NO831000L - Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblandinger - Google Patents
Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblandingerInfo
- Publication number
- NO831000L NO831000L NO831000A NO831000A NO831000L NO 831000 L NO831000 L NO 831000L NO 831000 A NO831000 A NO 831000A NO 831000 A NO831000 A NO 831000A NO 831000 L NO831000 L NO 831000L
- Authority
- NO
- Norway
- Prior art keywords
- amine
- sulfuric acid
- paraffin
- acid
- weight
- Prior art date
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title claims description 104
- 238000000034 method Methods 0.000 title claims description 22
- 239000011541 reaction mixture Substances 0.000 title claims description 6
- 150000001412 amines Chemical class 0.000 claims description 49
- 239000012188 paraffin wax Substances 0.000 claims description 29
- -1 amine sulfate Chemical class 0.000 claims description 24
- 239000002253 acid Substances 0.000 claims description 23
- 239000000203 mixture Substances 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 150000003839 salts Chemical class 0.000 claims description 5
- 229910021653 sulphate ion Inorganic materials 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 3
- 238000000605 extraction Methods 0.000 claims description 3
- 238000001256 steam distillation Methods 0.000 claims description 3
- 239000003513 alkali Substances 0.000 claims description 2
- 229910001854 alkali hydroxide Inorganic materials 0.000 claims description 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 18
- 238000000926 separation method Methods 0.000 description 18
- 239000012071 phase Substances 0.000 description 17
- JQVDAXLFBXTEQA-UHFFFAOYSA-N dibutylamine Chemical compound CCCCNCCCC JQVDAXLFBXTEQA-UHFFFAOYSA-N 0.000 description 10
- 235000011121 sodium hydroxide Nutrition 0.000 description 6
- 239000000243 solution Substances 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- 125000000217 alkyl group Chemical group 0.000 description 3
- 150000003863 ammonium salts Chemical class 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- CDULGHZNHURECF-UHFFFAOYSA-N 2,3-dimethylaniline 2,4-dimethylaniline 2,5-dimethylaniline 2,6-dimethylaniline 3,4-dimethylaniline 3,5-dimethylaniline Chemical group CC1=CC=C(N)C(C)=C1.CC1=CC=C(C)C(N)=C1.CC1=CC(C)=CC(N)=C1.CC1=CC=C(N)C=C1C.CC1=CC=CC(N)=C1C.CC1=CC=CC(C)=C1N CDULGHZNHURECF-UHFFFAOYSA-N 0.000 description 2
- MLPVBIWIRCKMJV-UHFFFAOYSA-N 2-ethylaniline Chemical compound CCC1=CC=CC=C1N MLPVBIWIRCKMJV-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- OJGMBLNIHDZDGS-UHFFFAOYSA-N N-Ethylaniline Chemical compound CCNC1=CC=CC=C1 OJGMBLNIHDZDGS-UHFFFAOYSA-N 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 125000001931 aliphatic group Chemical group 0.000 description 2
- 125000002947 alkylene group Chemical group 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- PAFZNILMFXTMIY-UHFFFAOYSA-N cyclohexylamine Chemical compound NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000003350 kerosene Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- JACMPVXHEARCBO-UHFFFAOYSA-N n-pentylpentan-1-amine Chemical compound CCCCCNCCCCC JACMPVXHEARCBO-UHFFFAOYSA-N 0.000 description 2
- RNVCVTLRINQCPJ-UHFFFAOYSA-N o-toluidine Chemical compound CC1=CC=CC=C1N RNVCVTLRINQCPJ-UHFFFAOYSA-N 0.000 description 2
- 239000012266 salt solution Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000006277 sulfonation reaction Methods 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 2
- 125000005270 trialkylamine group Chemical group 0.000 description 2
- IMFACGCPASFAPR-UHFFFAOYSA-N tributylamine Chemical compound CCCCN(CCCC)CCCC IMFACGCPASFAPR-UHFFFAOYSA-N 0.000 description 2
- GEYOCULIXLDCMW-UHFFFAOYSA-N 1,2-phenylenediamine Chemical compound NC1=CC=CC=C1N GEYOCULIXLDCMW-UHFFFAOYSA-N 0.000 description 1
