NO924394L - Fremgangsmaate for fremstilling av amidderivater fra halogenaminer og syrehalogenider - Google Patents
Fremgangsmaate for fremstilling av amidderivater fra halogenaminer og syrehalogeniderInfo
- Publication number
- NO924394L NO924394L NO92924394A NO924394A NO924394L NO 924394 L NO924394 L NO 924394L NO 92924394 A NO92924394 A NO 92924394A NO 924394 A NO924394 A NO 924394A NO 924394 L NO924394 L NO 924394L
- Authority
- NO
- Norway
- Prior art keywords
- halogenamines
- procedure
- amide derivatives
- preparing amide
- acid halogenides
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/14—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with hydrogen or carbon atoms directly attached to at least one ring carbon atom
- C07D251/24—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with hydrogen or carbon atoms directly attached to at least one ring carbon atom to three ring carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
- C07D401/14—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing three or more hetero rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/14—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with hydrogen or carbon atoms directly attached to at least one ring carbon atom
- C07D251/16—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with hydrogen or carbon atoms directly attached to at least one ring carbon atom to only one ring carbon atom
- C07D251/18—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with hydrogen or carbon atoms directly attached to at least one ring carbon atom to only one ring carbon atom with nitrogen atoms directly attached to the two other ring carbon atoms, e.g. guanamines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/54—Three nitrogen atoms
- C07D251/66—Derivatives of melamine in which a hetero atom is directly attached to a nitrogen atom of melamine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/54—Three nitrogen atoms
- C07D251/70—Other substituted melamines
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/40—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
- C08G59/50—Amines
- C08G59/5046—Amines heterocyclic
- C08G59/5053—Amines heterocyclic containing only nitrogen as a heteroatom
- C08G59/508—Amines heterocyclic containing only nitrogen as a heteroatom having three nitrogen atoms in the ring
- C08G59/5086—Triazines; Melamines; Guanamines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Cosmetics (AREA)
- Plural Heterocyclic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US79307791A | 1991-11-15 | 1991-11-15 | |
US07/968,871 US5288865A (en) | 1991-11-15 | 1992-10-30 | Process for preparing amide derivatives from haloaminotriazines and acid halides |
Publications (3)
Publication Number | Publication Date |
---|---|
NO924394D0 NO924394D0 (no) | 1992-11-13 |
NO924394L true NO924394L (no) | 1993-05-18 |
NO301711B1 NO301711B1 (no) | 1997-12-01 |
Family
ID=27121360
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
NO924394A NO301711B1 (no) | 1991-11-15 | 1992-11-13 | s-Triazin-2,4,6-triureaderivat |
Country Status (11)
Country | Link |
---|---|
US (3) | US5288865A (no) |
EP (5) | EP0930303B1 (no) |
JP (1) | JP3435654B2 (no) |
KR (1) | KR100254047B1 (no) |
