MX360039B - Proceso para purificar una corriente que comprende 1,4-butanodiol. - Google Patents

Proceso para purificar una corriente que comprende 1,4-butanodiol.

Info

Publication number
MX360039B
MX360039B MX2014002807A MX2014002807A MX360039B MX 360039 B MX360039 B MX 360039B MX 2014002807 A MX2014002807 A MX 2014002807A MX 2014002807 A MX2014002807 A MX 2014002807A MX 360039 B MX360039 B MX 360039B
Authority
MX
Mexico
Prior art keywords
stream
butanediol
distillation column
hydroxybutoxy
tetrahydrofuran
Prior art date
Application number
MX2014002807A
Other languages
English (en)
Other versions
MX2014002807A (es
Inventor
Graham Reed
Paul Gordon
Original Assignee
Johnson Matthey Davy Technologies Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Johnson Matthey Davy Technologies Ltd filed Critical Johnson Matthey Davy Technologies Ltd
Publication of MX2014002807A publication Critical patent/MX2014002807A/es
Publication of MX360039B publication Critical patent/MX360039B/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/001—Processes specially adapted for distillation or rectification of fermented solutions
    • B01D3/002—Processes specially adapted for distillation or rectification of fermented solutions by continuous methods
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C29/82—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by azeotropic distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C07C29/84—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation by extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
    • C07C29/90—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound using hydrogen only
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C07C31/207—1,4-Butanediol; 1,3-Butanediol; 1,2-Butanediol; 2,3-Butanediol
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Furan Compounds (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)

Abstract

Un proceso para purificar un chorro que comprende 1,4-butanodiol que comprende los pasos de: (a) proveer un chorro de producto en bruto que comprende 1,4-butandiol y uno o más de y-butirolactona, 2-(4- hidroxibutoxi)-tetrahidrofurano, 4-hidroxibutil(4-hidroxibut irato), y 3-(4- hidroxibutoxi)-tetrahidrofurano a una primera columna de destilación; (b) eliminar una gaveta lateral que comprende 1,4-butanodiol, y componentes livianos, dichos componentes livianos incluyendo por lo menos algunos de esos producidos por medio de la reacción en la primera columna de destilación; (c) pasar el chorro a una zona de hidrogenación; (d) someter el chorro de la etapa (c) a hidrogenación en la zona de hidrogenación en presencia de un catalizador de hidrogenación, y recuperar de la zona de hidrogenación un producto 1,4- butanodiol en chorro que tiene un contenido reducido de 2-(4-hidroxibutoxi)-t etrahidrofurano, y en forma opcional adicionalmente incluyendo (4-hidroxibutil)-4-hidroxibutirato formado por medio de la reacción de y-butirolactona; (e) pasar el chorro de producto 1,4- butanodiol de la etapa (d) a una segunda columna de hidrogenación operada de manera tal que (4-hidroxibutil)-4-hidroxibutirato se elimina como un chorro inferior y eliminar un chorro de 1 ,4-butanodiol en forma superior; y (f) pasar el chorro superior eliminado en (e) hasta una tercera columna de destilación y recuperar un chorro de 1 ,4-butanodiol purificado.
MX2014002807A 2011-09-09 2012-08-21 Proceso para purificar una corriente que comprende 1,4-butanodiol. MX360039B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GBGB1115617.1A GB201115617D0 (en) 2011-09-09 2011-09-09 Proacess
PCT/GB2012/052048 WO2013034881A1 (en) 2011-09-09 2012-08-21 Process for purifying a stream comprising 1,4- butanediol

Publications (2)

Publication Number Publication Date
MX2014002807A MX2014002807A (es) 2014-09-12
MX360039B true MX360039B (es) 2018-10-18

Family

ID=44908326

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2014002807A MX360039B (es) 2011-09-09 2012-08-21 Proceso para purificar una corriente que comprende 1,4-butanodiol.

