NO132870B - - Google Patents
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- Publication number
- NO132870B NO132870B NO3041/71A NO304171A NO132870B NO 132870 B NO132870 B NO 132870B NO 3041/71 A NO3041/71 A NO 3041/71A NO 304171 A NO304171 A NO 304171A NO 132870 B NO132870 B NO 132870B
- Authority
- NO
- Norway
- Prior art keywords
- solution
- dodecylamine
- amine
- butanol
- alcohol
- Prior art date
Links
- 239000002253 acid Substances 0.000 claims abstract description 31
- 150000007513 acids Chemical class 0.000 claims abstract description 26
- 238000000034 method Methods 0.000 claims abstract description 22
- 238000005194 fractionation Methods 0.000 claims abstract description 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 50
- 150000001412 amines Chemical class 0.000 claims description 39
- 229920001732 Lignosulfonate Polymers 0.000 claims description 32
- 238000000605 extraction Methods 0.000 claims description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 27
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 24
- JRBPAEWTRLWTQC-UHFFFAOYSA-N dodecylamine Chemical compound CCCCCCCCCCCCN JRBPAEWTRLWTQC-UHFFFAOYSA-N 0.000 claims description 14
- 239000003513 alkali Substances 0.000 claims description 6
- -1 amine compounds Chemical class 0.000 claims description 6
- 229920006395 saturated elastomer Polymers 0.000 claims description 4
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 claims description 3
- FOGYNLXERPKEGN-UHFFFAOYSA-N 3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfopropyl)phenoxy]propane-1-sulfonic acid Chemical compound COC1=CC=CC(CC(CS(O)(=O)=O)OC=2C(=CC(CCCS(O)(=O)=O)=CC=2)OC)=C1O FOGYNLXERPKEGN-UHFFFAOYSA-N 0.000 claims description 2
- GPRLSGONYQIRFK-UHFFFAOYSA-N hydron Chemical compound [H+] GPRLSGONYQIRFK-UHFFFAOYSA-N 0.000 claims description 2
- 239000007787 solid Substances 0.000 claims description 2
- 230000006735 deficit Effects 0.000 claims 1
- 239000000243 solution Substances 0.000 description 31
- 239000012071 phase Substances 0.000 description 19
- 238000000354 decomposition reaction Methods 0.000 description 11
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 8
- 239000002699 waste material Substances 0.000 description 8
- 229920002678 cellulose Polymers 0.000 description 7
- 239000001913 cellulose Substances 0.000 description 7
- 238000004821 distillation Methods 0.000 description 7
- 239000004117 Lignosulphonate Substances 0.000 description 6
- 150000001875 compounds Chemical class 0.000 description 6
- 235000019357 lignosulphonate Nutrition 0.000 description 6
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 4
- 239000012074 organic phase Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- FWVKYWMWPCRUHC-UHFFFAOYSA-N CCCCO.CCCCCCCCCCCCN Chemical compound CCCCO.CCCCCCCCCCCCN FWVKYWMWPCRUHC-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 229920005610 lignin Polymers 0.000 description 2
- 235000000346 sugar Nutrition 0.000 description 2
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 2
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 description 2
- 235000012141 vanillin Nutrition 0.000 description 2
- 239000002023 wood Substances 0.000 description 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000218657 Picea Species 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 229910001854 alkali hydroxide Inorganic materials 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 150000001447 alkali salts Chemical class 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- GBAOBIBJACZTNA-UHFFFAOYSA-L calcium sulfite Chemical compound [Ca+2].[O-]S([O-])=O GBAOBIBJACZTNA-UHFFFAOYSA-L 0.000 description 1
- 239000004295 calcium sulphite Substances 0.000 description 1
