MXPA04004955A - Procedimiento para la recuperacion de caprolactama. - Google Patents
Procedimiento para la recuperacion de caprolactama.Info
- Publication number
- MXPA04004955A MXPA04004955A MXPA04004955A MXPA04004955A MXPA04004955A MX PA04004955 A MXPA04004955 A MX PA04004955A MX PA04004955 A MXPA04004955 A MX PA04004955A MX PA04004955 A MXPA04004955 A MX PA04004955A MX PA04004955 A MXPA04004955 A MX PA04004955A
- Authority
- MX
- Mexico
- Prior art keywords
- caprolactam
- subjecting
- mixture
- water
- recovering
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
- C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
- C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D223/08—Oxygen atoms
- C07D223/10—Oxygen atoms attached in position 2
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/146—Multiple effect distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0033—Other features
- B01D5/0036—Multiple-effect condensation; Fractional condensation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pyrrole Compounds (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Processing Of Solid Wastes (AREA)
- Polyamides (AREA)
Abstract
La invencion describe un procediendo para la recuperacion de caprolactama a partir de una mezcla que comprende caprolactama, agua componentes ligeros y pesados, al someter la mezcla a una primera destilacion con vacio que resulta en un primer producto de fondo que comprende componentes pesados y caprolactama y en un primer producto de evaporacion que comprende caprolactama, agua, lactamas insaturadas y componentes ligeros; y sometiendo al menos una parte de las lactamas insaturadas a una hidrogenacion.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL1019432 | 2001-11-26 | ||
PCT/NL2002/000761 WO2003045911A1 (en) | 2001-11-26 | 2002-11-25 | Process for recovering caprolactam |
Publications (1)
Publication Number | Publication Date |
---|---|
MXPA04004955A true MXPA04004955A (es) | 2004-08-11 |
Family
ID=19774344
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MXPA04004955A MXPA04004955A (es) | 2001-11-26 | 2002-11-25 | Procedimiento para la recuperacion de caprolactama. |
Country Status (15)
Country | Link |
---|---|
US (1) | US7141668B2 (es) |
EP (1) | EP1448518A1 (es) |
JP (1) | JP2005510562A (es) |
KR (1) | KR20040063970A (es) |
CN (1) | CN1277818C (es) |
AU (1) | AU2002347653A1 (es) |
BR (1) | BR0214414A (es) |
CO (1) | CO5590953A2 (es) |
CZ (1) | CZ2004622A3 (es) |
EA (1) | EA007536B1 (es) |
MX (1) | MXPA04004955A (es) |
MY (1) | MY132420A (es) |
PL (1) | PL370209A1 (es) |
TW (1) | TW200408623A (es) |
WO (1) | WO2003045911A1 (es) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10253094A1 (de) * | 2002-11-13 | 2004-05-27 | Basf Ag | Verfahren zur Reinigung von Caprolactam |
MXPA05012688A (es) | 2003-05-23 | 2006-02-22 | Dsm Ip Assets Bv | Proceso para preparar carrolactama por medio de la redistribucion de beckman. |
JP5102491B2 (ja) * | 2003-07-25 | 2012-12-19 | ディーエスエム アイピー アセッツ ビー.ブイ. | カプロラクタムの精製方法 |
JP4755829B2 (ja) * | 2005-01-11 | 2011-08-24 | 花王株式会社 | ピロリジン誘導体の製造方法 |
JP4983041B2 (ja) * | 2006-02-21 | 2012-07-25 | 住友化学株式会社 | カプロラクタムの精製方法 |
EP2123767A1 (en) * | 2008-05-20 | 2009-11-25 | DSM IP Assets B.V. | Preparation of epsilon-caprolactam via lysine cyclisation |
TW201000635A (en) * | 2008-05-20 | 2010-01-01 | Dsm Ip Assets Bv | Preparation of epsilon-caprolactam from (Z)-6,7-dihydro-1H-azepin-2(5H)-one |
EP2123768A1 (en) * | 2008-05-20 | 2009-11-25 | DSM IP Assets B.V. | Preparation of (Z)-6,7-dihydro-1H-azepin-2(5H)-one |
US8202480B2 (en) * | 2009-06-25 | 2012-06-19 | Uop Llc | Apparatus for separating pitch from slurry hydrocracked vacuum gas oil |
US8540870B2 (en) * | 2009-06-25 | 2013-09-24 | Uop Llc | Process for separating pitch from slurry hydrocracked vacuum gas oil |
US8841445B2 (en) | 2012-12-19 | 2014-09-23 | Basf Se | Process for preparing purified caprolactam from the Beckmann rearrangement of cyclohexane oxime |
JP6003755B2 (ja) * | 2012-12-19 | 2016-10-05 | 東レ株式会社 | ラクタムの精製方法 |
DE102013107238A1 (de) | 2013-07-09 | 2015-01-15 | L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude | Verfahren zur Rückgewinnung von Epsilon-Caprolactam aus Extraktwasser |