Country Status (17)

Country Link
US (1) US10322988B2 (es)
EP (1) EP2753597B1 (es)
JP (1) JP2014530175A (es)
KR (1) KR101984335B1 (es)
CN (1) CN103796981B (es)
AR (1) AR087806A1 (es)
AU (1) AU2012306139A1 (es)
BR (1) BR112014005251B1 (es)
CA (1) CA2847228C (es)
EA (1) EA026323B1 (es)
ES (1) ES2705739T3 (es)
GB (2) GB201115617D0 (es)
MX (1) MX360039B (es)
MY (1) MY173499A (es)
SG (1) SG11201400238XA (es)
TW (1) TWI560174B (es)
WO (1) WO2013034881A1 (es)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108358755B (zh) * 2013-03-15 2021-08-10 基因组股份公司 用于从发酵肉汤中获得1,4-丁二醇的方法和系统
CN105418371A (zh) * 2015-11-10 2016-03-23 中国石化长城能源化工（宁夏）有限公司 一种1,4-丁二醇催化加氢脱色方法
GB201710508D0 (en) * 2017-06-30 2017-08-16 Johnson Matthey Davy Technologies Ltd Process
GB202203264D0 (en) 2022-03-09 2022-04-20 Johnson Matthey Davy Technologies Ltd Process for producing a refined 1,4-butanediol stream
CN114853573B (zh) * 2022-05-27 2023-06-13 辽宁石油化工大学 一种1,4-丁二醇的分离纯化方法与系统
CN114874074B (zh) * 2022-05-27 2023-06-13 辽宁石油化工大学 一种1,4-丁二醇的分离纯化工艺与系统
CN117843444A (zh) * 2023-12-26 2024-04-09 南京长江江宇环保科技股份有限公司 一种精制1, 4-丁二醇的工艺方法

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB8331793D0 (en) 1983-11-29 1984-01-04 Davy Mckee Ltd Process
GB8514002D0 (en) 1985-06-04 1985-07-10 Davy Mckee Ltd Process
JPH0635404B2 (ja) 1985-02-27 1994-05-11 三菱化成株式会社 粗１，４−ブタンジオ−ルの精製方法
GB8618888D0 (en) 1986-08-01 1986-09-10 Davy Mckee Ltd Process
WO1988000937A1 (en) 1986-08-01 1988-02-11 Davy Mckee (London) Limited Process for the co-production of butane-1,4-diol and gamma-butyrolactone
BR9007038A (pt) 1989-01-17 1991-11-12 Davy Mckee London Processo e aparelho
GB8917864D0 (en) 1989-08-04 1989-09-20 Davy Mckee London Process
DE3938121A1 (de) * 1989-11-16 1991-05-23 Basf Ag Verfahren zur abtrennung von (alpha)-butyrolacton aus gemischen, die bernsteinsaeurediethylester enthalten
JP3175360B2 (ja) * 1992-12-10 2001-06-11 三菱化学株式会社 １，４−ブタンジオールの精製方法
JP2934173B2 (ja) * 1995-08-25 1999-08-16 東燃化学株式会社 高純度１，４−ブタンジオールの製造方法
KR100500858B1 (ko) * 1996-03-29 2005-11-08 데이비 프로세스 테크놀로지 리미티드 부탄-1,4-디올의정제방법
ZA972614B (en) * 1996-03-29 1997-12-22 Kvaerner Process Tech Ltd Process for the production of butane-1,4-diol.
JPH10265418A (ja) * 1997-01-23 1998-10-06 Mitsubishi Chem Corp 粗１，４−ブタンジオールの精製方法
SG65043A1 (en) 1997-01-23 1999-05-25 Mitsubishi Chem Corp Process for purifying crude 1,4-butanediol
DE10021703A1 (de) 2000-05-04 2001-11-08 Basf Ag Verfahren zur destillativen Trennung von Tetrahydrofuran, gamma-Butyrolacton und/oder 1,4-Butandiol enthaltenden Gemischen
JP3998440B2 (ja) * 2001-07-17 2007-10-24 三菱化学株式会社 １，４−ブタンジオールの製造方法
JP3959993B2 (ja) 2001-08-01 2007-08-15 三菱化学株式会社 １，４−ブタンジオールの製造方法
GB0421928D0 (en) 2004-10-01 2004-11-03 Davy Process Techn Ltd Process
KR20090110879A (ko) * 2007-02-15 2009-10-22 바스프 에스이 매우 순수한 1,4-부탄디올의 제조 방법

