MY126773A - Method for producing alkali methylates - Google Patents

Method for producing alkali methylates

Info

Publication number
MY126773A
MY126773A MYPI20005773A MYPI20005773A MY126773A MY 126773 A MY126773 A MY 126773A MY PI20005773 A MYPI20005773 A MY PI20005773A MY PI20005773 A MYPI20005773 A MY PI20005773A MY 126773 A MY126773 A MY 126773A
Authority
MY
Malaysia
Prior art keywords
column
methanol
reaction
alkali metal
trays
Prior art date
Application number
MYPI20005773A
Other languages
English (en)
Inventor
Hans-Josef Sterzel Dr
Gerd Kaibel Dr
Guth Josef
Holger Friedrich Dr
Burkart Kirsten
Elke Hoffmann Dr
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of MY126773A publication Critical patent/MY126773A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/68Preparation of metal alcoholates
    • C07C29/70Preparation of metal alcoholates by converting hydroxy groups to O-metal groups
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/141Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/28Evaporating with vapour compression
    • B01D1/284Special features relating to the compressed vapour
    • B01D1/2856The compressed vapour is used for heating a reboiler or a heat exchanger outside an evaporator

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
MYPI20005773A 1999-12-08 2000-12-08 Method for producing alkali methylates MY126773A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19959153A DE19959153A1 (de) 1999-12-08 1999-12-08 Verfahren zur Herstellung von Alkalimethylaten

Publications (1)

Publication Number Publication Date
MY126773A true MY126773A (en) 2006-10-31

Family

ID=7931845

Family Applications (1)

Application Number Title Priority Date Filing Date
MYPI20005773A MY126773A (en) 1999-12-08 2000-12-08 Method for producing alkali methylates

Country Status (11)

Country Link
US (1) US6759560B2 (https=)
EP (1) EP1242345B1 (https=)
JP (1) JP4680462B2 (https=)
KR (1) KR100686683B1 (https=)
CN (1) CN1167658C (https=)
AT (1) ATE276222T1 (https=)
AU (1) AU3008501A (https=)
DE (2) DE19959153A1 (https=)
HU (1) HU229495B1 (https=)
MY (1) MY126773A (https=)
WO (1) WO2001042178A1 (https=)

