MXPA04006821A

MXPA04006821A - Colorantes cationicos amarillos para tenir material organico.

Colorantes cationicos amarillos para tenir material organico.

Info

Publication number: MXPA04006821A
Authority: MX; Mexico
Prior art keywords: formula; dye; page; line; compound
Prior art date: 2002-01-15

Application number

MXPA04006821A

Other languages

English (en)

Spanish (es)

Inventor

Hauser Julia

Original Assignee

Ciba Sc Holding Ag

Priority date

2002-01-15

Filing date

2003-01-07

Publication date

2004-12-08

2003-01-07 Application filed by Ciba Sc Holding Ag filed Critical Ciba Sc Holding Ag

2004-12-08 Publication of MXPA04006821A publication Critical patent/MXPA04006821A/es

Links

239000000975 dye Substances 0.000 title claims abstract description 272
125000002091 cationic group Chemical group 0.000 title claims abstract description 146
239000011368 organic material Substances 0.000 title claims abstract description 12
239000000203 mixture Substances 0.000 claims abstract description 460
210000004209 hair Anatomy 0.000 claims abstract description 212
238000000034 method Methods 0.000 claims abstract description 151
-1 wool Substances 0.000 claims abstract description 122
102000011782 Keratins Human genes 0.000 claims abstract description 100
108010076876 Keratins Proteins 0.000 claims abstract description 100
238000004043 dyeing Methods 0.000 claims abstract description 91
230000008569 process Effects 0.000 claims abstract description 82
238000002360 preparation method Methods 0.000 claims abstract description 48
229910052739 hydrogen Inorganic materials 0.000 claims abstract description 45
239000001257 hydrogen Substances 0.000 claims abstract description 44
SLRMQYXOBQWXCR-UHFFFAOYSA-N 2154-56-5 Chemical class [CH2]C1=CC=CC=C1 SLRMQYXOBQWXCR-UHFFFAOYSA-N 0.000 claims abstract description 34
150000003254 radicals Chemical class 0.000 claims abstract description 27
150000001450 anions Chemical group 0.000 claims abstract description 20
150000004820 halides Chemical class 0.000 claims abstract description 19
229920002678 cellulose Polymers 0.000 claims abstract description 18
239000001913 cellulose Substances 0.000 claims abstract description 17
XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 claims abstract description 13
239000004952 Polyamide Substances 0.000 claims abstract description 11
239000010985 leather Substances 0.000 claims abstract description 11
229920002647 polyamide Polymers 0.000 claims abstract description 11
210000002268 wool Anatomy 0.000 claims abstract description 11
WCYWZMWISLQXQU-UHFFFAOYSA-N methyl Chemical group [CH3] WCYWZMWISLQXQU-UHFFFAOYSA-N 0.000 claims abstract description 9
239000001043 yellow dye Substances 0.000 claims abstract description 9
239000004677 Nylon Substances 0.000 claims abstract description 6
229920001778 nylon Polymers 0.000 claims abstract description 6
229920000742 Cotton Polymers 0.000 claims abstract description 5
150000001875 compounds Chemical class 0.000 claims description 240
239000000835 fiber Substances 0.000 claims description 109
239000007800 oxidant agent Substances 0.000 claims description 77
238000004040 coloring Methods 0.000 claims description 73
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 72
239000002253 acid Substances 0.000 claims description 70
238000007254 oxidation reaction Methods 0.000 claims description 67
230000003647 oxidation Effects 0.000 claims description 66
230000008878 coupling Effects 0.000 claims description 54
238000010168 coupling process Methods 0.000 claims description 54
238000005859 coupling reaction Methods 0.000 claims description 54
230000001590 oxidative effect Effects 0.000 claims description 36
