MXPA04004955A - Procedimiento para la recuperacion de caprolactama. - Google Patents

Procedimiento para la recuperacion de caprolactama.

Info

Publication number
MXPA04004955A
MXPA04004955A MXPA04004955A MXPA04004955A MXPA04004955A MX PA04004955 A MXPA04004955 A MX PA04004955A MX PA04004955 A MXPA04004955 A MX PA04004955A MX PA04004955 A MXPA04004955 A MX PA04004955A MX PA04004955 A MXPA04004955 A MX PA04004955A
Authority
MX
Mexico
Prior art keywords
caprolactam
subjecting
mixture
water
recovering
Prior art date
Application number
MXPA04004955A
Other languages
English (en)
Inventor
Gerardus Wilhelmus Adria Hangx
Original Assignee
Dsm Ip Assets Bv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dsm Ip Assets Bv filed Critical Dsm Ip Assets Bv
Publication of MXPA04004955A publication Critical patent/MXPA04004955A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D223/00Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
    • C07D223/02Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D223/06Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D223/08Oxygen atoms
    • C07D223/10Oxygen atoms attached in position 2
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D201/00Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/16Separation or purification
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/143Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/146Multiple effect distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0033Other features
    • B01D5/0036Multiple-effect condensation; Fractional condensation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyrrole Compounds (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Processing Of Solid Wastes (AREA)
  • Polyamides (AREA)

Abstract

La invencion describe un procediendo para la recuperacion de caprolactama a partir de una mezcla que comprende caprolactama, agua componentes ligeros y pesados, al someter la mezcla a una primera destilacion con vacio que resulta en un primer producto de fondo que comprende componentes pesados y caprolactama y en un primer producto de evaporacion que comprende caprolactama, agua, lactamas insaturadas y componentes ligeros; y sometiendo al menos una parte de las lactamas insaturadas a una hidrogenacion.
MXPA04004955A 2001-11-26 2002-11-25 Procedimiento para la recuperacion de caprolactama. MXPA04004955A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NL1019432 2001-11-26
PCT/NL2002/000761 WO2003045911A1 (en) 2001-11-26 2002-11-25 Process for recovering caprolactam

Publications (1)

Publication Number Publication Date
MXPA04004955A true MXPA04004955A (es) 2004-08-11

Family

ID=19774344

Family Applications (1)

Application Number Title Priority Date Filing Date
MXPA04004955A MXPA04004955A (es) 2001-11-26 2002-11-25 Procedimiento para la recuperacion de caprolactama.

Country Status (15)

Country Link
US (1) US7141668B2 (es)
EP (1) EP1448518A1 (es)
JP (1) JP2005510562A (es)
KR (1) KR20040063970A (es)
CN (1) CN1277818C (es)
AU (1) AU2002347653A1 (es)
BR (1) BR0214414A (es)
CO (1) CO5590953A2 (es)
CZ (1) CZ2004622A3 (es)
EA (1) EA007536B1 (es)
MX (1) MXPA04004955A (es)
MY (1) MY132420A (es)
PL (1) PL370209A1 (es)
TW (1) TW200408623A (es)
WO (1) WO2003045911A1 (es)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10253094A1 (de) * 2002-11-13 2004-05-27 Basf Ag Verfahren zur Reinigung von Caprolactam
MXPA05012688A (es) 2003-05-23 2006-02-22 Dsm Ip Assets Bv Proceso para preparar carrolactama por medio de la redistribucion de beckman.
JP5102491B2 (ja) * 2003-07-25 2012-12-19 ディーエスエム アイピー アセッツ ビー.ブイ. カプロラクタムの精製方法
JP4755829B2 (ja) * 2005-01-11 2011-08-24 花王株式会社 ピロリジン誘導体の製造方法
JP4983041B2 (ja) * 2006-02-21 2012-07-25 住友化学株式会社 カプロラクタムの精製方法
EP2123767A1 (en) * 2008-05-20 2009-11-25 DSM IP Assets B.V. Preparation of epsilon-caprolactam via lysine cyclisation
TW201000635A (en) * 2008-05-20 2010-01-01 Dsm Ip Assets Bv Preparation of epsilon-caprolactam from (Z)-6,7-dihydro-1H-azepin-2(5H)-one
EP2123768A1 (en) * 2008-05-20 2009-11-25 DSM IP Assets B.V. Preparation of (Z)-6,7-dihydro-1H-azepin-2(5H)-one
US8202480B2 (en) * 2009-06-25 2012-06-19 Uop Llc Apparatus for separating pitch from slurry hydrocracked vacuum gas oil
US8540870B2 (en) * 2009-06-25 2013-09-24 Uop Llc Process for separating pitch from slurry hydrocracked vacuum gas oil
US8841445B2 (en) 2012-12-19 2014-09-23 Basf Se Process for preparing purified caprolactam from the Beckmann rearrangement of cyclohexane oxime
JP6003755B2 (ja) * 2012-12-19 2016-10-05 東レ株式会社 ラクタムの精製方法
DE102013107238A1 (de) 2013-07-09 2015-01-15 L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Verfahren zur Rückgewinnung von Epsilon-Caprolactam aus Extraktwasser
SG11201702075QA (en) * 2014-10-29 2017-04-27 Dong A St Co Ltd Novel pyridopyrimidinone compounds for modulating the catalytic activity of histone lysine demethylases (kdms)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL8102280A (nl) * 1981-05-09 1982-12-01 Stamicarbon Werkwijze voor het zuiveren van epsilon-caprolactam.
NL8303028A (nl) * 1983-08-31 1985-03-18 Stamicarbon Winning van caprolactam uit caprolactam-bevattend destillatie-residu.
DE3735054A1 (de) * 1987-10-16 1989-04-27 Basf Ag Verfahren zur gewinnung von caprolactam aus leichtsiedern oder schwersiedern der caprolactamdestillation oder gemischen derselben

Also Published As

Publication number Publication date
KR20040063970A (ko) 2004-07-15
PL370209A1 (en) 2005-05-16
CO5590953A2 (es) 2005-12-30
EP1448518A1 (en) 2004-08-25
US20050176954A1 (en) 2005-08-11
CN1277818C (zh) 2006-10-04
CN1596245A (zh) 2005-03-16
AU2002347653A1 (en) 2003-06-10
TW200408623A (en) 2004-06-01
WO2003045911A1 (en) 2003-06-05
EA007536B1 (ru) 2006-10-27
BR0214414A (pt) 2004-09-14
JP2005510562A (ja) 2005-04-21
MY132420A (en) 2007-10-31
CZ2004622A3 (cs) 2004-10-13
US7141668B2 (en) 2006-11-28
EA200400736A1 (ru) 2004-10-28

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