MY156559A - Process for preparing toluenediamine by hydrogenation of dinitrotoluene - Google Patents
Process for preparing toluenediamine by hydrogenation of dinitrotolueneInfo
- Publication number
- MY156559A MY156559A MYPI2012004968A MYPI2012004968A MY156559A MY 156559 A MY156559 A MY 156559A MY PI2012004968 A MYPI2012004968 A MY PI2012004968A MY PI2012004968 A MYPI2012004968 A MY PI2012004968A MY 156559 A MY156559 A MY 156559A
- Authority
- MY
- Malaysia
- Prior art keywords
- reactor
- dinitrotoluene
- toluenediamine
- hydrogenation
- liquid phase
- Prior art date
Links
- DYSXLQBUUOPLBB-UHFFFAOYSA-N 2,3-dinitrotoluene Chemical compound CC1=CC=CC([N+]([O-])=O)=C1[N+]([O-])=O DYSXLQBUUOPLBB-UHFFFAOYSA-N 0.000 title abstract 4
- VOZKAJLKRJDJLL-UHFFFAOYSA-N 2,4-diaminotoluene Chemical compound CC1=CC=C(N)C=C1N VOZKAJLKRJDJLL-UHFFFAOYSA-N 0.000 title abstract 3
- 238000005984 hydrogenation reaction Methods 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000007791 liquid phase Substances 0.000 abstract 4
- 239000003054 catalyst Substances 0.000 abstract 2
- 238000002955 isolation Methods 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical class [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/30—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds
- C07C209/32—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups
- C07C209/36—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of nitrogen-to-oxygen or nitrogen-to-nitrogen bonds by reduction of nitro groups by reduction of nitro groups bound to carbon atoms of six-membered aromatic rings in presence of hydrogen-containing gases and a catalyst
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C211/00—Compounds containing amino groups bound to a carbon skeleton
- C07C211/43—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton
- C07C211/44—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring
- C07C211/49—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to carbon atoms of six-membered aromatic rings of the carbon skeleton having amino groups bound to only one six-membered aromatic ring having at least two amino groups bound to the carbon skeleton
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP10162924 | 2010-05-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MY156559A true MY156559A (en) | 2016-02-26 |
Family
ID=44358176
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MYPI2012004968A MY156559A (en) | 2010-05-17 | 2011-05-09 | Process for preparing toluenediamine by hydrogenation of dinitrotoluene |
Country Status (9)
| Country | Link |
|---|---|
| EP (1) | EP2571844B1 (cg-RX-API-DMAC7.html) |
| JP (1) | JP2013530140A (cg-RX-API-DMAC7.html) |
| KR (1) | KR20130080445A (cg-RX-API-DMAC7.html) |
| CN (1) | CN102892747B (cg-RX-API-DMAC7.html) |
| BR (1) | BR112012027954A2 (cg-RX-API-DMAC7.html) |
| HU (1) | HUE037511T2 (cg-RX-API-DMAC7.html) |
| MY (1) | MY156559A (cg-RX-API-DMAC7.html) |
| SG (1) | SG185374A1 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2011144481A1 (cg-RX-API-DMAC7.html) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BR112013012865A2 (pt) * | 2010-12-06 | 2016-09-06 | Basf Se | processo para preparar aminas aromáticas, método de regular a concentração de nitrocompostos e nitrosocompostos, e aparelho |
| US8835688B2 (en) | 2011-03-16 | 2014-09-16 | Basf Se | Optimized introduction of the starting materials for a process for preparing aromatic amines by hydrogenation of nitroaromatics |
| US8895783B2 (en) | 2012-02-07 | 2014-11-25 | Basf Se | Monitoring of the stoichiometric ratio in the reaction of nitroaromatics with hydrogen |
| BR112014019503A8 (pt) * | 2012-02-07 | 2017-07-11 | Basf Se | Processo contínuo para preparar pelo menos uma amina aromática |
| US9302237B2 (en) | 2013-01-11 | 2016-04-05 | Basf Se | Apparatus and process for the continuous reaction of liquids with gases |