- BMVXCPBXGZKUPN-UHFFFAOYSA-N 1-hexanamine Chemical compound CCCCCCN BMVXCPBXGZKUPN-UHFFFAOYSA-N 0.000 description 1
- NJBCRXCAPCODGX-UHFFFAOYSA-N 2-methyl-n-(2-methylpropyl)propan-1-amine Chemical compound CC(C)CNCC(C)C NJBCRXCAPCODGX-UHFFFAOYSA-N 0.000 description 1
- FDECURPHVMNAKO-UHFFFAOYSA-N 4-nonylaniline Chemical compound CCCCCCCCCC1=CC=C(N)C=C1 FDECURPHVMNAKO-UHFFFAOYSA-N 0.000 description 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- XBPCUCUWBYBCDP-UHFFFAOYSA-N Dicyclohexylamine Chemical compound C1CCCCC1NC1CCCCC1 XBPCUCUWBYBCDP-UHFFFAOYSA-N 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- WJYIASZWHGOTOU-UHFFFAOYSA-N Heptylamine Chemical compound CCCCCCCN WJYIASZWHGOTOU-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- OCPOLAAAWHQKCX-UHFFFAOYSA-N dipentylazanium sulfate Chemical compound [O-]S([O-])(=O)=O.CCCCC[NH2+]CCCCC.CCCCC[NH2+]CCCCC OCPOLAAAWHQKCX-UHFFFAOYSA-N 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000012458 free base Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000004530 micro-emulsion Substances 0.000 description 1
- FRQONEWDWWHIPM-UHFFFAOYSA-N n,n-dicyclohexylcyclohexanamine Chemical compound C1CCCCC1N(C1CCCCC1)C1CCCCC1 FRQONEWDWWHIPM-UHFFFAOYSA-N 0.000 description 1
- DIAIBWNEUYXDNL-UHFFFAOYSA-N n,n-dihexylhexan-1-amine Chemical compound CCCCCCN(CCCCCC)CCCCCC DIAIBWNEUYXDNL-UHFFFAOYSA-N 0.000 description 1
- OOHAUGDGCWURIT-UHFFFAOYSA-N n,n-dipentylpentan-1-amine Chemical compound CCCCCN(CCCCC)CCCCC OOHAUGDGCWURIT-UHFFFAOYSA-N 0.000 description 1
- MTHFROHDIWGWFD-UHFFFAOYSA-N n-butyl-n-methylbutan-1-amine Chemical compound CCCCN(C)CCCC MTHFROHDIWGWFD-UHFFFAOYSA-N 0.000 description 1
- 238000006386 neutralization reaction Methods 0.000 description 1
- IOQPZZOEVPZRBK-UHFFFAOYSA-N octan-1-amine Chemical compound CCCCCCCCN IOQPZZOEVPZRBK-UHFFFAOYSA-N 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- RZXMPPFPUUCRFN-UHFFFAOYSA-N p-toluidine Chemical compound CC1=CC=C(N)C=C1 RZXMPPFPUUCRFN-UHFFFAOYSA-N 0.000 description 1
- 229940100684 pentylamine Drugs 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 description 1
- 239000003495 polar organic solvent Substances 0.000 description 1
- 239000002798 polar solvent Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- RPACBEVZENYWOL-XFULWGLBSA-M sodium;(2r)-2-[6-(4-chlorophenoxy)hexyl]oxirane-2-carboxylate Chemical compound [Na+].C=1C=C(Cl)C=CC=1OCCCCCC[C@]1(C(=O)[O-])CO1 RPACBEVZENYWOL-XFULWGLBSA-M 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/42—Separation; Purification; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19823210573 DE3210573A1 (de) | 1982-03-23 | 1982-03-23 | Verfahren zum abtrennen von schwefelsaeure aus dem bei der sulfoxidation von paraffinen anfallenden reaktionsgemisch |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO831000L true NO831000L (no) | 1983-09-26 |
Family
ID=6159035
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO831000A NO831000L (no) | 1982-03-23 | 1983-03-22 | Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblandinger |
Country Status (12)
| Country | Link |
|---|---|
| EP (1) | EP0089653A3 (cs) |
| JP (1) | JPS58172363A (cs) |
| AR (1) | AR229069A1 (cs) |
| AU (1) | AU1270683A (cs) |
| BR (1) | BR8301442A (cs) |
| CS (1) | CS195783A2 (cs) |
| DD (1) | DD209441A5 (cs) |
| DE (1) | DE3210573A1 (cs) |
| ES (1) | ES520801A0 (cs) |
| NO (1) | NO831000L (cs) |
| YU (1) | YU67983A (cs) |
| ZA (1) | ZA831993B (cs) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3801942A1 (de) * | 1988-01-23 | 1989-07-27 | Basf Ag | Verfahren zur herstellung von alkalisalzen der biphenyl-4,4'-disulfonsaeure |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1593860B1 (de) * | 1967-03-15 | 1971-02-11 | Hoechst Ag | Verfahren zur Herstellung von Aminsalzen von n-Paraffinsulfonsaeuren |
| US3719703A (en) * | 1969-04-29 | 1973-03-06 | Atomic Energy Commission | Separation of sulfonic acids from sulfuric acid |
