MX2007013763A - Calcinacion en un gas inerte en presencia de una concentracion pequena de un componente oxidante. - Google Patents
Calcinacion en un gas inerte en presencia de una concentracion pequena de un componente oxidante.Info
- Publication number
- MX2007013763A MX2007013763A MX2007013763A MX2007013763A MX2007013763A MX 2007013763 A MX2007013763 A MX 2007013763A MX 2007013763 A MX2007013763 A MX 2007013763A MX 2007013763 A MX2007013763 A MX 2007013763A MX 2007013763 A MX2007013763 A MX 2007013763A
- Authority
- MX
- Mexico
- Prior art keywords
- silver
- containing compound
- inert gas
- oxidizing component
- calcination
- Prior art date
Links
- 239000011261 inert gas Substances 0.000 title abstract 2
- 230000001590 oxidative effect Effects 0.000 title abstract 2
- 238000001354 calcination Methods 0.000 title 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 abstract 5
- 229910052709 silver Inorganic materials 0.000 abstract 5
- 239000004332 silver Substances 0.000 abstract 5
- 150000001875 compounds Chemical class 0.000 abstract 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- 239000001301 oxygen Substances 0.000 abstract 2
- 229910052760 oxygen Inorganic materials 0.000 abstract 2
- 230000001737 promoting effect Effects 0.000 abstract 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 abstract 1
- 239000005977 Ethylene Substances 0.000 abstract 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000007789 gas Substances 0.000 abstract 1
- 239000011368 organic material Substances 0.000 abstract 1
- 229910052723 transition metal Inorganic materials 0.000 abstract 1
- 150000003624 transition metals Chemical class 0.000 abstract 1
- 239000012808 vapor phase Substances 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/66—Silver or gold
- B01J23/68—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/04—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen
- C07D301/08—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase
- C07D301/10—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with air or molecular oxygen in the gaseous phase with catalysts containing silver or gold
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/66—Silver or gold
- B01J23/68—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/683—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with chromium, molybdenum or tungsten
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/66—Silver or gold
- B01J23/68—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/688—Silver or gold with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with manganese, technetium or rhenium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0201—Impregnation
- B01J37/0203—Impregnation the impregnation liquid containing organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/08—Heat treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
- B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/66—Silver or gold
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/12—Oxidising
- B01J37/14—Oxidising with gases containing free oxygen
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Catalysts (AREA)