239000003795 chemical substances by application Substances 0.000 claims description 35
239000002243 precursor Substances 0.000 claims description 29
125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 25
239000000126 substance Substances 0.000 claims description 21
HKOOXMFOFWEVGF-UHFFFAOYSA-N phenylhydrazine Chemical compound NNC1=CC=CC=C1 HKOOXMFOFWEVGF-UHFFFAOYSA-N 0.000 claims description 16
229940067157 phenylhydrazine Drugs 0.000 claims description 16
150000007857 hydrazones Chemical class 0.000 claims description 15
BGUWFUQJCDRPTL-UHFFFAOYSA-N pyridine-4-carbaldehyde Chemical compound O=CC1=CC=NC=C1 BGUWFUQJCDRPTL-UHFFFAOYSA-N 0.000 claims description 15
230000002378 acidificating effect Effects 0.000 claims description 12
239000000463 material Substances 0.000 claims description 11
230000002152 alkylating effect Effects 0.000 claims description 10
150000001989 diazonium salts Chemical class 0.000 claims description 10
238000005956 quaternization reaction Methods 0.000 claims description 10
239000000654 additive Substances 0.000 claims description 8
125000001424 substituent group Chemical group 0.000 claims description 8
230000009471 action Effects 0.000 claims description 7
AJDUTMFFZHIJEM-UHFFFAOYSA-N n-(9,10-dioxoanthracen-1-yl)-4-[4-[[4-[4-[(9,10-dioxoanthracen-1-yl)carbamoyl]phenyl]phenyl]diazenyl]phenyl]benzamide Chemical compound O=C1C2=CC=CC=C2C(=O)C2=C1C=CC=C2NC(=O)C(C=C1)=CC=C1C(C=C1)=CC=C1N=NC(C=C1)=CC=C1C(C=C1)=CC=C1C(=O)NC1=CC=CC2=C1C(=O)C1=CC=CC=C1C2=O AJDUTMFFZHIJEM-UHFFFAOYSA-N 0.000 claims description 5
239000002195 soluble material Substances 0.000 claims 1
150000002431 hydrogen Chemical group 0.000 abstract description 14
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract description 6
239000000982 direct dye Substances 0.000 description 99
239000000243 solution Substances 0.000 description 90
KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 87
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 72
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 60
235000002639 sodium chloride Nutrition 0.000 description 44
239000000985 reactive dye Substances 0.000 description 43
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 42
238000007792 addition Methods 0.000 description 38
238000006243 chemical reaction Methods 0.000 description 38
150000003839 salts Chemical class 0.000 description 37
238000005406 washing Methods 0.000 description 33
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 31
239000000047 product Substances 0.000 description 31
238000003756 stirring Methods 0.000 description 31
235000015165 citric acid Nutrition 0.000 description 29
239000006096 absorbing agent Substances 0.000 description 28
239000000499 gel Substances 0.000 description 27
239000002453 shampoo Substances 0.000 description 27
239000000843 powder Substances 0.000 description 26
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 25
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 25
238000009472 formulation Methods 0.000 description 25
239000002585 base Substances 0.000 description 24
125000004432 carbon atom Chemical group C* 0.000 description 23
239000011541 reaction mixture Substances 0.000 description 22
239000000980 acid dye Substances 0.000 description 19
238000002156 mixing Methods 0.000 description 19
238000010186 staining Methods 0.000 description 19
125000000217 alkyl group Chemical group 0.000 description 17
GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 17
239000002904 solvent Substances 0.000 description 17
235000010980 cellulose Nutrition 0.000 description 16
238000011282 treatment Methods 0.000 description 16
PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 15
239000007795 chemical reaction product Substances 0.000 description 15
