MX365785B - Metodo para la purificacion de acidos carboxilicos a partir de los caldos de fermentacion. - Google Patents
Metodo para la purificacion de acidos carboxilicos a partir de los caldos de fermentacion.Info
- Publication number
- MX365785B MX365785B MX2015008597A MX2015008597A MX365785B MX 365785 B MX365785 B MX 365785B MX 2015008597 A MX2015008597 A MX 2015008597A MX 2015008597 A MX2015008597 A MX 2015008597A MX 365785 B MX365785 B MX 365785B
- Authority
- MX
- Mexico
- Prior art keywords
- carboxylic acid
- concentration
- solution containing
- evaporation
- purifying
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/02—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor with moving adsorbents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D61/00—Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
- B01D61/02—Reverse osmosis; Hyperfiltration ; Nanofiltration
- B01D61/025—Reverse osmosis; Hyperfiltration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2311/00—Details relating to membrane separation process operations and control
- B01D2311/02—Specific process operations before starting the membrane separation process
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Water Supply & Treatment (AREA)
- Analytical Chemistry (AREA)
- Nanotechnology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
La invención se refiere a un procedimiento y un dispositivo para la separación y purificación de ácidos carboxílicos de caldos de fermentación que contienen sales amonio de ácidos carboxílicos, comprendiendo el procedimiento las siguientes etapas, a) una separación de biomasa y de solidos eventualmente presentes a partir del caldo de fermentación, b) preparación de una disolución que contiene el ácido carboxílico deseado y de otra disolución que contiene sales de amonio, llevándose a cabo una cromatografía en el lecho móvil simulado (SMB), c) una purificación fina de la disolución que contiene el ácido carboxílico deseado de la etapa b) del procedimiento, d) una concentración de la disolución purificada de ácido carboxílico de la etapa c) del procedimiento, e) cristalización de la disolución concentrada de ácido carboxílico de la etapa d) del procedimiento, f) una concentración de la disolución adicional que contiene sales de amonio de la etapa b) del procedimiento, caracterizado porque en las etapas d) y f) del procedimiento en la concentración se lleva a cabo una combinación a base de ósmosis inversa y vaporización, y el vapor de la vaporización de la etapa f) del procedimiento se conduce a la vaporización de la etapa d) del procedimiento.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102013000027.0A DE102013000027A1 (de) | 2013-01-03 | 2013-01-03 | Verfahren zur Aufreinigung von Carbonsäuren aus Fermentationsbrühen |
PCT/EP2013/003892 WO2014106532A2 (de) | 2013-01-03 | 2013-12-20 | Verfahren zur aufreinigung von carbonsäuren aus fermentationsbrühen |
Publications (2)
Publication Number | Publication Date |
---|---|
MX2015008597A MX2015008597A (es) | 2016-01-15 |
MX365785B true MX365785B (es) | 2019-06-05 |
Family
ID=50101851
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2015008597A MX365785B (es) | 2013-01-03 | 2013-12-20 | Metodo para la purificacion de acidos carboxilicos a partir de los caldos de fermentacion. |
Country Status (10)
Country | Link |
---|---|
US (1) | US9422220B2 (es) |
EP (1) | EP2941412B1 (es) |
CN (1) | CN105073703A (es) |
BR (1) | BR112015015931B1 (es) |
DE (1) | DE102013000027A1 (es) |
HU (1) | HUE042352T2 (es) |
MX (1) | MX365785B (es) |
MY (1) | MY185170A (es) |
PL (1) | PL2941412T3 (es) |
WO (1) | WO2014106532A2 (es) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102014213637A1 (de) * | 2014-07-14 | 2016-01-14 | Thyssenkrupp Ag | Verfahren und Vorrichtung zur Aufkonzentration und Kristallisation von fermentierbaren Carbonsäuren |
FR3028864B1 (fr) | 2014-11-26 | 2018-05-18 | Roquette Freres | Procede de recuperation de cristaux d'acide succinique avec mise en œuvre de tensioactifs au cours de la cristallisation, cristaux obtenus et leurs utilisations |
BR112017011767B1 (pt) * | 2014-12-02 | 2020-12-08 | Dsm Ip Assets B.V. | processo para fabricação de ácido succínico a partir de um caldo de fermentação com uso de nanofiltração para purificar licor-mãe reciclado |
DE102015216815A1 (de) | 2015-09-02 | 2017-03-02 | Thyssenkrupp Ag | Verfahren und Anlage zur Gewinnung einer in einem Fermentationsprozess hergestellten Carbonsäure |
DE102016119938A1 (de) | 2016-10-19 | 2018-04-19 | Thyssenkrupp Ag | Reinigung und Konzentrierung von Carbonsäuren aus Fermentationsprozessen |
