MX2017011729A - Digestor basado en reactor de columna de burbujeo y metodo para su uso. - Google Patents

Digestor basado en reactor de columna de burbujeo y metodo para su uso.

Info

Publication number
MX2017011729A
MX2017011729A MX2017011729A MX2017011729A MX2017011729A MX 2017011729 A MX2017011729 A MX 2017011729A MX 2017011729 A MX2017011729 A MX 2017011729A MX 2017011729 A MX2017011729 A MX 2017011729A MX 2017011729 A MX2017011729 A MX 2017011729A
Authority
MX
Mexico
Prior art keywords
bubble column
digestion
column reactor
andmethod
oxidation
Prior art date
Application number
MX2017011729A
Other languages
English (en)
Inventor
G Wonders Alan
Original Assignee
Grupo Petrotemex Sa De Cv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Grupo Petrotemex Sa De Cv filed Critical Grupo Petrotemex Sa De Cv
Publication of MX2017011729A publication Critical patent/MX2017011729A/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/002—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out in foam, aerosol or bubbles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/242—Tubular reactors in series
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
    • C07C63/14—Monocyclic dicarboxylic acids
    • C07C63/15—Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
    • C07C63/26—1,4 - Benzenedicarboxylic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00777—Baffles attached to the reactor wall horizontal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Se proporciona un método para digestión de una suspensión de ácido tereftálico crudo obtenida de la oxidación de para-xileno en un proceso de oxidación de reactor de columna de burbujeo. El método se conduce en uno o más reactores de columna de burbujeo que tiene una o más zonas segregadas definidas por deflectores horizontales y el flujo de partículas a través del sistema de digestión se controla para maximizar la conversión de los intermediarios de oxidación parcial a ácido tereftálico mientras que se minimiza la formación de otros productos contaminantes. La temperatura, el flujo de oxígeno y el contenido así como otras variables del proceso y del equipo se controlan por todo el proceso para soportar la formación del ácido tereftálico. También se proporcionan sistemas de digestión de columna de burbujeo estructurados para conducir el método de digestión.
MX2017011729A 2015-03-13 2016-03-11 Digestor basado en reactor de columna de burbujeo y metodo para su uso. MX2017011729A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US14/657,523 US20160264511A1 (en) 2015-03-13 2015-03-13 Bubble column reactor based digester and method for its use
PCT/US2016/021912 WO2016149060A1 (en) 2015-03-13 2016-03-11 Bubble column reactor based digester andmethod for its use

Publications (1)

Publication Number Publication Date
MX2017011729A true MX2017011729A (es) 2017-11-13

Family

ID=56887404

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2017011729A MX2017011729A (es) 2015-03-13 2016-03-11 Digestor basado en reactor de columna de burbujeo y metodo para su uso.

Country Status (16)

Country Link
US (1) US20160264511A1 (es)
EP (1) EP3268341B1 (es)
JP (1) JP6882182B2 (es)
KR (1) KR20170128462A (es)
CN (1) CN107531602B (es)
BR (1) BR112017019452B1 (es)
CA (1) CA2979681A1 (es)
EA (1) EA034735B1 (es)
ES (1) ES2880688T3 (es)
LT (1) LT3268341T (es)
MX (1) MX2017011729A (es)
MY (1) MY188141A (es)
PL (1) PL3268341T3 (es)
PT (1) PT3268341T (es)
SG (2) SG11201707399XA (es)
WO (1) WO2016149060A1 (es)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US11203769B1 (en) * 2017-02-13 2021-12-21 Solugen, Inc. Hydrogen peroxide and gluconic acid production
US10000435B1 (en) * 2017-02-28 2018-06-19 Grupo Petrotemex, S.A. De C.V. Energy and environmentally integrated method for production of aromatic dicarboxylic acids by oxidation

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5200557A (en) * 1991-04-12 1993-04-06 Amoco Corporation Process for preparation of crude terephthalic acid suitable for reduction to prepare purified terephthalic acid
DE19843573A1 (de) * 1998-09-23 2000-03-30 Degussa Blasensäule und deren Verwendung
US7196215B2 (en) * 2001-06-04 2007-03-27 Eastman Chemical Company Process for the production of purified terephthalic acid
US7683210B2 (en) * 2004-09-02 2010-03-23 Eastman Chemical Company Optimized liquid-phase oxidation
US7608732B2 (en) * 2005-03-08 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7355068B2 (en) * 2006-01-04 2008-04-08 Eastman Chemical Company Oxidation system with internal secondary reactor
US7816556B2 (en) * 2006-03-01 2010-10-19 Eastman Chemical Company Polycarboxylic acid production system employing enhanced multistage oxidative digestion
CN101531588B (zh) * 2008-03-13 2016-02-24 周向进 一种新的精对苯二甲酸的制造方法
CN202700501U (zh) 2012-05-15 2013-01-30 中国昆仑工程公司 适于kpta生产的无搅拌氧化和深度氧化反应系统
CN102731297B (zh) * 2012-07-11 2014-06-04 浙江大学 一种逐级升温氧化制备中纯度对苯二甲酸的方法

Also Published As

Publication number Publication date
ES2880688T3 (es) 2021-11-25
CN107531602A (zh) 2018-01-02
PL3268341T3 (pl) 2021-11-02
BR112017019452B1 (pt) 2020-11-17
SG10201908521RA (en) 2019-11-28
US20160264511A1 (en) 2016-09-15
EP3268341A4 (en) 2018-10-31
WO2016149060A1 (en) 2016-09-22
EP3268341A1 (en) 2018-01-17
JP2018513125A (ja) 2018-05-24
LT3268341T (lt) 2021-07-26
JP6882182B2 (ja) 2021-06-02
PT3268341T (pt) 2021-06-30
SG11201707399XA (en) 2017-10-30
EA034735B1 (ru) 2020-03-13
BR112017019452A2 (pt) 2018-05-15
EP3268341B1 (en) 2021-04-21
MY188141A (en) 2021-11-23
KR20170128462A (ko) 2017-11-22
CN107531602B (zh) 2021-02-12
EA201792031A1 (ru) 2018-02-28
CA2979681A1 (en) 2016-09-22

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