮溶液肟的连续化制备系统及方法
WO2023110831A1 (en) 2021-12-17 2023-06-22 Ineos Europe Ag Filtration device
CN114653328A (zh) * 2022-03-25 2022-06-24 中国科学院过程工程研究所 一种内置膜搅拌反应器
CN114712926A (zh) * 2022-04-18 2022-07-08 成都思达能环保设备有限公司 用于正极材料前驱体共沉淀反应设备的浓缩设备

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB577581A (en) * 1943-02-24 1946-05-23 Texaco Development Corp Improvements in or relating to the alkylation of organic compounds
FR2038694A5 (pl) * 1969-03-27 1971-01-08 Progil
FR2076365A5 (pl) * 1970-01-13 1971-10-15 Naphtachimie Sa
DE3245312A1 (de) * 1982-12-08 1984-06-14 Hoechst Ag, 6230 Frankfurt Verfahren zum durchfuehren (bio-)chemischer reaktionen
US5324853A (en) * 1993-01-19 1994-06-28 Exxon Chemical Patents Inc. Process for the production of plasticizer and polyolesters
KR100208654B1 (ko) * 1996-12-03 1999-07-15 윤덕용 하단 천공된 드래프트관을 갖는 내부순환유동층 가스화 반응기
BE1011581A3 (fr) * 1997-12-01 1999-11-09 Solvay Catalyseur a base de zeolite, son utilisation et procede d'epoxydation en presence de ce catalyseur.
AU1935601A (en) * 1999-12-10 2001-06-18 Inca International S.P.A. Impeller draft tube agitation system for gas-liquid mixing in a stirred tank reactor
BRPI0412565A (pt) * 2003-07-15 2006-09-19 Sasol Tech Pty Ltd processo para produzir lìquidos e, opcionalmente, gasosos de reagentes gasosos
JP4577205B2 (ja) * 2004-12-22 2010-11-10 住友化学株式会社 シクロヘキサノンオキシムの製造方法
SG123723A1 (en) * 2004-12-22 2006-07-26 Sumitomo Chemical Co Process for producing cyclohexanone oxime
JP2007203207A (ja) * 2006-02-02 2007-08-16 Sumitomo Chemical Co Ltd スパージャー、それを用いた反応器およびオキシムの製造方法。
CN101116804B (zh) * 2006-07-31 2010-06-23 中国石油化工股份有限公司 一体化反应分离设备
US20100084350A1 (en) * 2008-10-06 2010-04-08 Jing Liu Systems and Methods for Continuous Multiphase Reaction and Separation
CN201596496U (zh) * 2010-01-19 2010-10-06 河北瑞通美邦工程有限公司 一种环己酮氨肟化反应器
CN201988375U (zh) * 2011-03-04 2011-09-28 河北美邦工程科技有限公司 一种环己酮氨肟化反应催化剂分离装置
JP6058515B2 (ja) * 2013-10-04 2017-01-11 漢民科技股▲分▼有限公司 気相成膜装置

Also Published As

Publication number Publication date
WO2012152600A1 (en) 2012-11-15
CN102773048B (zh) 2017-06-06
JP2014523863A (ja) 2014-09-18
EP2707128B1 (en) 2020-03-18
CN102773048A (zh) 2012-11-14
US20140093437A1 (en) 2014-04-03
EP2707128A1 (en) 2014-03-19
KR101941313B1 (ko) 2019-01-22
BR112013028740A2 (pt) 2017-01-24
KR20140038445A (ko) 2014-03-28
TW201249783A (en) 2012-12-16
HUE049692T2 (hu) 2020-10-28
TWI538899B (zh) 2016-06-21
ES2786002T3 (es) 2020-10-08
JP6058638B2 (ja) 2017-01-11
US10525429B2 (en) 2020-01-07
MY166458A (en) 2018-06-27
BR112013028740B1 (pt) 2020-04-14

Similar Documents

Publication Publication Date Title
HUE049692T2 (hu) Ammoximációs reaktor ciklohexanon-oxim elõállítására
EP2940004A4 (en) PROCESS FOR PRODUCING OXIME
EP2761522A4 (en) OAUTH FRAME
ZA201305910B (en) Polyurea microcapsules
EP2784166A4 (en) PROCESS FOR MANUFACTURING HIGH PURITY NICKEL SULPHATE
ZA201209124B (en) Process for producing microcapsules
SG11201406618WA (en) Process for producing phenol and cyclohexanone
ZA201301956B (en) Process for producing polydienes
SG2014009591A (en) Spin forming method
ZA201401948B (en) Improved nitric acid production
SG11201501585SA (en) Process for separating methylcyclopentanone from cyclohexanone
SG11201502692RA (en) Process for producing phenol and cyclohexanone
EP2763554A4 (en) NEW SUBSTITUTED CYCLOHEXANE COMPOUNDS
GB201121953D0 (en) Magnetic fastening
SG11201405489RA (en) Process for preparing cyclohexanol and cyclohexanone by cyclohexane oxidation
EP2703386A4 (en) METHOD FOR PRODUCING A DIAMIN COMPOUND
EP2695879A4 (en) PROCESS FOR PREPARING CYCLOALKANONE-OXIM
EP2551261A4 (en) PROCESS FOR PREPARING OXIM
EP2868655A4 (en) PROCESS FOR PREPARING CYCLOALKANONE OXIM
HK1199637A1 (en) Process for making nitriles
IL219622A0 (en) A process for obtaining microcapsules
EP2796444A4 (en) PROCESS FOR PREPARING HIGH-PURITY CERAMID
ZA201205924B (en) Reactor
EP2719681A4 (en) METHOD FOR PRODUCING A CYCLOPENTANONE COMPOUND AND INTERMEDIATE PRODUCT THEREOF
EP2752402A4 (en) METHOD OF PREPARING A 2-ALKENYLAMINE COMPOUND