| WO2014108351A1 (de) | 2013-01-11 | 2014-07-17 | Basf Se | Vorrichtung und verfahren zur kontinuierlichen umsetzung von flüssigkeiten mit gasen |
| US9295971B2 (en) | 2013-01-11 | 2016-03-29 | Basf Se | Apparatus and process for the continuous reaction of liquids with gases |
| EP3055284B1 (de) * | 2013-10-08 | 2017-08-30 | Covestro Deutschland AG | Verfahren zur hydrierung von dinitrotoluol in der gasphase zur herstellung von toluylendiamin |
| CN104098475A (zh) * | 2014-07-28 | 2014-10-15 | 淮安嘉诚高新化工股份有限公司 | 二硝基甲苯连续液相催化加氢还原生产二氨基甲苯的装置及方法 |
| WO2018069278A1 (de) * | 2016-10-10 | 2018-04-19 | Basf Se | Katalysatormodifikation mit alkalimetall-, erdalkalimetall- oder seltenerdmetallionen in der kontinuierlichen flüssigphasen-hydrierung von nitroverbindungen |
| CN107325006A (zh) * | 2017-08-04 | 2017-11-07 | 赛鼎工程有限公司 | 一种二硝基甲苯加氢管式增稠的工艺 |
| EP3697753B1 (de) * | 2017-10-16 | 2025-10-01 | Basf Se | Erhöhung der katalysatorselektivität bei der kontinuierlichen hydrierung von nitroverbindungen durch zugabe von ammoniak |
| CN109053462B (zh) * | 2018-08-14 | 2021-11-05 | 浙江今晖新材料股份有限公司 | 一种对氟苯胺的制备方法 |
| CN116440898B (zh) * | 2023-05-08 | 2025-02-07 | 中国科学院金属研究所 | 用于二硝基甲苯加氢反应的原子级分散Pd-Pt催化剂及其制备方法和应用 |
| WO2025257162A1 (en) | 2024-06-11 | 2025-12-18 | Basf Se | Mixture comprising toluene diamine and method for controlling a hydrogenation process for preparing toluene diamine |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60172947A (ja) * | 1984-02-16 | 1985-09-06 | Mitsui Toatsu Chem Inc | トリレンジアミンの連続的製造方法 |
| DE19844901C1 (de) | 1998-09-30 | 1999-11-04 | Bayer Ag | Verfahren zur Dosierung von flüssigen Nitroaromaten mit mehr als einer Nitrogruppe in Reaktoren zur Sumpfphasen-Hydrierung |
| DE59905881D1 (de) | 1998-12-12 | 2003-07-10 | Basf Ag | Verfahren zur herstellung von aminen |
| DE19909168A1 (de) * | 1999-03-03 | 2000-09-07 | Basf Ag | Verfahren zur Herstellung von Aminen |
| DE19909177A1 (de) | 1999-03-03 | 2000-09-07 | Kataleuna Gmbh Catalysts | Katalysator zur Hydrierung funktioneller Gruppen und Verfahren zu seiner Herstellung |
| DE19909176A1 (de) | 1999-03-03 | 2000-09-07 | Kataleuna Gmbh Catalysts | Hydrierkatalysator und Verfahren zu seiner Herstellung |
| JP2006508017A (ja) * | 2002-02-06 | 2006-03-09 | ビーエーエスエフ アクチェンゲゼルシャフト | アミンの製造方法 |
| DE10206214A1 (de) * | 2002-02-15 | 2003-08-28 | Basf Ag | Verfahren zur Herstellung von Aminen |
| DE10349095A1 (de) | 2003-10-17 | 2005-05-19 | Basf Ag | Verfahren zur Herstellung von Aminen |
| EP2155386B1 (de) | 2007-05-10 | 2012-02-22 | Basf Se | Verfahren zur herstellung von aminen |
| BRPI0721717A2 (pt) | 2007-05-29 | 2013-02-13 | Evonik Degussa Gmbh | hidrogenaÇço de compostos nitro, hidrogenaÇço de aromÁticos nitrados, hidrogenaÇço contÍnua de aromÁticos nitrados e catalisadores de ni ativado |
-
2011
- 2011-05-09 SG SG2012079281A patent/SG185374A1/en unknown
- 2011-05-09 JP JP2013510563A patent/JP2013530140A/ja active Pending
- 2011-05-09 KR KR1020127032972A patent/KR20130080445A/ko not_active Withdrawn
- 2011-05-09 EP EP11718109.9A patent/EP2571844B1/de active Active
- 2011-05-09 CN CN201180024339.XA patent/CN102892747B/zh active Active
- 2011-05-09 HU HUE11718109A patent/HUE037511T2/hu unknown
- 2011-05-09 WO PCT/EP2011/057427 patent/WO2011144481A1/de not_active Ceased
- 2011-05-09 MY MYPI2012004968A patent/MY156559A/en unknown
- 2011-05-09 BR BR112012027954A patent/BR112012027954A2/pt not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| CN102892747B (zh) | 2014-05-21 |
| SG185374A1 (en) | 2012-12-28 |
| CN102892747A (zh) | 2013-01-23 |
| EP2571844A1 (de) | 2013-03-27 |
| JP2013530140A (ja) | 2013-07-25 |
| BR112012027954A2 (pt) | 2017-07-25 |
| WO2011144481A1 (de) | 2011-11-24 |
| EP2571844B1 (de) | 2017-10-04 |
| HUE037511T2 (hu) | 2018-09-28 |
| KR20130080445A (ko) | 2013-07-12 |
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