Families Citing this family (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10008634A1 (de) * 2000-02-24 2001-08-30 Basf Ag Trennwandkolonne zur Auftrennung eines Vielstoffgemisches
JP4484572B2 (ja) * 2003-08-21 2010-06-16 昭和電工株式会社 ヘキサフルオロエタンの製造方法およびその用途
CN1298689C (zh) * 2004-08-13 2007-02-07 于志波 碱法生产甲/乙醇钠工艺
JP4229395B2 (ja) * 2004-09-27 2009-02-25 旭化成ケミカルズ株式会社 芳香族カーボネートの工業的製造方法
DE102005062654A1 (de) * 2005-12-23 2007-06-28 Basf Ag Verfahren zur Gewinnung von Alkoholaten
DE102007025904A1 (de) 2007-06-01 2008-12-04 Evonik Degussa Gmbh Verfahren zur Herstellung von Alkalimetallalkoholaten
RU2358963C2 (ru) * 2007-08-10 2009-06-20 Закрытое акционерное общество "Химтэк Инжиниринг" Способ получения метилата калия
US20090134369A1 (en) * 2007-11-26 2009-05-28 Applied Nanoworks, Inc. Metal alkoxides, apparatus for manufacturing metal alkoxides, related methods and uses thereof
WO2010097318A1 (de) 2009-02-26 2010-09-02 Basf Se Verfahren zur destillativen aufarbeitung eines methanol/wasser-gemischs sowie verfahren zur herstellung von alkalimethylaten
JP4803470B2 (ja) * 2009-10-05 2011-10-26 独立行政法人産業技術総合研究所 熱交換型蒸留装置
AR093211A1 (es) 2012-05-10 2015-05-27 Ypf Soc Anonima Metodo para preparar alcoxidos de metales alcalinos
WO2014165100A1 (en) * 2013-03-13 2014-10-09 Bp Corporation North America Inc. Method of recycling centrate to generate steam in a stripper
CN103288593B (zh) * 2013-06-04 2015-06-03 江苏乐科热力科技有限公司 机械蒸气再压缩甲醇钠生产装置及方法
CN103387483B (zh) * 2013-08-14 2015-06-17 重庆紫光化工股份有限公司 甲醇碱金属盐的生产装置和工艺
WO2016083175A1 (de) * 2014-11-24 2016-06-02 Basf Se Herstellung eines metallalkoxids mittels reaktivdestillation
CN108299159B (zh) 2018-03-01 2020-06-12 浙江大学 一种连续制备2-甲基烯丙醇盐醇溶液的方法
CN109199298B (zh) * 2018-10-22 2024-01-23 东莞理工学院 一种除湿干燥装置及洗碗机
CN110204423A (zh) * 2019-07-12 2019-09-06 浙江圣安化工股份有限公司 一种碱金属醇盐的制备方法
EP4077253B1 (de) 2019-12-18 2024-06-12 Basf Se Verfahren zur herstellung von metallalkoholaten
WO2021148175A1 (de) 2020-01-23 2021-07-29 Evonik Functional Solutions Gmbh Verfahren zur energieeffizienten herstellung von natrium- und kaliumalkoholaten
EP4093724B1 (de) 2020-01-23 2024-01-31 Evonik Operations GmbH Verfahren zur gleichzeitigen herstellung von natrium- und kaliumalkoholaten
KR20230118125A (ko) 2020-12-04 2023-08-10 바스프 에스이 알칼리 금속 메톡사이드의 병렬 제조를 위한 통합식방법
TWI828051B (zh) 2021-02-05 2024-01-01 德商贏創運營有限公司 鹼金屬烷氧化物之高能效製備方法
ES3053209T3 (en) 2021-04-16 2026-01-20 Evonik Operations Gmbh Method for the energy-efficient production of alkali metal ethanolates
EP4074685B1 (de) 2021-04-16 2025-09-03 Evonik Operations GmbH Verfahren zur energieeffizienten herstellung von alkalimetallalkoholaten
ES3035391T3 (en) 2021-06-16 2025-09-02 Evonik Operations Gmbh Process for workup of a methanol/water mixture in the production of alkali metal methoxides in a reaction column
CA3247324A1 (en) 2022-04-04 2025-04-14 Evonik Operations Gmbh IMPROVED PROCESS FOR DEPOLYMERIZING POLYETHYLENE TEREPTHALATE
CN118973706A (zh) 2022-04-04 2024-11-15 赢创运营有限公司 聚对苯二甲酸乙二醇酯的解聚的改进方法
KR20250092186A (ko) 2022-10-19 2025-06-23 에보닉 오퍼레이션스 게엠베하 폴리에틸렌 테레프탈레이트의 개선된 탈중합 방법
CN120077092A (zh) 2022-10-19 2025-05-30 赢创运营有限公司 用于聚对苯二甲酸乙二醇酯解聚的改进方法
JP2025536143A (ja) 2022-10-20 2025-10-31 エボニック オペレーションズ ゲーエムベーハー アルカリ金属メトキシドを製造するための改善された方法
KR20250114030A (ko) 2022-11-30 2025-07-28 에보닉 오퍼레이션스 게엠베하 알칼리 금속 메톡사이드를 제조하기 위한 개선된 프로세스
JP2025540297A (ja) 2022-12-07 2025-12-11 エボニック オペレーションズ ゲーエムベーハー 金属アルコキシド化合物の改善された調製プロセス
WO2024125775A1 (de) 2022-12-14 2024-06-20 Evonik Operations Gmbh Verbessertes verfahren zur herstellung von metallalkoholatverbindungen
KR20250139281A (ko) 2023-01-23 2025-09-23 에보닉 오퍼레이션스 게엠베하 저융점 폴리올레핀과 혼합된 폴리알킬렌 테레프탈레이트의 탈중합 방법
EP4655342A1 (en) 2023-01-23 2025-12-03 Evonik Operations GmbH Process for depolymerization of polyalkylene terephthalates in an extruder
WO2024156567A1 (en) 2023-01-23 2024-08-02 Evonik Operations Gmbh Process for depolymerization of polyalkylene terephthalates in an extruder
WO2025125585A1 (en) 2023-12-14 2025-06-19 Basf Se Integrated process for simultaneous preparation of alkali metal methoxides
WO2025125586A1 (en) 2023-12-14 2025-06-19 Basf Se Integrated process for simultaneously preparing alkali metal methoxides
AR134707A1 (es) 2023-12-14 2026-03-04 Basf Se Proceso integrado para la preparación simultánea de metóxidos de metales alcalinos
WO2025233486A1 (en) 2024-05-10 2025-11-13 Basf Se Integrated process for simultaneously preparing n mixtures comprising alkali metal methoxide and methanol and for preparing solid alkali metal methoxide