AT (3) | ATE200078T1 (no) |
AU (1) | AU655688B2 (no) |
BR (1) | BR9204416A (no) |
CA (1) | CA2082880A1 (no) |
DE (3) | DE69231759T2 (no) |
ES (1) | ES2215338T3 (no) |
NO (1) | NO301711B1 (no) |
Families Citing this family (44)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
TW328955B (en) * | 1993-05-14 | 1998-04-01 | Cytec Tech Corp | Process for preparing bis- or tris-carbamate functional 1,3,5-triazines, substantially halogen contamination free crosslinker compositions and new bis-or tris-carbamate functional 1,3,5-triazines |
DE4331085A1 (de) * | 1993-09-13 | 1995-03-16 | Basf Ag | Stabile, nach phosgenfreien Verfahren erhältliche Polyisocyanatzusammensetzungen und ein Verfahren zu ihrer Herstellung |
US6197957B1 (en) * | 1993-10-15 | 2001-03-06 | Cytec Technology Corp. | Process for preparing derivatives of (halo)amino-1,3,5-triazines by carbonylation |
US5556971A (en) * | 1994-05-06 | 1996-09-17 | Cytec Technology Corp. | Process for preparing isocyanate and isocyanate-based derivatives of certain amino-1,3,5-triazines by direct phosgenation |
US6204382B1 (en) * | 1994-08-05 | 2001-03-20 | Cytec Technology Corp. | Carboxylated amino-1,3,5-triazines, derivatives thereof and processes for preparing the same |
US6448398B1 (en) | 1994-10-18 | 2002-09-10 | Cytec Technology Corp. | Process for preparing acid amides from (Si, Ge, or Sn substituted amino)-1,3,5-triazines and acid halides |
US5596047A (en) * | 1994-11-16 | 1997-01-21 | Cytec Technology Corp. | Water-dispersible and curable waterborne compositions containing 1,3,5-triazine carbamates |
US5672703A (en) * | 1995-03-21 | 1997-09-30 | Cytec Technology Corp. | 1,3,5-triazine compounds substituted with acetal and/or cyclized acetal-based groups |
US5565243A (en) * | 1995-05-01 | 1996-10-15 | Ppg Industries, Inc. | Color-clear composite coatings having improved hardness, acid etch resistance, and mar and abrasion resistance |
KR19990044020A (ko) * | 1995-08-30 | 1999-06-25 | 마이클 제이. 켈리 | 1,3,5-트리아진 카바메이트 및 에폭시 화합물을 함유하는조성물 |
WO1997031914A1 (en) * | 1996-03-01 | 1997-09-04 | Cytec Technology Corp. | Cyclic imido-1,3,5-triazine crosslinking agents |
DE19648843C2 (de) * | 1996-11-26 | 1998-09-17 | Zts Chemie Gmbh | Melamin-polycarbonsäureamide und ihre Verwendung als Korrosionsschutzmittel |
ES2157094T5 (es) * | 1996-12-18 | 2005-04-01 | Basf Coatings Aktiengesellschaft | Producto de revestimiento y procedimiento de preparacion del mismo. |
WO1998027166A2 (de) | 1996-12-18 | 1998-06-25 | Basf Coatings Ag | Beschichtungsmittel und verfahren zu dessen herstellung |
DE19730889A1 (de) | 1997-07-18 | 1999-01-21 | Basf Coatings Ag | Wäßriger Lack, enthaltend eine mehrkomponentige wäßrige Dispersion |
BR9815213A (pt) | 1997-10-15 | 2000-10-24 | Du Pont | Composição de revestimento, substrato e processo pra revestir um substrato |
WO1999065883A1 (en) | 1998-06-16 | 1999-12-23 | Cytec Technology Corp. | Process for the preparation of triazine carbamates |
DE19839453A1 (de) | 1998-08-29 | 2000-03-02 | Basf Coatings Ag | Oligomere und hochmolekulare Umsetzungsprodukte von Allophansäureestern mit nucleophilen Verbindungen und niedermolekulare, oligomere und hochmolekulare Verbindungen mit Allophanatseiten- und/oder -endgruppen sowie ihre Verwendung |