Also Published As

Publication number Publication date
GB201404911D0 (en) 2014-04-30
CN103796981B (zh) 2016-05-18
CA2847228C (en) 2016-05-17
EP2753597B1 (en) 2018-10-17
EP2753597A1 (en) 2014-07-16
SG11201400238XA (en) 2014-03-28
GB201115617D0 (en) 2011-10-26
US20140350308A1 (en) 2014-11-27
ES2705739T3 (es) 2019-03-26
WO2013034881A1 (en) 2013-03-14
BR112014005251B1 (pt) 2020-10-06
NZ621826A (en) 2015-02-27
TWI560174B (en) 2016-12-01
AR087806A1 (es) 2014-04-16
CA2847228A1 (en) 2013-03-14
CN103796981A (zh) 2014-05-14
EA201490581A1 (ru) 2014-09-30
KR101984335B1 (ko) 2019-05-30
BR112014005251A2 (pt) 2017-04-04
GB2541350A (en) 2017-02-22
EA026323B1 (ru) 2017-03-31
KR20140095468A (ko) 2014-08-01
TW201311626A (zh) 2013-03-16
MX2014002807A (es) 2014-09-12
AU2012306139A1 (en) 2014-03-13
MY173499A (en) 2020-01-29
JP2014530175A (ja) 2014-11-17
US10322988B2 (en) 2019-06-18

Similar Documents

Publication Publication Date Title
MX360039B (es) Proceso para purificar una corriente que comprende 1,4-butanodiol.
TW200704635A (en) Process for the production of acetic acid
BRPI0506587A (pt) processo para a preparação de 3-pentenonitrila
FI20115217L (fi) Menetelmä polttoainekomponenttien tuottamiseksi
BR112012019032A2 (pt) "processo para purificação de etanol"
MX2009005158A (es) Proceso para separar fluoruro de hidrogeno a partir de corrientes de alimentacion organicas.
MX2013012674A (es) Proceso integrado para la produccion de 1 - cloro - 3, 3, 3 - trifluoropropeno.
WO2013169811A3 (en) Biogenic activated carbon and methods of making and using same
WO2008130974A3 (en) System and process for producing biodiesel
NO20072248L (no) Prosess til rensing av 1,4-butandiol
MY154900A (en) Method for the production of very pure 1, 4-butanediol
BR112013027340A2 (pt) processo para recuperar álcool com redução de água do topo de uma coluna de ácido
WO2009032552A3 (en) Method of reducing methanol in recycle streams in bisphenol-a-production process
MX2021005608A (es) Proceso para recuperar acetonitrilo de corrientes residuales de acetonitrilo.
WO2007069109A3 (en) Method and apparatus for producing purified methyl isobutyl ketone
MX2023004496A (es) Procesos para purificar acido acetico e hidratar un anhidrido.
EA201791013A1 (ru) Способ получения циклогексанона из фенола
MY140932A (en) Method for producing phthalic anhydride that conforms to specifications
SA518391246B1 (ar) عملية لتنقية ميث أكريلات الميثيل
WO2012149156A3 (en) Process to reduce ethanol recycled to acetic acid hydrogenation reactor
MY155146A (en) Process for the treatment of the aqueous stream coming from the fischer-tropsch reaction
SA521421132B1 (ar) عملية لتنقية سيانيد الهيدروجين
MX2023002639A (es) Proceso para recuperar acetonitrilo.
MX2022008198A (es) Procedimiento para separar tricianohexano.
MX2022008202A (es) Métodos de purificación del tricianohexano.

Legal Events

Date Code Title Description
FG Grant or registration