- Epoxy Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La presente invencion se refiere a un proceso mejorado para preparar catalizadores de plata utiles para produccion en fase de vapor de oxido de etileno desde etileno y oxigeno. Un soporte inerte es impregnado con una solucion de una cantidad cataliticamente efectiva de un compuesto que contiene plata, una cantidad promotora de un compuesto que contiene metal alcalino, y una cantidad promotora de un compuesto que contiene metal de transicion. El soporte impregnado es calcinado mediante calentamiento a una temperatura desde 200 degree Chasta aproximadamente 600 degree Cpara convertir la plata del compuesto que contiene plata, en plata metalica y descomponer y remover sustancialmente todos los materiales organicos. El calentamiento se lleva a cabo bajo una atmosfera que comprende una combinacion de un gas inerte y desde 10 ppm hasta aproximadamente 5% por volumen de un gas del componente oxidante que contiene oxigeno.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11/124,646 US7759284B2 (en) | 2005-05-09 | 2005-05-09 | Calcination in an inert gas in the presence of a small concentration of an oxidizing component |
PCT/IB2006/002030 WO2007000664A1 (en) | 2005-05-09 | 2006-05-05 | Calcination in an inert gas in the presence of a small concentration of an oxidizing component |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2007013763A true MX2007013763A (es) | 2008-04-07 |
Family
ID=37394740
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2007013763A MX2007013763A (es) | 2005-05-09 | 2006-05-05 | Calcinacion en un gas inerte en presencia de una concentracion pequena de un componente oxidante. |
Country Status (11)
Country | Link |
---|---|
US (1) | US7759284B2 (es) |
EP (1) | EP1893331B1 (es) |
JP (1) | JP4981792B2 (es) |
KR (1) | KR101324286B1 (es) |
CN (1) | CN101171080B (es) |
AR (1) | AR054356A1 (es) |
BR (1) | BRPI0611295A2 (es) |
MX (1) | MX2007013763A (es) |
RU (1) | RU2411997C2 (es) |
TW (1) | TWI385028B (es) |
WO (1) | WO2007000664A1 (es) |
Families Citing this family (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8097557B2 (en) * | 2006-08-08 | 2012-01-17 | Sd Lizenverwertungsgesellschaft Mbh & Co. Kg | Two-stage calcination for catalyst production |
DE102008014910A1 (de) * | 2008-03-19 | 2009-09-24 | Basf Se | Verwendung eines geträgerten edelmetallhaltigen Katalysators zur oxidativen Dehydrierung |
CN102177145B (zh) * | 2008-10-08 | 2014-07-30 | 巴斯夫欧洲公司 | 生产烯化氧的方法 |
US20110152073A1 (en) * | 2009-12-23 | 2011-06-23 | Scientific Design Company, Inc. | Epoxidation process and microstructure |
TW201208763A (en) | 2010-05-17 | 2012-03-01 | Scient Design Co | Method for making a highly selective ethylene oxide catalyst |
TW201213013A (en) | 2010-05-17 | 2012-04-01 | Scient Design Co | Method for preparing an epoxidation catalyst |
WO2014105924A1 (en) * | 2012-12-31 | 2014-07-03 | Scientific Design Company, Inc. | Calcination process for producing an improved ethylene oxide catalyst |
WO2018017453A1 (en) * | 2016-07-18 | 2018-01-25 | Scientific Design Company, Inc. | Epoxidation process |
US11439986B2 (en) * | 2017-12-13 | 2022-09-13 | Scientific Design Company, Inc. | Silver impregnation solution containing high-boiling oxygenated additive and its use in ethylene oxide catalyst preparation |
TWI808125B (zh) | 2018-02-07 | 2023-07-11 | 德商巴斯夫歐洲公司 | 有效地將乙烯氧化轉化為環氧乙烷之催化劑 |
DK3749449T3 (da) | 2018-02-07 | 2022-04-19 | Basf Se | Fremgangsmåde til fremstilling af en sølvimprægnerings-opløsning |
EP3639923A1 (en) | 2018-10-15 | 2020-04-22 | Basf Se | Process for producing ethylene oxide by gas-phase oxidation of ethylene |
EP3639924A1 (en) | 2018-10-15 | 2020-04-22 | Basf Se | Catalyst for producing ethylene oxide by gas-phase oxidation |
EP3659703A1 (en) | 2018-11-28 | 2020-06-03 | Basf Se | Catalyst for producing ethylene oxide by gas-phase oxidation |
CN109574133A (zh) * | 2018-12-29 | 2019-04-05 | 重庆科技学院 | 有机废水光降解方法 |
WO2021038027A1 (en) | 2019-08-28 | 2021-03-04 | Basf Se | Process for preparing an epoxidation catalyst |
EP3885038A1 (en) | 2020-03-27 | 2021-09-29 | Basf Se | Process for producing an epoxidation catalyst |