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE968903C (de) * 1952-05-13 1958-04-10 Huels Chemische Werke Ag Verfahren zur kontinuierlichen Herstellung von Alkalialkoholaten
US2877274A (en) * 1958-01-21 1959-03-10 Du Pont Production of sodium methoxide
DE3413212C1 (de) 1984-04-07 1985-09-12 Dynamit Nobel Ag, 5210 Troisdorf Verfahren zur Herstellung von wasserfreiem Kalium-tert.-butoxid
DE3680358D1 (de) * 1985-02-20 1991-08-29 Ciba Geigy Ag Verfahren zur herstellung von alkalialkoholaten.
DE3701268C1 (de) 1987-01-17 1988-04-14 Dynamit Nobel Ag Verfahren zur kontinuierlichen Herstellung von Kalium-tert.-butoxid
DE3702052C1 (de) * 1987-01-24 1988-07-14 Degussa Verfahren zur Herstellung von Natriumalkoholat hoher Reinheit aus dem Filtrationsrueckstand von schmelzelektrolytisch gewonnenem Rohnatrium
DE3723193A1 (de) * 1987-07-14 1989-01-26 Metallgesellschaft Ag Verfahren zur herstellung von alkoholaten
ES2035594T3 (es) * 1988-03-29 1993-04-16 Elf Atochem S.A. Procedimiento para la preparacion de fluoralcoholatos de sodio.
FI94063C (fi) * 1993-08-17 1995-07-10 Kemira Oy Menetelmä alkalimetalli- tai ammoniumperoksodisulfaattisuolojen ja alkalimetallihydroksidin samanaikaiseksi valmistamiseksi
DE4418488A1 (de) * 1994-05-27 1995-11-30 Basf Ag Verfahren und Vorrichtung zur destillativen Trennung von Stoffgemischen

Also Published As

Publication number Publication date
DE19959153A1 (de) 2001-06-21
HUP0301074A3 (en) 2005-11-28
US6759560B2 (en) 2004-07-06
HU229495B1 (en) 2014-01-28
DE50007815D1 (de) 2004-10-21
KR20020060253A (ko) 2002-07-16
JP4680462B2 (ja) 2011-05-11
AU3008501A (en) 2001-06-18
HUP0301074A2 (hu) 2003-08-28
EP1242345B1 (de) 2004-09-15
US20020183566A1 (en) 2002-12-05
ATE276222T1 (de) 2004-10-15
KR100686683B1 (ko) 2007-02-27
EP1242345A1 (de) 2002-09-25
CN1409696A (zh) 2003-04-09
JP2003516373A (ja) 2003-05-13
CN1167658C (zh) 2004-09-22
WO2001042178A1 (de) 2001-06-14

Similar Documents

Publication Publication Date Title
MY126773A (en) Method for producing alkali methylates
DE50101248D1 (de) Destillative Reinigung von Ammoniak
WO2001044150A3 (en) Continuous process for the preparation of polytrimethylene ether glycol
CN103282336B (zh) 用于生产高纯度新戊二醇的隔壁塔以及使用其的制造方法
MY142637A (en) A method for the esterification of a fatty acid
EP1132365A4 (en) AZEOTROPIC MIXTURE OF 1,1,1,3,3-PENTAFLUORO-PROPANE AND 1,1,1-TRIFLUORO-3-CHLORO-2-PROPENE, A METHOD FOR THE SEPARATION AND CLEANING OF THE SAME, AND A METHOD FOR THE PRODUCTION OF 1,1,1,3 , 3-PENTAFLUOROPROPAN AND 1,1,1-TRIFLUORO-3-CHLORO-PROPENE
MA25363A1 (fr) Procede d'elimination de petrole, de produits petroliers et/ou de polluants chimiques d'un liquide et/ou d'un gaz et/ou d'une surface
CA2299985A1 (en) Integrated deethanizer ethylene fractionation column
EP1013324A3 (de) Gegenstromkolonne mit Flüssigkeitsverteiler
AU3666100A (en) Variable capacity fluid mixture separation apparatus and process
BRPI0615856A2 (pt) processo para preparar dioxolano
FR2804109B1 (fr) Procede de fabrication en continu de triethanolamine, et produit obtenu
BG104648A (en) Continuous method for producing polyamides from aminonitriles
EP0337294A3 (en) Process for purifying nitrogen trifluoride gas
US4802956A (en) Process for the purification of dimethylether by distillation
BG104649A (en) Continuous method for producing polyamides from aminonitriles
JP2004323526A (ja) 高純度トリエチレンジアミン(teda)を蒸留により精製する方法
TW363062B (en) Distillation of ethylene oxide
EP1375481A4 (en) CLEANING PROCEDURE FOR N- (2-HYDROXYETHYL) -2-PYRROLIDONE
CA2031204A1 (en) A process for the production of low cholesterol butter fat or butter, butter (fat), as well as an installation for its production
Hanika et al. 2-Methylpropylacetate synthesis via catalytic distillation
CA2095285A1 (en) A distillation column with vaporous sidestream removal
JPS57140312A (en) Manufacture of trichlorosilane
TH68229B (th) กระบวนการสำหรับการแยกไดแอลคิล คาร์บอเนทออกมาในเชิงอุตสาหกรรม
SU1064997A1 (ru) Способ очистки пирогаза от кислых компонентов