239000004094 surface-active agent Substances 0.000 description 15
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 14
239000000194 fatty acid Substances 0.000 description 14
CWLKGDAVCFYWJK-UHFFFAOYSA-N 3-aminophenol Chemical class NC1=CC=CC(O)=C1 CWLKGDAVCFYWJK-UHFFFAOYSA-N 0.000 description 13
WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid group Chemical group C(C1=CC=CC=C1)(=O)O WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 13
239000003086 colorant Substances 0.000 description 13
229920001577 copolymer Polymers 0.000 description 13
235000014113 dietary fatty acids Nutrition 0.000 description 13
229930195729 fatty acid Natural products 0.000 description 13
DNIAPMSPPWPWGF-UHFFFAOYSA-N monopropylene glycol Natural products CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 13
239000003921 oil Substances 0.000 description 13
239000002671 adjuvant Substances 0.000 description 12
239000000839 emulsion Substances 0.000 description 12
229920000642 polymer Polymers 0.000 description 12
239000011734 sodium Substances 0.000 description 12
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 11
239000002537 cosmetic Substances 0.000 description 11
239000006071 cream Substances 0.000 description 11
150000002148 esters Chemical class 0.000 description 11
239000008240 homogeneous mixture Substances 0.000 description 11
229910052757 nitrogen Inorganic materials 0.000 description 11
229910052708 sodium Inorganic materials 0.000 description 11
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 10
CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 10
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 10
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 10
239000003960 organic solvent Substances 0.000 description 10
239000012071 phase Substances 0.000 description 10
GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 10
KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 9
SIKJAQJRHWYJAI-UHFFFAOYSA-N Indole Chemical compound C1=CC=C2NC=CC2=C1 SIKJAQJRHWYJAI-UHFFFAOYSA-N 0.000 description 9
238000013019 agitation Methods 0.000 description 9
229910052799 carbon Inorganic materials 0.000 description 9
239000006260 foam Substances 0.000 description 9
229960001755 resorcinol Drugs 0.000 description 9
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 8
BMTSZVZQNMNPCT-UHFFFAOYSA-N 2-aminopyridin-3-ol Chemical compound NC1=NC=CC=C1O BMTSZVZQNMNPCT-UHFFFAOYSA-N 0.000 description 8
LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 8
QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 8
FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 8
LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 8
IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 8
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
239000005642 Oleic acid Substances 0.000 description 8
ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 8
DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 description 8
150000007513 acids Chemical class 0.000 description 8
125000002252 acyl group Chemical group 0.000 description 8
229910052783 alkali metal Inorganic materials 0.000 description 8
125000000129 anionic group Chemical group 0.000 description 8
239000003963 antioxidant agent Substances 0.000 description 8
235000006708 antioxidants Nutrition 0.000 description 8
150000004665 fatty acids Chemical class 0.000 description 8
QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 8
239000007788 liquid Substances 0.000 description 8
ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 8
239000002304 perfume Substances 0.000 description 8
QGNGOGOOPUYKMC-UHFFFAOYSA-N 4-hydroxy-6-methylaniline Chemical compound CC1=CC(O)=CC=C1N QGNGOGOOPUYKMC-UHFFFAOYSA-N 0.000 description 7