| US3720707A (en) * | 1970-02-27 | 1973-03-13 | Labofina Sa | Process for reducing the sulfuric acid content of alkylarylsulfonic acids |
| IT941650B (it) * | 1970-08-07 | 1973-03-10 | Aquitaine Petrole | Procedimento per la preparazione di acidi solfonici e di solfonati |
| IT1074825B (it) * | 1977-01-11 | 1985-04-20 | Euteco Spa | Procedimento per la purificazione di acidi alchilsolfonici |
| DE3048058C2 (de) * | 1980-12-19 | 1983-04-28 | Hoechst Ag, 6230 Frankfurt | Verfahren zur Abtrennung von Schwefelsäure aus dem bei der Sulfoxidation von n-Paraffinen anfallenden rohen Sulfonierungsgemisch |
-
1982
- 1982-03-23 DE DE19823210573 patent/DE3210573A1/de not_active Withdrawn
-
1983
- 1983-03-19 EP EP83102734A patent/EP0089653A3/de not_active Withdrawn
- 1983-03-21 DD DD83249010A patent/DD209441A5/de unknown
- 1983-03-21 YU YU00679/83A patent/YU67983A/xx unknown
- 1983-03-21 AR AR292452A patent/AR229069A1/es active
- 1983-03-21 ES ES520801A patent/ES520801A0/es active Granted
- 1983-03-22 AU AU12706/83A patent/AU1270683A/en not_active Abandoned
- 1983-03-22 CS CS831957A patent/CS195783A2/cs unknown
- 1983-03-22 JP JP58046088A patent/JPS58172363A/ja active Pending
- 1983-03-22 NO NO831000A patent/NO831000L/no unknown
- 1983-03-22 BR BR8301442A patent/BR8301442A/pt unknown
- 1983-03-22 ZA ZA831993A patent/ZA831993B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BR8301442A (pt) | 1983-11-29 |
| AR229069A1 (es) | 1983-05-31 |
| EP0089653A2 (de) | 1983-09-28 |
| YU67983A (en) | 1986-02-28 |
| EP0089653A3 (de) | 1984-05-23 |
| DE3210573A1 (de) | 1983-10-06 |
| JPS58172363A (ja) | 1983-10-11 |
| DD209441A5 (de) | 1984-05-09 |
| ES8402564A1 (es) | 1984-02-01 |
| CS195783A2 (en) | 1985-07-16 |
| ES520801A0 (es) | 1984-02-01 |
| ZA831993B (en) | 1983-11-30 |
| AU1270683A (en) | 1983-09-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2017533883A (ja) | アルカリイセチオン酸塩およびアルカリビニルスルホン酸塩からタウリンを生産するための循環プロセス | |
| NO831000L (no) | Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblandinger | |
| BR112016026310B1 (pt) | Processo para a reação de compostos químicos | |
| US2820056A (en) | Alkaryl sulfonates | |
| NO814347L (no) | Fremgangsmaate til adskillelse av svovelsyre fra den ved sulfoksydasjon av parafiner dannede reaksjonsblanding | |
| US3063806A (en) | Process for the production of anhydrous hydrazine | |
| EP0593551B1 (en) | Process for making alkyl naphthalene sulfonate surfactants | |
| PT91757B (pt) | Processo de preparacao de gama-butirobetaina | |
| US3577456A (en) | Process for the manufacture of aqueous alkali paraffin sulphonate solutions containing small amounts of alkali sulfate | |
| JPS6038356A (ja) | パラフインのスルホキシド化の際に得られる反応混合物からパラフイン‐スルホン酸またはパラフイン‐スルホナートを穏やかな条件下で単離する方法 | |
| US2413615A (en) | Nicotinic acid processes | |
| JPS60146854A (ja) | ニトリロ三酢酸塩の製造方法 | |
| JP5463839B2 (ja) | ２−ヒドロキシ−４−メチルチオブタン酸の製造方法 | |
| US1406745A (en) | Manufacture of resorcinol | |
| SU48139A1 (ru) | Способ выделени солей кислых сернокислых эфиров лейко-соединений кубовых красителей | |
| SU148808A1 (ru) | Способ получени третичных ароматических алкиламинов | |
| US2407351A (en) | Process for the manufacture of o-sulphobenzoic acids | |
| Fischer et al. | Introduction to the preparation of organic compounds | |
| US1979033A (en) | Process for the manufacture of nsulphoethyl compounds of arylamino sulphonic acids | |
| SU52447A1 (ru) | Способ получени диэтил-амино-пропилового эфира | |
| Robson et al. | The direct isolation of arginine and lysine picrates from gelatin hydrolysates | |
| JP3164691B2 (ja) | β−ナフタレンスルホン酸塩の製造法 | |
| JP2731816B2 (ja) | クレゾールの精製方法 | |
| JPS5885855A (ja) | 光スルホン化脂肪酸エステルまたは石油パラフィンのアルカノ−ルアミン塩の連続的製造方法 | |
| DE707029C (de) | Verfahren zur Herstellung als Druckhilfsstoffe geeigneter quartaerer Ammoniumverbindungen |