MX369608B - Proceso para la separacion de metacroleina. - Google Patents

Proceso para la separacion de metacroleina.

Info

Publication number
MX369608B
MX369608B MX2016005046A MX2016005046A MX369608B MX 369608 B MX369608 B MX 369608B MX 2016005046 A MX2016005046 A MX 2016005046A MX 2016005046 A MX2016005046 A MX 2016005046A MX 369608 B MX369608 B MX 369608B
Authority
MX
Mexico
Prior art keywords
methacrolein
separating methacrolein
separating
disclosed
methyl methacrylate
Prior art date
Application number
MX2016005046A
Other languages
English (en)
Other versions
MX2016005046A (es
Inventor
A Kraptchetov Dmitri
William Hoy Stacy Iv
A Silvano Mark
Original Assignee
Rohm & Haas
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rohm & Haas filed Critical Rohm & Haas
Publication of MX2016005046A publication Critical patent/MX2016005046A/es
Publication of MX369608B publication Critical patent/MX369608B/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78Separation; Purification; Stabilisation; Use of additives
    • C07C45/81Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C07C45/83Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation by extractive distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/49Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide
    • C07C45/50Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide by oxo-reactions
    • C07C45/505Asymmetric hydroformylation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/65Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78Separation; Purification; Stabilisation; Use of additives
    • C07C45/80Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78Separation; Purification; Stabilisation; Use of additives
    • C07C45/81Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C45/82Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C47/00Compounds having —CHO groups
    • C07C47/20Unsaturated compounds having —CHO groups bound to acyclic carbon atoms
    • C07C47/21Unsaturated compounds having —CHO groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C47/22Acryaldehyde; Methacryaldehyde
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/44Preparation of carboxylic acid esters by oxidation-reduction of aldehydes, e.g. Tishchenko reaction

Abstract

Un proceso para la preparación de metacroleína seca, y un proceso para la producción de metacrilato de metilo se describen.
MX2016005046A 2013-10-28 2014-09-18 Proceso para la separacion de metacroleina. MX369608B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201361896378P 2013-10-28 2013-10-28
PCT/US2014/056268 WO2015065610A1 (en) 2013-10-28 2014-09-18 Process for separating methacrolein

Publications (2)

Publication Number Publication Date
MX2016005046A MX2016005046A (es) 2016-08-03
MX369608B true MX369608B (es) 2019-11-13

Family

ID=51656116

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2016005046A MX369608B (es) 2013-10-28 2014-09-18 Proceso para la separacion de metacroleina.

Country Status (11)

Country Link
US (1) US9765007B2 (es)
EP (1) EP3063117B1 (es)
JP (1) JP6382969B2 (es)
KR (1) KR102291247B1 (es)
CN (1) CN105683142B (es)
CA (1) CA2928807C (es)
MX (1) MX369608B (es)
SA (1) SA516371005B1 (es)
SG (1) SG11201601819WA (es)
TW (1) TW201536398A (es)
WO (1) WO2015065610A1 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3630711B1 (en) * 2017-05-25 2021-03-17 Rohm and Haas Company Process for preparing methacrolein
KR102567203B1 (ko) 2017-05-25 2023-08-16 롬 앤드 하아스 컴패니 메타크롤레인의 제조 방법
EP3613726A1 (en) * 2018-08-21 2020-02-26 Röhm GmbH Continuous process for preparing methacrolein
EP3786146A1 (de) 2019-08-30 2021-03-03 Röhm GmbH Verfahren zur herstellung von methacrolein aus formaldehyd und propionaldehyd sowie herstellanlage hierfür
EP3786147A1 (de) 2019-08-30 2021-03-03 Röhm GmbH Verfahren zur herstellung von methacrolein aus formaldehyd und propionaldehyd sowie herstellanlage hierfür
CN117916217A (zh) 2021-09-06 2024-04-19 罗姆化学有限责任公司 甲基丙烯醛合成中优化的催化剂后处理和再循环

Family Cites Families (34)