DBFYESDCPWWCHN-UHFFFAOYSA-N 5-amino-2-methylphenol Chemical compound CC1=CC=C(N)C=C1O DBFYESDCPWWCHN-UHFFFAOYSA-N 0.000 description 7
NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 7
150000001299 aldehydes Chemical class 0.000 description 7
239000003945 anionic surfactant Substances 0.000 description 7
KCXMKQUNVWSEMD-UHFFFAOYSA-N benzyl chloride Chemical compound ClCC1=CC=CC=C1 KCXMKQUNVWSEMD-UHFFFAOYSA-N 0.000 description 7
229940073608 benzyl chloride Drugs 0.000 description 7
239000000460 chlorine Substances 0.000 description 7
239000012065 filter cake Substances 0.000 description 7
230000037308 hair color Effects 0.000 description 7
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 7
239000002736 nonionic surfactant Substances 0.000 description 7
239000000546 pharmaceutical excipient Substances 0.000 description 7
229920005862 polyol Polymers 0.000 description 7
229960004063 propylene glycol Drugs 0.000 description 7
235000013772 propylene glycol Nutrition 0.000 description 7
239000011780 sodium chloride Substances 0.000 description 7
QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 6
239000005711 Benzoic acid Substances 0.000 description 6
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 6
WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical compound C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 description 6
FSYKKLYZXJSNPZ-UHFFFAOYSA-N N-methylaminoacetic acid Natural products C[NH2+]CC([O-])=O FSYKKLYZXJSNPZ-UHFFFAOYSA-N 0.000 description 6
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 6
XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 6
150000001412 amines Chemical class 0.000 description 6
ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 description 6
150000004982 aromatic amines Chemical class 0.000 description 6
235000010233 benzoic acid Nutrition 0.000 description 6
229920001296 polysiloxane Polymers 0.000 description 6
238000001953 recrystallisation Methods 0.000 description 6
235000019333 sodium laurylsulphate Nutrition 0.000 description 6
239000007921 spray Substances 0.000 description 6
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 5
OBCSAIDCZQSFQH-UHFFFAOYSA-N 2-methyl-1,4-phenylenediamine Chemical compound CC1=CC(N)=CC=C1N OBCSAIDCZQSFQH-UHFFFAOYSA-N 0.000 description 5
229940018563 3-aminophenol Drugs 0.000 description 5
TWLMSPNQBKSXOP-UHFFFAOYSA-N 6358-09-4 Chemical compound NC1=CC([N+]([O-])=O)=CC(Cl)=C1O TWLMSPNQBKSXOP-UHFFFAOYSA-N 0.000 description 5
108090000790 Enzymes Proteins 0.000 description 5
102000004190 Enzymes Human genes 0.000 description 5
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 5
LUSZGTFNYDARNI-UHFFFAOYSA-N Sesamol Chemical compound OC1=CC=C2OCOC2=C1 LUSZGTFNYDARNI-UHFFFAOYSA-N 0.000 description 5
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 5
229910021529 ammonia Inorganic materials 0.000 description 5
125000003118 aryl group Chemical group 0.000 description 5
235000010323 ascorbic acid Nutrition 0.000 description 5
239000011668 ascorbic acid Substances 0.000 description 5
229960005070 ascorbic acid Drugs 0.000 description 5
238000005574 benzylation reaction Methods 0.000 description 5
MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical group OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 5
238000009826 distribution Methods 0.000 description 5
238000001035 drying Methods 0.000 description 5
235000011187 glycerol Nutrition 0.000 description 5
JZMJDSHXVKJFKW-UHFFFAOYSA-M methyl sulfate(1-) Chemical compound COS([O-])(=O)=O JZMJDSHXVKJFKW-UHFFFAOYSA-M 0.000 description 5
229910052760 oxygen Inorganic materials 0.000 description 5
150000003077 polyols Chemical class 0.000 description 5
229910052700 potassium Inorganic materials 0.000 description 5