WO2021191414A1 (en) * | 2020-03-27 | 2021-09-30 | Basf Se | Process for producing a silver-based epoxidation catalyst |
JP2023532004A (ja) | 2020-06-26 | 2023-07-26 | ビーエーエスエフ ソシエタス・ヨーロピア | 多孔質アルファ-アルミナ触媒支持体を生成する方法 |
US20230256420A1 (en) | 2020-06-26 | 2023-08-17 | Basf Se | Shaped catalyst body for the production of ethylene oxide |
US20230256415A1 (en) | 2020-06-26 | 2023-08-17 | Basf Se | Production of porous alpha-alumina supports from boehmitic derived aluminas |
EP4284552A1 (en) | 2021-01-26 | 2023-12-06 | Basf Se | Epoxidation catalyst |
WO2022268348A1 (en) | 2021-06-25 | 2022-12-29 | Basf Se | High purity tableted alpha-alumina catalyst support |
TW202421267A (zh) | 2022-10-12 | 2024-06-01 | 德商巴斯夫歐洲公司 | 環氧化催化劑 |
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US3702309A (en) | 1954-08-13 | 1972-11-07 | Karl Ziegler | Polymerization of ethylene using reduced group iv-b,v-b and vi-b metal salts as the polymerization catalyst |
US4774222A (en) * | 1982-06-16 | 1988-09-27 | Scientific Design Company, Inc. | Catalyst for oxidation of ethylene to ethylene oxide and process for preparing the catalyst |
US4820675A (en) * | 1986-10-31 | 1989-04-11 | Shell Oil Company | Ethylene oxide catalyst & process for preparing the catalyst |
US4766105A (en) * | 1986-10-31 | 1988-08-23 | Shell Oil Company | Ethylene oxide catalyst and process for preparing the catalyst |
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GB8626687D0 (en) * | 1986-11-07 | 1986-12-10 | Shell Int Research | Preparing silver catalyst |
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US5602070A (en) * | 1995-01-09 | 1997-02-11 | Scientific Design Company, Inc. | Process for preparing silver catalyst |
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DE19803890A1 (de) * | 1998-01-31 | 1999-08-05 | Erdoelchemie Gmbh | Silberhaltige Trägerkatalysatoren und Katalysator-Zwischenprodukte, Verfahren zu ihrer Herstellung und ihre Verwendung |
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US20060293180A1 (en) * | 2003-08-22 | 2006-12-28 | Thorsteinson Erlind M | Modified alumina carriers and silver-based catalysts for the production of alkylene oxides |
-
2005
- 2005-05-09 US US11/124,646 patent/US7759284B2/en active Active
-
2006
- 2006-04-18 TW TW095113805A patent/TWI385028B/zh not_active IP Right Cessation
- 2006-05-05 BR BRPI0611295-1A patent/BRPI0611295A2/pt not_active IP Right Cessation
- 2006-05-05 RU RU2007145501/04A patent/RU2411997C2/ru not_active IP Right Cessation
- 2006-05-05 JP JP2008510672A patent/JP4981792B2/ja not_active Expired - Fee Related
- 2006-05-05 EP EP06795157.4A patent/EP1893331B1/en active Active
- 2006-05-05 CN CN2006800155627A patent/CN101171080B/zh not_active Expired - Fee Related
- 2006-05-05 KR KR1020077024009A patent/KR101324286B1/ko not_active IP Right Cessation
- 2006-05-05 MX MX2007013763A patent/MX2007013763A/es active IP Right Grant
- 2006-05-05 WO PCT/IB2006/002030 patent/WO2007000664A1/en active Application Filing
- 2006-05-09 AR ARP060101856A patent/AR054356A1/es active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
JP2008540098A (ja) | 2008-11-20 |
TW200642756A (en) | 2006-12-16 |
US7759284B2 (en) | 2010-07-20 |
WO2007000664A1 (en) | 2007-01-04 |
CN101171080A (zh) | 2008-04-30 |
US20060252639A1 (en) | 2006-11-09 |
EP1893331B1 (en) | 2013-07-10 |
EP1893331A1 (en) | 2008-03-05 |
KR20080005505A (ko) | 2008-01-14 |
TWI385028B (zh) | 2013-02-11 |
RU2411997C2 (ru) | 2011-02-20 |
JP4981792B2 (ja) | 2012-07-25 |
RU2007145501A (ru) | 2009-06-20 |
BRPI0611295A2 (pt) | 2010-08-31 |
KR101324286B1 (ko) | 2013-11-01 |
AR054356A1 (es) | 2007-06-20 |
CN101171080B (zh) | 2012-07-11 |
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