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US2514967A (en) 1948-09-17 1950-07-11 Shell Dev Refining and concentrating crude unsaturated aldehydes
GB825021A (en) * 1956-05-09 1959-12-09 Celanese Corp Unsaturated aldehydes
US3098798A (en) * 1960-03-18 1963-07-23 Du Pont Preparation of purified methacrolein
US3597880A (en) 1969-03-14 1971-08-10 Leo I Norgiel Ice-skating grinding apparatus
JPS4823409B1 (es) * 1970-03-04 1973-07-13
JPS547768B2 (es) 1973-01-06 1979-04-10
US4247486A (en) 1977-03-11 1981-01-27 Union Carbide Corporation Cyclic hydroformylation process
GB2008430B (en) 1977-11-17 1982-04-28 Asahi Chemical Ind Process for producing carboxylic esters
JPS5823409B2 (ja) * 1978-03-02 1983-05-14 川崎化成工業株式会社 ゴムの老化防止剤
DE3018071C2 (de) 1979-05-17 1985-06-05 Asahi Kasei Kogyo K.K., Osaka Verfahren zur Herstellung von Carbonsäureestern
DE3213681A1 (de) 1982-04-14 1983-10-27 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von (alpha)-alkylacroleinen
JPS58198442A (ja) 1982-05-14 1983-11-18 Asahi Chem Ind Co Ltd メタクリル酸メチル又はアクリル酸メチルの改良製造方法
US4492613A (en) * 1982-08-02 1985-01-08 The B. F. Goodrich Company Recovery of components of a binary azeotrope
JPH062700B2 (ja) * 1985-10-29 1994-01-12 三井東圧化学株式会社 メタクロレインの分離法
US4716250A (en) 1986-07-10 1987-12-29 Union Carbide Corporation Hydroformylation using low volatile/organic soluble phosphine ligands
US4731486A (en) 1986-11-18 1988-03-15 Union Carbide Corporation Hydroformylation using low volatile phosphine ligands
US5087763A (en) 1990-11-09 1992-02-11 Union Carbide Chemicals & Plastics Technology Corporation Hydroformylation process
DE4225321A1 (de) * 1992-07-31 1994-02-03 Basf Ag Verfahren zur Abtrennung von Methacrolein aus einem gasförmigen Gemisch
US5288918A (en) 1992-09-29 1994-02-22 Union Carbide Chemicals & Plastics Technology Corporation Hydroformylation process
DE69632788T2 (de) 1995-07-18 2005-07-14 Asahi Kasei Chemicals Corp. Katalysator zur herstellung von carbonsäureestern
DE19536132A1 (de) 1995-09-28 1997-04-03 Daimler Benz Aerospace Ag Hohlleiteroszillator
JPH09216850A (ja) 1996-02-09 1997-08-19 Mitsubishi Rayon Co Ltd カルボン酸エステルの製造方法
TW385304B (en) 1996-09-10 2000-03-21 Asahi Chemical Ind Process for producing methacrylic acid ester or acrylic acid ester
SG71815A1 (en) 1997-07-08 2000-04-18 Asahi Chemical Ind Method of producing methyl methacrylate
US7141702B2 (en) 2004-03-26 2006-11-28 Council Of Scientific And Industrial Research Process for the synthesis of α-substituted acroleins
CN100368368C (zh) 2006-02-28 2008-02-13 中国科学院过程工程研究所 一种甲基丙烯酸甲酯生产中甲基丙烯醛的分离方法
CN101020625B (zh) * 2007-03-12 2010-05-19 中国科学院过程工程研究所 一种用离子液体吸收甲基丙烯醛的方法
JP5058915B2 (ja) * 2007-09-20 2012-10-24 ローム アンド ハース カンパニー エタンからエチレン及び一酸化炭素の混合物を製造するための触媒プロセス
EP2740535A1 (en) 2012-12-04 2014-06-11 Dow Technology Investments LLC Bidentate ligands for hydroformylation of ethylene
US20140206897A1 (en) 2013-01-22 2014-07-24 Saudi Basic Industries Corporation Method for making methyl methacrylate from propionaldehyde and formaldehyde via oxidative esterification
TW201509522A (zh) 2013-07-29 2015-03-16 Rohm & Haas 氧化酯化催化劑
TW201512168A (zh) 2013-07-29 2015-04-01 Rohm & Haas 氧化酯化方法
TW201509901A (zh) 2013-07-29 2015-03-16 Rohm & Haas 氧化酯化方法

Also Published As

Publication number Publication date
EP3063117B1 (en) 2020-01-08
SA516371005B1 (ar) 2018-01-09
CN105683142A (zh) 2016-06-15
CA2928807A1 (en) 2015-05-07
JP6382969B2 (ja) 2018-08-29
KR20160078367A (ko) 2016-07-04
SG11201601819WA (en) 2016-05-30
JP2016538259A (ja) 2016-12-08
CN105683142B (zh) 2018-11-13
KR102291247B1 (ko) 2021-08-20
US20160229779A1 (en) 2016-08-11
CA2928807C (en) 2023-03-21
EP3063117A1 (en) 2016-09-07
US9765007B2 (en) 2017-09-19
MX2016005046A (es) 2016-08-03
WO2015065610A1 (en) 2015-05-07
TW201536398A (zh) 2015-10-01

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