CN110498740A (zh) * | 2019-09-18 | 2019-11-26 | 重庆医药高等专科学校 | 一种生产3-羟基丙酸的方法 |
EP3822356A1 (en) * | 2019-11-18 | 2021-05-19 | Corvay Bioproducts GmbH | Method for the production of a dicarboxylic acid |
CN111635302B (zh) * | 2020-07-08 | 2021-06-15 | 江南大学 | 一种多柱连续色谱除盐以纯化羟基乙酸的方法 |
IT202000017368A1 (it) | 2020-07-16 | 2022-01-16 | Radici Chimica S P A | Purificazione di acidi dicarbossilici alifatici prodotti mediante processi biotecnologici |
CN113185397B (zh) * | 2021-04-09 | 2023-12-01 | 安徽丰原集团有限公司 | 一种从发酵液中回收苹果酸的方法 |
EP4352036A1 (en) * | 2021-06-09 | 2024-04-17 | Avantium Knowledge Centre B.V. | Process and system for the recovery of glyoxylic acid |
WO2024097329A1 (en) * | 2022-11-02 | 2024-05-10 | Amalgamated Research Llc | Smb separator for organic acid purification using a strong acid cation resin |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3328093A1 (de) | 1983-08-04 | 1985-02-21 | Hoechst Ag, 6230 Frankfurt | Isolierung von durch fermentation erzeugten carbonsaeuren |
US5168055A (en) | 1986-06-11 | 1992-12-01 | Rathin Datta | Fermentation and purification process for succinic acid |
US5143834A (en) | 1986-06-11 | 1992-09-01 | Glassner David A | Process for the production and purification of succinic acid |
US5034105A (en) | 1989-07-27 | 1991-07-23 | Michigan Biotechnology Institute | Carboxylic acid purification and crystallization process |
WO1993006226A1 (en) | 1991-09-13 | 1993-04-01 | Purdue Research Foundation | Fermentation process for producing lactic acid |
BE1011197A3 (fr) | 1997-06-06 | 1999-06-01 | Brussels Biotech En Abrege Bb | Procede de purification d'acide lactique. |
US5958744A (en) | 1997-08-18 | 1999-09-28 | Applied Carbochemicals | Succinic acid production and purification |
US6229046B1 (en) | 1997-10-14 | 2001-05-08 | Cargill, Incorported | Lactic acid processing methods arrangements and products |
US6034269A (en) * | 1998-08-03 | 2000-03-07 | E. I. Du Pont De Nemours And Company | Process for producing pure carboxylic acids |
US6291708B1 (en) | 1999-04-28 | 2001-09-18 | A.E. Staley Manufacturing Co. | Process for production of organic acids and esters thereof |
DE19939630C2 (de) | 1999-08-20 | 2001-07-12 | Mg Technologies Ag | Verfahren zum Feinreinigen einer wässrigen Lösung, die eine fermentativ hergestellte organische Säure enthält |
US7381386B2 (en) * | 2003-06-05 | 2008-06-03 | Eastman Chemical Company | Extraction process for removal of impurities from mother liquor in the synthesis of carboxylic acid |
DE102004026152A1 (de) | 2004-05-28 | 2005-12-15 | Basf Ag | Fermentative Herstellung von Feinchemikalien |
WO2006124633A1 (en) | 2005-05-13 | 2006-11-23 | Cargill, Incorporated | Production of lactic acid |
DE102007045701B3 (de) | 2007-09-24 | 2009-05-14 | Uhde Gmbh | Gewinnung von Milchsäure durch Fermentation und Extraktion mit Aminen |
DE102009019248A1 (de) | 2009-04-30 | 2010-11-04 | Uhde Gmbh | Isolierung von organischen Säuren aus Fermenterbrühe mit Hilfe chromatographischer Methoden |
JP2013516180A (ja) * | 2009-12-31 | 2013-05-13 | ミリアント・コーポレイション | コハク酸アンモニウムを含有する発酵ブロスからのコハク酸の精製 |
DE102010025167A1 (de) * | 2010-06-25 | 2011-12-29 | Uhde Gmbh | Verfahren zur Abtrennung, Gewinnung und Reinigung von Bernsteinsäure |
-
2013
- 2013-01-03 DE DE102013000027.0A patent/DE102013000027A1/de not_active Ceased
- 2013-12-20 MX MX2015008597A patent/MX365785B/es active IP Right Grant
- 2013-12-20 WO PCT/EP2013/003892 patent/WO2014106532A2/de active Application Filing
- 2013-12-20 US US14/759,141 patent/US9422220B2/en active Active
- 2013-12-20 HU HUE13829059A patent/HUE042352T2/hu unknown
- 2013-12-20 EP EP13829059.8A patent/EP2941412B1/de active Active
- 2013-12-20 BR BR112015015931-1A patent/BR112015015931B1/pt not_active IP Right Cessation
- 2013-12-20 MY MYPI2015001704A patent/MY185170A/en unknown
- 2013-12-20 CN CN201380072983.3A patent/CN105073703A/zh active Pending
- 2013-12-20 PL PL13829059T patent/PL2941412T3/pl unknown
Also Published As
Publication number | Publication date |
---|---|
US20150344397A1 (en) | 2015-12-03 |
EP2941412B1 (de) | 2018-10-24 |
BR112015015931A2 (pt) | 2017-07-11 |
DE102013000027A1 (de) | 2014-07-03 |
PL2941412T3 (pl) | 2019-04-30 |
HUE042352T2 (hu) | 2019-06-28 |
EP2941412A2 (de) | 2015-11-11 |
MX2015008597A (es) | 2016-01-15 |
CN105073703A (zh) | 2015-11-18 |
MY185170A (en) | 2021-04-30 |
WO2014106532A2 (de) | 2014-07-10 |
WO2014106532A3 (de) | 2014-09-12 |
US9422220B2 (en) | 2016-08-23 |
BR112015015931B1 (pt) | 2020-10-20 |
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Legal Events
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FG | Grant or registration |