DE19840605A1 (de) | 1998-09-05 | 2000-03-09 | Basf Coatings Ag | Hyperverzweigte Verbindungen mit einer tetrafunktionellen Zentralgruppe und ihre Verwendung |
DE19841842C2 (de) | 1998-09-12 | 2000-07-06 | Basf Coatings Ag | Strukturviskose, von organischen Lösemitteln und externen Emulgatoren freie Pulverklarlack-Slurry, Verfahren zu ihrer Herstellung und ihre Verwendung |
US6121446A (en) * | 1998-11-10 | 2000-09-19 | Cytec Technology Corporation | Preparation of tris-substituted alkoxycarbonylamino-1,3,5-triazine compounds |
DE19908013A1 (de) | 1999-02-25 | 2000-08-31 | Basf Coatings Ag | Mit aktinischer Strahlung und gegebenenfalls themisch härtbare Pulverslurrys, Verfahren zu ihrer Herstellung und ihre Verwendung |
DE10001442A1 (de) * | 2000-01-15 | 2001-10-18 | Basf Coatings Ag | Strukturviskose, von organischen Lösemitteln freie Pulverklarlack-Slurry, Verfahren zu ihrer Herstellung und ihre Verwendung |
DE10004498A1 (de) * | 2000-02-02 | 2001-08-09 | Basf Coatings Ag | Diethyloctandioldicarbamate und Diethyloctandioldiallophanate, Verfahren zu ihrer Herstellung und ihre Verwendung |
DE10010405A1 (de) * | 2000-03-03 | 2001-09-13 | Basf Coatings Ag | Wäßrige (Meth)Acrylatcopolymerisat-Dispersionen, Verfahren zu ihrer Herstellung und ihre Verwendung |
DE10040223C2 (de) * | 2000-08-17 | 2002-12-05 | Basf Coatings Ag | Strukturviskose, von organischen Lösemitteln und externen Emulgatoren freie Pulverklarlack-Slurry, Verfahren zu ihrer Herstellung und ihre Verwendung |
DE10055464B4 (de) * | 2000-11-09 | 2006-06-14 | Basf Coatings Ag | Strukturviskose, von organischen Lösemitteln und externen Emulgatoren freie Pulverklarlack-Slurry und ihre Verwendung |
DE10126651A1 (de) * | 2001-06-01 | 2002-12-12 | Basf Coatings Ag | Pulverlacksuspensionen (Pulverslurries) und Pulverlacke, Verfahren zu ihrer Herstellung und ihre Verwendung |
US20040030176A1 (en) * | 2001-09-05 | 2004-02-12 | Ohrbom Walter H. | Gamma hydroxy carbamate compounds and method of making and using the same |
US6977309B2 (en) | 2002-10-31 | 2005-12-20 | Basf Corporation | Compounds having a secondary or tertiary hydroxy of halide group separated from a primary carbamate group by three or more carbon atoms and a method of making the same |
US6858674B2 (en) | 2002-10-31 | 2005-02-22 | Basf Corporation | Carbamate functional materials, a method of making said materials, and curable coating compositions containing said materials |
US6900270B2 (en) | 2002-10-31 | 2005-05-31 | Basf Corporation | Curable coating compositions with carbamate compounds |
US6890994B2 (en) * | 2002-10-31 | 2005-05-10 | Basf Corporation | Curable coating compositions with carbamate-containing acrylic polymers |
DE10259672A1 (de) * | 2002-12-18 | 2004-07-01 | Basf Ag | Verfahren zur Herstellung von Alkoxycarbonylamino-triazinen |
DE10353638A1 (de) | 2003-11-17 | 2005-06-23 | Basf Coatings Ag | Strukturviskose, wässrige Dispersionen, Verfahren zu ihrer Herstellung und ihre Verwendung |
US20050249879A1 (en) * | 2004-05-10 | 2005-11-10 | Jenkins Steven A | Packaging coating containing 1,3,5-triazine carbamate crosslinker |
DE102008016050A1 (de) | 2007-12-24 | 2009-06-25 | Voest-Alpine Stahl Gmbh | Flexibler Primer und dessen Verwendung |