SG11201702075QA (en) * | 2014-10-29 | 2017-04-27 | Dong A St Co Ltd | Novel pyridopyrimidinone compounds for modulating the catalytic activity of histone lysine demethylases (kdms) |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL8102280A (nl) * | 1981-05-09 | 1982-12-01 | Stamicarbon | Werkwijze voor het zuiveren van epsilon-caprolactam. |
NL8303028A (nl) * | 1983-08-31 | 1985-03-18 | Stamicarbon | Winning van caprolactam uit caprolactam-bevattend destillatie-residu. |
DE3735054A1 (de) * | 1987-10-16 | 1989-04-27 | Basf Ag | Verfahren zur gewinnung von caprolactam aus leichtsiedern oder schwersiedern der caprolactamdestillation oder gemischen derselben |
-
2002
- 2002-11-25 PL PL02370209A patent/PL370209A1/xx not_active Application Discontinuation
- 2002-11-25 CZ CZ2004622A patent/CZ2004622A3/cs unknown
- 2002-11-25 JP JP2003547363A patent/JP2005510562A/ja active Pending
- 2002-11-25 MX MXPA04004955A patent/MXPA04004955A/es active IP Right Grant
- 2002-11-25 EP EP02783832A patent/EP1448518A1/en not_active Withdrawn
- 2002-11-25 AU AU2002347653A patent/AU2002347653A1/en not_active Abandoned
- 2002-11-25 WO PCT/NL2002/000761 patent/WO2003045911A1/en active Application Filing
- 2002-11-25 US US10/495,862 patent/US7141668B2/en not_active Expired - Fee Related
- 2002-11-25 BR BR0214414-0A patent/BR0214414A/pt not_active IP Right Cessation
- 2002-11-25 EA EA200400736A patent/EA007536B1/ru not_active IP Right Cessation
- 2002-11-25 KR KR10-2004-7007900A patent/KR20040063970A/ko not_active Application Discontinuation
- 2002-11-25 CN CNB028235207A patent/CN1277818C/zh not_active Expired - Fee Related
- 2002-11-26 TW TW091134343A patent/TW200408623A/zh unknown
- 2002-11-26 MY MYPI20024417A patent/MY132420A/en unknown
-
2004
- 2004-06-28 CO CO04061091A patent/CO5590953A2/es not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
KR20040063970A (ko) | 2004-07-15 |
PL370209A1 (en) | 2005-05-16 |
CO5590953A2 (es) | 2005-12-30 |
EP1448518A1 (en) | 2004-08-25 |
US20050176954A1 (en) | 2005-08-11 |
CN1277818C (zh) | 2006-10-04 |
CN1596245A (zh) | 2005-03-16 |
AU2002347653A1 (en) | 2003-06-10 |
TW200408623A (en) | 2004-06-01 |
WO2003045911A1 (en) | 2003-06-05 |
EA007536B1 (ru) | 2006-10-27 |
BR0214414A (pt) | 2004-09-14 |
JP2005510562A (ja) | 2005-04-21 |
MY132420A (en) | 2007-10-31 |
CZ2004622A3 (cs) | 2004-10-13 |
US7141668B2 (en) | 2006-11-28 |
EA200400736A1 (ru) | 2004-10-28 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
MXPA04004955A (es) | Procedimiento para la recuperacion de caprolactama. | |
IL148194A0 (en) | A method of producing a compressed product | |
AU1703502A (en) | Method and device for obtaining 1,3 pure butadiene from 1,3 raw butadiene by distillation | |
PL327478A1 (en) | Method of depolymerising polyamides | |
BG104776A (en) | Method for the production of phenol, methylethylketone and acetone | |
TW200616947A (en) | Process | |
MY115717A (en) | Process for the distillation of alcohols | |
BG104590A (en) | Method for acetone hydration | |
MXPA05014144A (es) | Metodo de fabricacion de cemento portland de adquisicion temprana de alta resistencia. | |
AU2102397A (en) | Purification method | |
AU8297001A (en) | Method for production of rare carotenoids from commercially available lutein | |
AU6856598A (en) | Process for recovering caprolactam from a neutralized rearrangement mixture | |
BG104699A (en) | Method for producing polyamides | |
HUP9801083A3 (en) | Process for producing (15,4r)- or (1r,4s)-4-[(2-amino-6-chloro-9h-purin)-9-yl]-2-cyclopentene-1-methanol | |
TW328081B (en) | A separation process of pivalic acid | |
AU1662495A (en) | Skin package | |
TW375603B (en) | Separation of 2-aminomethyl cyclopentylamine from a mixture comprising hexamethylenediamine and 2-aminomethyl cyclopentylamine | |
GB9711484D0 (en) | Recovery of products from toluenediisocyanate residues | |
WO2002072723A3 (en) | Gelatin manufacturing process and product | |
AU7652100A (en) | Method for extracting bacterio-rhodopsin | |
CA2337321A1 (fr) | Procede de distillation d'ammoniac | |
IL152295A0 (en) | Method for producing 2-alkyl-3-chlorophenols | |
IL133923A0 (en) | Method for preparing 3-cyano-2,4-dihalogen-5-fluoro-benzoic acid | |
BR9912484B1 (pt) | Processo de separação da água de uma solução aquosa de lactama | |
MXPA05011240A (es) | Envase para articulos planos comprimibles. |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG | Grant or registration |