- 235000010261 calcium sulphite Nutrition 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229920000867 polyelectrolyte Polymers 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 150000008163 sugars Chemical class 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 235000011149 sulphuric acid Nutrition 0.000 description 1
- 150000007968 uric acids Chemical class 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H6/00—Macromolecular compounds derived from lignin, e.g. tannins, humic acids
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S210/00—Liquid purification or separation
- Y10S210/928—Paper mill waste, e.g. white water, black liquor treated
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Extraction Or Liquid Replacement (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Compounds Of Unknown Constitution (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FI702238A FI45979C (fi) | 1970-08-14 | 1970-08-14 | Menetelmä lignosulfonihappojen fraktioimiseksi |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NO132870B true NO132870B (OSRAM) | 1975-10-13 |
| NO132870C NO132870C (OSRAM) | 1976-01-21 |
Family
ID=8506837
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO3041/71A NO132870C (OSRAM) | 1970-08-14 | 1971-08-16 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3825526A (OSRAM) |
| CA (1) | CA970771A (OSRAM) |
| CH (1) | CH568329A5 (OSRAM) |
| DE (1) | DE2055292C3 (OSRAM) |
| FI (1) | FI45979C (OSRAM) |
| NO (1) | NO132870C (OSRAM) |
| SE (1) | SE383519B (OSRAM) |
| SU (1) | SU575032A3 (OSRAM) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4111928A (en) * | 1975-08-28 | 1978-09-05 | Holsopple Dale B | Method of separating lignin and making epoxide-lignin |
| FI60873C (fi) * | 1979-05-28 | 1982-04-13 | Tampella Oy Ab | Foerfarande foer avskiljning av lignosulfonsyror och lignosulfonater genom extraktion ur avlut fraon kok av cellulosahaltigt material |
| FI62114C (fi) * | 1979-11-05 | 1982-11-10 | Flowcon Oy | Ligninprodukt foer att goera cement och andra finfoerdelade mieralmaterial laettflytande |
| DE3447686C1 (de) * | 1984-12-28 | 1986-10-30 | Jörg Dipl.-Ing. Dr. Seewalchen Oberkofler | Verfahren zur Herabsetzung der Schleimbildung in Anlagen mit einem Wasserkreislauf und Anwendung des Verfahrens |
| US4988799A (en) * | 1987-08-11 | 1991-01-29 | Daishowa Chemicals Inc. | Lignosulfonate based pharmacologic agent with anti-coagulant and anti-thrombotic activity |
| US4964995A (en) * | 1989-06-16 | 1990-10-23 | Midwest Research Institute | Supercritical separation process for complex organic mixtures |
| CA2070500C (en) * | 1991-06-13 | 1997-10-14 | Ted Mcvay | Reactive phenolic resin modifier |
| US5202403A (en) * | 1992-01-15 | 1993-04-13 | Georgia-Pacific Resins, Inc. | Lignin modified phenol-formaldehyde resins |
-
1970
- 1970-08-14 FI FI702238A patent/FI45979C/fi active
- 1970-11-10 DE DE2055292A patent/DE2055292C3/de not_active Expired
-
1971
- 1971-08-13 SU SU7101692119A patent/SU575032A3/ru active
- 1971-08-13 SE SE7110344-4A patent/SE383519B/xx unknown
- 1971-08-13 US US00171704A patent/US3825526A/en not_active Expired - Lifetime
- 1971-08-13 CH CH1191871A patent/CH568329A5/xx not_active IP Right Cessation
- 1971-08-13 CA CA120,506A patent/CA970771A/en not_active Expired
- 1971-08-16 NO NO3041/71A patent/NO132870C/no unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE2055292A1 (de) | 1972-02-17 |
| NO132870C (OSRAM) | 1976-01-21 |
| DE2055292C3 (de) | 1974-05-22 |
| FI45979C (fi) | 1972-11-10 |
| SU575032A3 (ru) | 1977-09-30 |
| DE2055292B2 (de) | 1973-08-23 |
| CH568329A5 (OSRAM) | 1975-10-31 |
| CA970771A (en) | 1975-07-08 |
| US3825526A (en) | 1974-07-23 |
| FI45979B (OSRAM) | 1972-07-31 |
| SE383519B (sv) | 1976-03-15 |
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