US8143400B2 (en) * | 2008-01-10 | 2012-03-27 | Apotex Pharmachem Inc. | Process for the preparation and purification of cis-2-methylspiro(1,3-oxathiolane-5,3′)quiniclidine hydrochloride |
CN103946321B (zh) | 2011-11-17 | 2016-08-24 | 巴斯夫涂料有限公司 | 包含甘油二酯的涂料及其在多层漆中的用途 |
DE102014006519A1 (de) | 2014-05-03 | 2015-11-05 | Smart Material Printing B.V. | Verwendung magnetischer und/oder magnetisierbarer, polymerer Mikro- und/oder Nanocomposite zur Herstellung komplexer, magnetischer und/oder magnetisierbarer Formteile mithilfe additiver Fabrikatoren |
DE102015000814A1 (de) | 2015-01-21 | 2016-07-21 | Smart Material Printing B.V. | Biozide Ausrüstung von Gegenständen mit Polyoxometallat-Mikro- und/oder -Nanopartikeln |
EP3247210A1 (de) | 2015-01-21 | 2017-11-29 | Smartmaterialprinting B.V. | Biozide ausrüstung von gegenständen und wasserhaltigen reinigungs- und körperpflegemitteln mit polyoxometallat-mikro und/oder - nanopartikeln |
DE102018000418A1 (de) | 2018-01-20 | 2019-07-25 | Bürkle Consulting Gmbh | Mechanochemisches Verfahren zur Herstellung von von persistenten organischen Schadstoffen und anderen Organohalogenverbindungen freien Wertprodukten aus Abfällen von Kunststoffen und Kunststofflaminaten |
DE102018003906A1 (de) | 2018-05-07 | 2019-11-07 | Smart Material Printing | Verwendung von Polyoxometallaten gegen den Befall von Eukaryotenkulturen, Virenkulturen und Mikroorganismenpopulationen durch Mollicuten sowie mollicutenhemmende und -abtötende polyoxometallathaltige Stoffe und Verfahren |
Family Cites Families (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2184888A (en) * | 1939-12-26 | Halogenated material and method of | ||
US2184886A (en) * | 1939-12-26 | Organic composition of high | ||
US2577418A (en) * | 1951-12-04 | Tall oil-melamine reaction product | ||
US2184883A (en) * | 1939-12-26 | Composition of matter and method | ||
US2472361A (en) * | 1944-10-30 | 1949-06-07 | William C Arsem | Active halogen compounds and processes for their production |
US2507700A (en) * | 1946-11-27 | 1950-05-16 | Monsanto Chemicals | N, n', n''-triacylmelamines |
NL285972A (no) * | 1961-11-28 | 1900-01-01 | ||
CH436320A (de) * | 1962-02-06 | 1967-05-31 | Geigy Ag J R | Verfahren zur Herstellung von Acylmelaminverbindungen |
BE755460A (fr) * | 1969-08-28 | 1971-02-01 | Bayer Ag | Isocyanates de s-triazinyle, leur preparation et leur utilisation dans la fabrication de resines de polyurethanes |
US3684765A (en) * | 1970-01-08 | 1972-08-15 | Sankyo Co | Stabilization of synthetic polymers |
US3743642A (en) * | 1971-04-02 | 1973-07-03 | Basf Ag | Triazine derivatives |
CH572047A5 (no) * | 1973-03-01 | 1976-01-30 | Ciba Geigy Ag | |
US3920832A (en) * | 1974-04-18 | 1975-11-18 | Sol J Barer | N-chloro carbamates as insecticides and fungicides |
DE2640409C2 (de) * | 1976-09-08 | 1985-04-18 | Chemische Werke Hüls AG, 4370 Marl | Epoxidharz-Härter-Mischungen zur Herstellung von Formkörpern und Überzügen |
JPS58146582A (ja) * | 1982-02-26 | 1983-09-01 | Toshiba Corp | トリアジン系化合物およびその製造方法 |
GB2150565B (en) * | 1983-12-02 | 1987-08-26 | Ciba Geigy Ag | Pesticidal acylamino-s-triazines |
US4732899A (en) * | 1985-12-02 | 1988-03-22 | Ciba-Geigy Corporation | (Di)alkoxycarbonylamino-s-triazine derivatives and the use thereof against pests which are parasites of domestic animals and cultivated plants |