239000011591 potassium Substances 0.000 description 5
125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 5
230000009467 reduction Effects 0.000 description 5
235000010265 sodium sulphite Nutrition 0.000 description 5
239000007787 solid Substances 0.000 description 5
239000007858 starting material Substances 0.000 description 5
239000002562 thickening agent Substances 0.000 description 5
BOKGTLAJQHTOKE-UHFFFAOYSA-N 1,5-dihydroxynaphthalene Chemical compound C1=CC=C2C(O)=CC=CC2=C1O BOKGTLAJQHTOKE-UHFFFAOYSA-N 0.000 description 4
HCPJEHJGFKWRFM-UHFFFAOYSA-N 2-amino-5-methylphenol Chemical compound CC1=CC=C(N)C(O)=C1 HCPJEHJGFKWRFM-UHFFFAOYSA-N 0.000 description 4
CDAWCLOXVUBKRW-UHFFFAOYSA-N 2-aminophenol Chemical compound NC1=CC=CC=C1O CDAWCLOXVUBKRW-UHFFFAOYSA-N 0.000 description 4
ZTMADXFOCUXMJE-UHFFFAOYSA-N 2-methylbenzene-1,3-diol Chemical compound CC1=C(O)C=CC=C1O ZTMADXFOCUXMJE-UHFFFAOYSA-N 0.000 description 4
XYRDGCCCBJITBH-UHFFFAOYSA-N 3-amino-2-chloro-6-methylphenol Chemical compound CC1=CC=C(N)C(Cl)=C1O XYRDGCCCBJITBH-UHFFFAOYSA-N 0.000 description 4
IHDBZCJYSHDCKF-UHFFFAOYSA-N 4,6-dichlorotriazine Chemical compound ClC1=CC(Cl)=NN=N1 IHDBZCJYSHDCKF-UHFFFAOYSA-N 0.000 description 4
NZDXSXLYLMHYJA-UHFFFAOYSA-M 4-[(1,3-dimethylimidazol-1-ium-2-yl)diazenyl]-n,n-dimethylaniline;chloride Chemical compound [Cl-].C1=CC(N(C)C)=CC=C1N=NC1=[N+](C)C=CN1C NZDXSXLYLMHYJA-UHFFFAOYSA-M 0.000 description 4
KEVCVWPVGPWWOI-UHFFFAOYSA-N 4-[(1,3-dimethylimidazol-1-ium-2-yl)diazenyl]aniline;chloride Chemical compound [Cl-].CN1C=C[N+](C)=C1N=NC1=CC=C(N)C=C1 KEVCVWPVGPWWOI-UHFFFAOYSA-N 0.000 description 4
PLIKAWJENQZMHA-UHFFFAOYSA-N 4-aminophenol Chemical compound NC1=CC=C(O)C=C1 PLIKAWJENQZMHA-UHFFFAOYSA-N 0.000 description 4
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 4
229910002016 Aerosil® 200 Inorganic materials 0.000 description 4
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
JVTAAEKCZFNVCJ-UHFFFAOYSA-M Lactate Chemical compound CC(O)C([O-])=O JVTAAEKCZFNVCJ-UHFFFAOYSA-M 0.000 description 4
244000208060 Lawsonia inermis Species 0.000 description 4
229910019142 PO4 Inorganic materials 0.000 description 4
SJEYSFABYSGQBG-UHFFFAOYSA-M Patent blue Chemical compound [Na+].C1=CC(N(CC)CC)=CC=C1C(C=1C(=CC(=CC=1)S([O-])(=O)=O)S([O-])(=O)=O)=C1C=CC(=[N+](CC)CC)C=C1 SJEYSFABYSGQBG-UHFFFAOYSA-M 0.000 description 4
ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 4
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 4
239000007983 Tris buffer Substances 0.000 description 4
239000004904 UV filter Substances 0.000 description 4
244000172533 Viola sororia Species 0.000 description 4
RFQSMLBZXQOMKK-UHFFFAOYSA-N [3-[(4,8-diamino-6-bromo-1,5-dioxonaphthalen-2-yl)amino]phenyl]-trimethylazanium;chloride Chemical compound [Cl-].C[N+](C)(C)C1=CC=CC(NC=2C(C3=C(N)C=C(Br)C(=O)C3=C(N)C=2)=O)=C1 RFQSMLBZXQOMKK-UHFFFAOYSA-N 0.000 description 4
239000004480 active ingredient Substances 0.000 description 4
150000008044 alkali metal hydroxides Chemical class 0.000 description 4
150000001340 alkali metals Chemical class 0.000 description 4
239000012670 alkaline solution Substances 0.000 description 4
239000002168 alkylating agent Substances 0.000 description 4
229940100198 alkylating agent Drugs 0.000 description 4
238000005804 alkylation reaction Methods 0.000 description 4
229940083916 aluminum distearate Drugs 0.000 description 4
RDIVANOKKPKCTO-UHFFFAOYSA-K aluminum;octadecanoate;hydroxide Chemical compound [OH-].[Al+3].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O RDIVANOKKPKCTO-UHFFFAOYSA-K 0.000 description 4
229940054051 antipsychotic indole derivative Drugs 0.000 description 4
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