IT1188640B (it) * | 1986-03-28 | 1988-01-20 | Montedipe Spa | Processo per la produzione di tricloromelammina |
US4939213A (en) * | 1988-12-19 | 1990-07-03 | American Cyanamid Company | Triazine crosslinking agents and curable compositions containing the same |
US5084541A (en) * | 1988-12-19 | 1992-01-28 | American Cyanamid Company | Triazine crosslinking agents and curable compositions |
-
1992
- 1992-10-30 US US07/968,871 patent/US5288865A/en not_active Expired - Lifetime
- 1992-11-13 DE DE69231759T patent/DE69231759T2/de not_active Expired - Fee Related
- 1992-11-13 EP EP99101493A patent/EP0930303B1/en not_active Expired - Lifetime
- 1992-11-13 ES ES99101493T patent/ES2215338T3/es not_active Expired - Lifetime
- 1992-11-13 DE DE69233001T patent/DE69233001T2/de not_active Expired - Fee Related
- 1992-11-13 EP EP99101466A patent/EP0933371B1/en not_active Expired - Lifetime
- 1992-11-13 AT AT92119485T patent/ATE200078T1/de not_active IP Right Cessation
- 1992-11-13 AT AT99101466T patent/ATE236889T1/de not_active IP Right Cessation
- 1992-11-13 AU AU28361/92A patent/AU655688B2/en not_active Ceased
- 1992-11-13 EP EP99101495A patent/EP0933369A1/en not_active Withdrawn
- 1992-11-13 NO NO924394A patent/NO301711B1/no not_active IP Right Cessation
- 1992-11-13 EP EP99101496A patent/EP0933370A1/en not_active Withdrawn
- 1992-11-13 DE DE69233302T patent/DE69233302T2/de not_active Expired - Fee Related
- 1992-11-13 EP EP92119485A patent/EP0565774B1/en not_active Expired - Lifetime
- 1992-11-13 AT AT99101493T patent/ATE258925T1/de not_active IP Right Cessation
- 1992-11-13 CA CA002082880A patent/CA2082880A1/en not_active Abandoned
- 1992-11-14 KR KR1019920021428A patent/KR100254047B1/ko not_active IP Right Cessation
- 1992-11-16 BR BR929204416A patent/BR9204416A/pt not_active IP Right Cessation
- 1992-11-16 JP JP33005092A patent/JP3435654B2/ja not_active Expired - Fee Related
-
1993
- 1993-11-10 US US08/150,679 patent/US5405959A/en not_active Expired - Lifetime
-
1995
- 1995-03-03 US US08/398,256 patent/US5571915A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
EP0933371A1 (en) | 1999-08-04 |
KR100254047B1 (ko) | 2000-05-01 |
NO924394D0 (no) | 1992-11-13 |
ATE258925T1 (de) | 2004-02-15 |
EP0933370A1 (en) | 1999-08-04 |
CA2082880A1 (en) | 1993-05-16 |
ES2215338T3 (es) | 2004-10-01 |
DE69231759T2 (de) | 2001-10-04 |
US5288865A (en) | 1994-02-22 |
AU2836192A (en) | 1993-05-20 |
EP0933371B1 (en) | 2003-04-09 |
DE69233302D1 (de) | 2004-03-11 |
DE69233302T2 (de) | 2004-07-01 |
EP0565774A2 (en) | 1993-10-20 |
EP0565774A3 (en) | 1994-08-17 |
ATE236889T1 (de) | 2003-04-15 |
EP0930303A2 (en) | 1999-07-21 |
JP3435654B2 (ja) | 2003-08-11 |
DE69233001D1 (de) | 2003-05-15 |
BR9204416A (pt) | 1993-07-20 |
EP0930303A3 (en) | 1999-07-28 |
JPH05239038A (ja) | 1993-09-17 |
EP0930303B1 (en) | 2004-02-04 |
US5571915A (en) | 1996-11-05 |
ATE200078T1 (de) | 2001-04-15 |
EP0933369A1 (en) | 1999-08-04 |
EP0565774B1 (en) | 2001-03-28 |
DE69231759D1 (de) | 2001-05-03 |
US5405959A (en) | 1995-04-11 |
NO301711B1 (no) | 1997-12-01 |
DE69233001T2 (de) | 2004-02-12 |
AU655688B2 (en) | 1995-01-05 |
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